Patent classifications
C01F17/32
Method for producing high-purity scandium oxide
Provided is a method for obtaining high-purity scandium oxide efficiently from a solution containing scandium. The method for producing high-purity scandium oxide of the present invention has a first firing step S12 for subjecting a solution containing scandium to oxalation treatment using oxalic acid and firing the obtained crystals of scandium oxalate at a temperature of 400 to 600° C., inclusive, a dissolution step S13 for dissolving the scandium compound obtained by firing in one or more solutions selected from hydrochloric acid and nitric acid to obtain a solution, a reprecipitation step S14 for subjecting the solution to oxalation treatment using oxalic acid and generating a reprecipitate of scandium oxalate, and a second firing step S15 for firing the reprecipitate of obtained scandium oxalate to obtain scandium oxide.
Method for producing high-purity scandium oxide
Provided is a method for obtaining high-purity scandium oxide efficiently from a solution containing scandium. The method for producing high-purity scandium oxide of the present invention has a first firing step S12 for subjecting a solution containing scandium to oxalation treatment using oxalic acid and firing the obtained crystals of scandium oxalate at a temperature of 400 to 600° C., inclusive, a dissolution step S13 for dissolving the scandium compound obtained by firing in one or more solutions selected from hydrochloric acid and nitric acid to obtain a solution, a reprecipitation step S14 for subjecting the solution to oxalation treatment using oxalic acid and generating a reprecipitate of scandium oxalate, and a second firing step S15 for firing the reprecipitate of obtained scandium oxalate to obtain scandium oxide.
TRANSPARENT CERAMICS, MANUFACTURING METHOD THEREOF, AND MAGNETO-OPTICAL DEVICE
A transparent ceramic material is manufactured by molding a source powder into a compact, the source powder comprising a rare earth oxide consisting of at least 40 mol % of terbium oxide and the balance of another rare earth oxide, and a sintering aid, sintering the compact at a temperature T (1,300 C.T1,650 C.) by heating from room temperature to T1 (1200 C.T1T) at a rate of at least 100 C./h, and optionally heating from T1 at a rate of 1-95 C./h, and HIP treating the sintered compact at 1,300-1,650 C. The ceramic material has improved diffuse transmittance in the visible region and functions as a magneto-optical part in a broad visible to NIR region.
TRANSPARENT CERAMICS, MANUFACTURING METHOD THEREOF, AND MAGNETO-OPTICAL DEVICE
A transparent ceramic material is manufactured by molding a source powder into a compact, the source powder comprising a rare earth oxide consisting of at least 40 mol % of terbium oxide and the balance of another rare earth oxide, and a sintering aid, sintering the compact at a temperature T (1,300 C.T1,650 C.) by heating from room temperature to T1 (1200 C.T1T) at a rate of at least 100 C./h, and optionally heating from T1 at a rate of 1-95 C./h, and HIP treating the sintered compact at 1,300-1,650 C. The ceramic material has improved diffuse transmittance in the visible region and functions as a magneto-optical part in a broad visible to NIR region.
METHOD FOR PRODUCING HIGH-PURITY SCANDIUM OXIDE
Provided is a method for obtaining high-purity scandium oxide efficiently from a solution containing scandium. The method for producing high-purity scandium oxide of the present invention has a first firing step S12 for subjecting a solution containing scandium to oxalation treatment using oxalic acid and firing the obtained crystals of scandium oxalate at a temperature of 400 to 600 C., inclusive, a dissolution step S13 for dissolving the scandium compound obtained by firing in one or more solutions selected from hydrochloric acid and nitric acid to obtain a solution, a reprecipitation step S14 for subjecting the solution to oxalation treatment using oxalic acid and generating a reprecipitate of scandium oxalate, and a second firing step S15 for firing the reprecipitate of obtained scandium oxalate to obtain scandium oxide.
METHOD FOR PRODUCING HIGH-PURITY SCANDIUM OXIDE
Provided is a method for obtaining high-purity scandium oxide efficiently from a solution containing scandium. The method for producing high-purity scandium oxide of the present invention has a first firing step S12 for subjecting a solution containing scandium to oxalation treatment using oxalic acid and firing the obtained crystals of scandium oxalate at a temperature of 400 to 600 C., inclusive, a dissolution step S13 for dissolving the scandium compound obtained by firing in one or more solutions selected from hydrochloric acid and nitric acid to obtain a solution, a reprecipitation step S14 for subjecting the solution to oxalation treatment using oxalic acid and generating a reprecipitate of scandium oxalate, and a second firing step S15 for firing the reprecipitate of obtained scandium oxalate to obtain scandium oxide.
Transparent ceramics, manufacturing method thereof, and magneto-optical device
A transparent ceramic material is manufactured by molding a source powder into a compact, the source powder comprising a rare earth oxide consisting of at least 40 mol % of terbium oxide and the balance of another rare earth oxide, and a sintering aid, sintering the compact at a temperature T (1,300 C.T1,650 C.) by heating from room temperature to T1 (1200 C.T1T) at a rate of at least 100 C./h, and optionally heating from T1 at a rate of 1-95 C./h, and HIP treating the sintered compact at 1,300-1,650 C. The ceramic material has improved diffuse transmittance in the visible region and functions as a magneto-optical part in a broad visible to NIR region.
Transparent ceramics, manufacturing method thereof, and magneto-optical device
A transparent ceramic material is manufactured by molding a source powder into a compact, the source powder comprising a rare earth oxide consisting of at least 40 mol % of terbium oxide and the balance of another rare earth oxide, and a sintering aid, sintering the compact at a temperature T (1,300 C.T1,650 C.) by heating from room temperature to T1 (1200 C.T1T) at a rate of at least 100 C./h, and optionally heating from T1 at a rate of 1-95 C./h, and HIP treating the sintered compact at 1,300-1,650 C. The ceramic material has improved diffuse transmittance in the visible region and functions as a magneto-optical part in a broad visible to NIR region.
ORIENTED APATITE TYPE OXIDE ION CONDUCTOR AND METHOD FOR PRODUCING SAME
An oriented apatite-type oxide ion conductor includes a composite oxide expressed as A.sub.9.33+x[T.sub.6.00yM.sub.y]O.sub.26.0+z, where A represents one or two or more elements selected from the group consisting of La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Be, Mg, Ca, Sr, and Ba, T represents an element including Si or Ge or both, and M represents one or two or more elements selected from the group consisting of B, Ge, Zn, Sn, W, and Mo, and where x is from 1.00 to 1.00, y is from 0.40 to less than 1.00, and z is from 3.00 to 2.00.
Stimuli responsive materials, methods of making, and methods of use thereof
A mechanochromic system comprising a first inorganic/polymer composite layer; and a first elastomer layer bonded to the composite layer to form a composite/elastomer assembly, methods of making, and methods of use thereof are provided.