Patent classifications
C01F7/16
METHOD FOR MANUFACTURING CRYSTALS OF ALUMINATE OF AT LEAST ONE METAL AND/OR ONE METALLOID AND/OR ONE LANTHANIDE, AND APPLICATIONS OF SAME
Disclosed is a method for manufacturing crystals of aluminates of one or more element(s) other than aluminium, referred to as A. The method includes: placing starting reagents, including at least one aluminium element source and a source of the element(s) A that has a degree of oxidation of between 1 and 6, in suspension in a liquid medium, forming a suspension referred to as the starting suspension; milling the starting suspension at 50 C., in a three-dimensional liquid medium ball mill for 5 minutes; recovering, at the outlet of the three-dimensional ball mill, a suspension referred to as the end suspension including the starting reagents in activated form or crystals of aluminate of the element(s) A generally in hydrated form; if required, calcination of the end suspension when it includes the starting reagents in activated form, to obtain generally non-hydrated crystals of aluminate of the element(s) A.
Mg-doped ALUMINA AEROGEL AND MANUFACTURING METHOD THEREOF
A Mg-doped alumina aerogel and a manufacturing method thereof are provided. The Mg-doped alumina aerogel is a three-dimensional cross-linked network structure including a plurality of magnesium atoms, a plurality of aluminum atoms, a plurality of oxygen atoms, and a plurality of hydrogen atoms. The three-dimensional cross-linked network structure has a MgOAl bond at least on the main chain.
LOW-COST PROCESS OF MANUFACTURING TRANSPARENT SPINEL
The invention provides ballistic-resistant transparent objects of complex shapes consisting of magnesium aluminate spinel. The invention also provides a cost-effective industrial process for making the objects, including slip casting and sintering.
Aluminum hydroxide coagulant recovery from water/wastewater treatment sludge
A method for recovery of aluminum hydroxide Al(OH).sub.3 from an aluminum enriched water/wastewater treatment sludge is disclosed. The method includes the steps of: adding a hydrated lime slurry to the aluminum enriched water/wastewater treatment sludge to form an alkaline sludge; adding sodium carbonate Na.sub.2CO.sub.3 to the alkaline sludge to form a Na.sub.2CO.sub.3 treated sludge; forming a first supernatant from the Na.sub.2CO.sub.3 treated sludge of step b) containing NaAl(OH).sub.4; introducing CO.sub.2 to the first supernatant to form a precipitate of Al(OH).sub.3 and a second supernatant containing NaHCO.sub.3; and recycling at least a portion of the NaHCO.sub.3 from the second supernatant back to the alkaline sludge of step a).
ALUMINUM HYDROXIDE COAGULANT RECOVERY FROM WATER/WASTEWATER TREATMENT SLUDGE
A method for recovery of aluminum hydroxide Al(OH).sub.3 from an aluminum enriched water/wastewater treatment sludge is disclosed. The method includes the steps of: adding a hydrated lime slurry to the aluminum enriched water/wastewater treatment sludge to form an alkaline sludge; adding sodium carbonate Na.sub.2CO.sub.3 to the alkaline sludge to form a Na.sub.2CO.sub.3 treated sludge; forming a first supernatant from the Na.sub.2CO.sub.3 treated sludge of step b) containing NaAl(OH).sub.4; introducing CO.sub.2 to the first supernatant to form a precipitate of Al(OH).sub.3 and a second supernatant containing NaHCO.sub.3; and recycling at least a portion of the NaHCO.sub.3 from the second supernatant back to the alkaline sludge of step a).
NOx trap catalyst support material with improved stability against BaAl2O4 formation
The present invention relates to a method for the production of a support material for a nitrogen oxide storage component that is applicable in catalysts for treating exhaust gases from lean-burn engines and a support material made according to said process that is stable against the reaction with a Barium compound to form BaAl.sub.2O.sub.4.
Method for producing conductive mayenite compound powder having large specific surface area
If a conductive mayenite compound having a large specific surface area is obtained, the usefulness thereof in respective applications is remarkably increased. A conductive mayenite compound powder having a conduction electron density of 10.sup.15 cm.sup.?3 or more and a specific surface area of 5 m.sup.2g.sup.?1 or more is produced by: the following steps: (1) forming a precursor powder by subjecting a mixture of a starting material powder and water to a hydrothermal treatment; (2) forming a mayenite compound powder by heating and dehydrating the precursor powder; (3) forming an activated mayenite compound powder by heating the compound powder in an inert gas atmosphere or in a vacuum; and (4) injecting electrons into the mayenite compound through a reduction treatment by mixing the activated mayenite compound powder with a reducing agent.
Method of producing magnesium aluminate spinels
The invention provides for a method of making a magnesium aluminate spinel including an alumina compound and a magnesium compound, the method including the steps of; dispersing the alumina compound by dispersing it in a aqueous solution, to form an alumina dispersion, the aqueous solution having a pH of between 2 and 5; preferably between 2 and 4, flocculating the alumina by increasing the pH of the alumina dispersion to a pH of between 8 and 10 by adding a base; adding the alumina dispersion to an aqueous dispersion of the magnesium compound to form a slurry; drying the slurry to produce a dried spinel precursor; and calcining the dried spinel precursor to produce the magnesium aluminate spinel. Dispersing at such a low pH results in a conversion to spinel as well as allows for the control of the surface area of the spinel.
Monolithic bodies of sintered chemically bonded ceramic (CBC) biomaterial prepared ex vivo for implantation, preparation and use thereof
The present invention generally relates to the use of pre-formed bodies of Chemically Bonded Ceramics (CBCs) biomaterial for implantation purposes wherein the bodies are prepared ex vivo allowing process parameters to be optimized for desired long term properties of the resulting CBC biomaterial. More particularly, the pre-formed CBC material bodies of the present invention are sintered. The pre-formed body of CBC material is machined to the desired geometry and then implanted using a CBC cementation paste for fixation of the body to tissue. The invention also relates to a method of preparing pre-formed bodies of CBC biomaterial for implantation purposes, methods of preparing an implant thereof having desired geometry, and a method of implantation of the implant, as well as a kit for use in the method of implantation.
AEROSOL-BASED HIGH-TEMPERATURE SYNTHESIS OF MATERIALS
A material synthesis method may comprise: adding at least one liquid precursor solution to an atomizer device; generating by the atomizer device an aerosol comprising liquid droplets; transporting the aerosol to a reactive zone for evaporating one or more solvents from the aerosol; and collecting particles synthesized from at least evaporating the aerosol.