Pyrometallurgic process for obtaining lithium compounds and intermediates, the process being characterized by comprising the steps of a) contacting lithium aluminosilicate particles with at least a fluorine solid compound, b) heating until a temperature of 25 to 900° C. obtaining a solid mixture and c) carrying out at least a leaching process of the mixture in step b).

Zinc oxide particles are prepared as a dry powder through a vapor phase formed by a plasma process, or by introducing defects into stoichiometric zinc oxide particles in a liquid carrier through mechanical stress. The zinc oxide has an O:Zn ratio of at least 0.99, an average particle size of 10 to 300 nm, and a sufficient concentration of oxygen vacancies and zinc vacancies to give a dispersion of the particles in C12-C15 alkyl benzoate an orange to tan color corresponding to a ΔE value of at least 15 in a Dispersion Color Test. The particles contain no aggregates and have no detectable particles 500 nm or larger, on a number-weighted basis.

An exemplary embodiment of the present invention provides a filler comprising a silica core, a first layer in communication with the core, and a second layer in communication with the first layer. The presence of the second layer can decrease the coefficient of thermal expansion, decrease the composite modulus, and increase the glass transition temperature of the modulus as compared to fillers without a second layer.

A solid electrolyte including a compound represented by Formula 1 or 3, the compound having a glass transition temperature of −30° C. or less, and a glass or glass-ceramic structure,
AQX—Ga.sub.1−zM.sub.z1(F.sub.1−kCl.sub.k).sub.3−3zZ.sub.3z1  Formula 1
wherein, in Formula 1, Q is Li or a combination of Li and Na, K, or a combination thereof, M is a trivalent cation, or a combination thereof, X is a halogen other than F, pseudohalogen, OH, or a combination thereof, Z is a monovalent anion, or a combination thereof, 1<A<5, 0≤z≤1, 0≤z1≤1, and 0≤k<1,
AQX-aM.sub.z1Z.sub.3z1-bGa.sub.1−z(F.sub.1−kCl.sub.k).sub.3−3z  Formula 3 wherein, in Formula 3, Q is Li or a combination of Li and Na, K, or a combination thereof; M is a trivalent cation, or a combination thereof, X is a halogen other than F, pseudohalogen, OH, or a combination thereof, Z is a monovalent anion, or a combination thereof, 0<a≤1, 0<b≤1, 0<a+b, a+b=4−A, 1<A<5, 0≤z<1, 0≤z1≤1, and 0≤k<1.

A method for obtaining aluminum-containing nanoparticles is provided. The method includes exposing at least one surface comprising aluminum to an alkaline aqueous solution. The method further includes exposing the at least one surface to electro-hydraulic shock waves and an electron flux. The at least one surface undergoes electro-erosion which creates alumina-hydrated nanoparticles having a negative surface electrical charge. The method further includes transforming the alumina-hydrated nanoparticles into aquachelate nanoparticles by attaching water molecules to the alumina-hydrated nanoparticles.

A method of inhibiting an irregular aggregation of a nanosized powder includes (A) providing a nanosized ceramic powder to perform thereon a thermal analysis and thereby attain an endothermic peak temperature; (B) performing an impurity-removal heat treatment on the nanosized ceramic powder at a temperature higher than the endothermic peak temperature; (C) switching the nanosized ceramic powder from a temperature environment of the impurity-removal heat treatment to an environment of a temperature higher than a phase change temperature of the nanosized ceramic powder, followed by performing a calcination heat treatment on the nanosized ceramic powder in the environment of the temperature higher than the phase change temperature of the nanosized ceramic powder, wherein the nanosized ceramic powder skips the temperature environment between impurity-removal heat treatment and calcination heat treatment to shun generating a vermicular structure, avoid crystalline irregularity and abnormal growth, reduce particle aggregation, and achieve satisfactory distribution.

The present invention relates to a method of reducing a metal oxide comprising the steps of preparing a mixture by mixing a metal oxide and a metal hydride (step 1) and reducing the mixture by heat treatment (step 2) and a method of producing a photocatalyst using the same, and The method of reducing a metal oxide of the present invention can easily reduce such metal oxides as TiO.sub.2, ZrO.sub.2, V.sub.2O.sub.3, and Fe.sub.2O.sub.3.

A device comprising a nonlinear optical (NLO) material according to the formula XLi.sub.2Al.sub.4B.sub.6O.sub.20F. A device comprising a nonlinear optical material (NLO) according to the formula KSrCO.sub.3F, wherein the NLO comprises at least one single crystal. A nonlinear optical material selected from the group consisting of KSrCO.sub.3F Rb.sub.3Ba.sub.3Li.sub.2Al.sub.4B.sub.6O.sub.20F and K.sub.3Sr.sub.3Li.sub.2Al.sub.4B.sub.6O.sub.20F.

The invention relates to a method for producing functionalised bimodal periodic mesoporous organosilicates (PMOs) by means of pseudomorphic transformation, to functionalised bimodal periodic mesoporous organosilicates (PMOs) that comprise at least one organosilicate and at least one functional component, and to the use of the PMO as a filter material, adsorption means, sensor material or carrier material for pharmaceutical products, insecticides or pesticides.

A method for making a vanadium pentoxide-based active material for a cathode of an alkali metal ion battery includes steps of: a) preparing an aqueous solution of a triazine derivative of Formula (I) ##STR00001## wherein each R independently represents hydrogen or an amino group; and b) adding vanadium pentoxide to the aqueous solution of the triazine derivative under stirring, so as to permit condensation among hydrolyzed vanadium pentoxide along with self-assembly of the triazine derivatives to obtain a reaction solution containing the active material.