Patent classifications
C01F7/42
Method of producing a highly-pure aluminum hydroxide
A method of producing a highly-pure aluminum hydroxide, comprising the following steps: (1) reacting alcohol with metal aluminum to produce aluminum alkoxide, then hydrolyzing the aluminum alkoxide with water to produce an aluminum hydroxide slurry and an alcohol, filtering the aluminum hydroxide slurry, washing a resulting filter cake with water to remove the alcohol trapped therein, and drying the filter cake after the water washing to produce an aluminum hydroxide powder, (2) sending the alcohol-containing water produced in step (1) to an alcohol extraction unit for separating water and alcohol through extraction, and sending the separated water back to step (1) for recycling, (3) dehydrating the hydrous alcohol produced by hydrolyzing the aluminum alkoxide in step (1) before using it as the raw materials for reacting metal aluminum with alcohol to produce aluminum alkoxide in step (1). The method can improve the recovery of alcohol, reduce the production cost of a highly-pure aluminum hydroxide, improve the purity of aluminum oxide and achieve a zero discharge of sewage by recycling water.
Method of producing a highly-pure aluminum hydroxide
A method of producing a highly-pure aluminum hydroxide, comprising the following steps: (1) reacting alcohol with metal aluminum to produce aluminum alkoxide, then hydrolyzing the aluminum alkoxide with water to produce an aluminum hydroxide slurry and an alcohol, filtering the aluminum hydroxide slurry, washing a resulting filter cake with water to remove the alcohol trapped therein, and drying the filter cake after the water washing to produce an aluminum hydroxide powder, (2) sending the alcohol-containing water produced in step (1) to an alcohol extraction unit for separating water and alcohol through extraction, and sending the separated water back to step (1) for recycling, (3) dehydrating the hydrous alcohol produced by hydrolyzing the aluminum alkoxide in step (1) before using it as the raw materials for reacting metal aluminum with alcohol to produce aluminum alkoxide in step (1). The method can improve the recovery of alcohol, reduce the production cost of a highly-pure aluminum hydroxide, improve the purity of aluminum oxide and achieve a zero discharge of sewage by recycling water.
METHOD OF OBTAINING METAL-CONTAINING NANOPARTICLES
A method for obtaining aluminum-containing nanoparticles is provided. The method includes exposing at least one surface comprising aluminum to an alkaline aqueous solution. The method further includes exposing the at least one surface to electro-hydraulic shock waves and an electron flux. The at least one surface undergoes electro-erosion which creates alumina-hydrated nanoparticles having a negative surface electrical charge. The method further includes transforming the alumina-hydrated nanoparticles into aquachelate nanoparticles by attaching water molecules to the alumina-hydrated nanoparticles
METHOD OF OBTAINING METAL-CONTAINING NANOPARTICLES
A method for obtaining aluminum-containing nanoparticles is provided. The method includes exposing at least one surface comprising aluminum to an alkaline aqueous solution. The method further includes exposing the at least one surface to electro-hydraulic shock waves and an electron flux. The at least one surface undergoes electro-erosion which creates alumina-hydrated nanoparticles having a negative surface electrical charge. The method further includes transforming the alumina-hydrated nanoparticles into aquachelate nanoparticles by attaching water molecules to the alumina-hydrated nanoparticles
Methods for producing hollow ceramic spheres
A method is presented for producing hollow microspheres of metal oxides (HMOMS) and/or hollow metal silicates microspheres (HMSMS) in a transforming solution. The transforming solution contains an atom M, or an M-ion, or a radical containing M. M in the transforming solution has the thermodynamic ability to replace silicon atoms in hollow silica microspheres (HSMS) and/or hollow glass microspheres (HGMS). The maximum temperature for transformation is set by the chemical physical properties of the transforming solution, and the viscosity of the silica in the walls of the HSMS and/or the glass in the walls of the HGMS. Viscosity, of enough magnitude, helps retain the desired shape of the hollow sphere as it is transformed to HMOMS and/or HMSMS. Non-spherical shapes can be produced by increasing the transformation temperature whereby the viscosity of the walls of the HSMS and/or the HGMS is reduced. Transformation can take place at a single temperature or at several temperatures, each temperature for a separate hold time. Methods are presented for: 1. production of micro composite castings and continuous production of sheets of micro composites, both consisting of hollow spheres in a matrix, 2. harvesting of HMOMS and HMSMS, and 3. specialty castings for anisotropic properties using 3-dimensional printing.
Methods for producing hollow ceramic spheres
A method is presented for producing hollow microspheres of metal oxides (HMOMS) and/or hollow metal silicates microspheres (HMSMS) in a transforming solution. The transforming solution contains an atom M, or an M-ion, or a radical containing M. M in the transforming solution has the thermodynamic ability to replace silicon atoms in hollow silica microspheres (HSMS) and/or hollow glass microspheres (HGMS). The maximum temperature for transformation is set by the chemical physical properties of the transforming solution, and the viscosity of the silica in the walls of the HSMS and/or the glass in the walls of the HGMS. Viscosity, of enough magnitude, helps retain the desired shape of the hollow sphere as it is transformed to HMOMS and/or HMSMS. Non-spherical shapes can be produced by increasing the transformation temperature whereby the viscosity of the walls of the HSMS and/or the HGMS is reduced. Transformation can take place at a single temperature or at several temperatures, each temperature for a separate hold time. Methods are presented for: 1. production of micro composite castings and continuous production of sheets of micro composites, both consisting of hollow spheres in a matrix, 2. harvesting of HMOMS and HMSMS, and 3. specialty castings for anisotropic properties using 3-dimensional printing.
Method to recycle plastics, electronics, munitions or propellants using a metal reactant alloy composition
This invention relates to a method and apparatus for recycling plastics, electronics, munitions or propellants. In particular, the method comprises reacting a feed stock with a molten aluminum or aluminum alloy bath. The apparatus includes a reaction vessel for carrying out the reaction, as well as other equipment necessary for capturing and removing the reaction products. Further, the process can be used to cogenerate electricity using the excess heat generated by the process.
Method to recycle plastics, electronics, munitions or propellants using a metal reactant alloy composition
This invention relates to a method and apparatus for recycling plastics, electronics, munitions or propellants. In particular, the method comprises reacting a feed stock with a molten aluminum or aluminum alloy bath. The apparatus includes a reaction vessel for carrying out the reaction, as well as other equipment necessary for capturing and removing the reaction products. Further, the process can be used to cogenerate electricity using the excess heat generated by the process.
COMBINED MATERIAL INCLUDING ANODIC POROUS ALUMINA AND A POLYMER MATRIX, AND ITS USE FOR THE DENTAL RECONDITION
The present invention relates to anodic porous alumina (APA) in the form of microparticles, characterized in that it contains interconnected through nanopores, and to its use in the preparation of a new composite material, which is useful for example in the field of conservative dentistry. The invention further relates to a process for preparing the nanoporous alumina of the invention in microparticles.
COMBINED MATERIAL INCLUDING ANODIC POROUS ALUMINA AND A POLYMER MATRIX, AND ITS USE FOR THE DENTAL RECONDITION
The present invention relates to anodic porous alumina (APA) in the form of microparticles, characterized in that it contains interconnected through nanopores, and to its use in the preparation of a new composite material, which is useful for example in the field of conservative dentistry. The invention further relates to a process for preparing the nanoporous alumina of the invention in microparticles.