The present invention is directed to additive manufacturing compositions and methods for producing additive manufacturing composite blends with oxidized discrete carbon nanotubes with dispersion agents bonded to at least one sidewall of the oxidized discrete carbon nanotubes. Such compositions are especially useful when radiation cured, sintered or melt fused.

The present application pertains to dispersions comprising oxidized, discrete carbon nanotubes and high-surface area carbon nanotubes. The oxidized, discrete carbon nanotubes comprise an interior and exterior surface, each surface comprising an interior surface oxidized species content and an exterior surface oxidized species content. The interior surface oxidized species content differs from the exterior surface oxidized species content by at least 20%, and as high as 100%. The high-surface area nanotubes are generally single-wall nanotubes. The BET surface area of the high-surface area nanotubes is from about 550 m.sup.2/g to about 1500 m.sup.2/g according to ASTM D6556-16. The aspect ratio is at least about 500 up to about 6000. The dispersions comprise from about 0.1 to about 30% by weight nanotubes based on the total weight of the dispersion.

The invention relates to a mechanochemical process to produce exfoliated nanoparticles comprising the steps of providing a solid feedstock comprising a carbonaceous and/or mineral-based material; providing a flow of an oxidizing gas; introducing the solid feedstock and the flow of an oxidizing gas into a mechanical agitation unit, subjecting the material of the solid feedstock in the presence of the oxidizing gas to a mechanical agitation operation in the mechanical agitation unit at a pressure of at least 1 atm (15 psi).

The invention further relates to nanoparticles obtainable by the mechanochemical process and to the use of such nanoparticles.

Chlorosilanes of the general formula H.sub.nSiCl.sub.4-n and/or H.sub.mCl.sub.6-mSi.sub.2, where n=1-4 and m=0-4, are produced in a fluidized bed reactor by reaction of a hydrogen chloride-containing reaction gas with a silicon contact mass granulation mixture composed of a coarse grain fraction and a fine grain fraction, wherein the average particle size of the fine grain fraction d.sub.50,fine is smaller than the average particle size of the coarse grain fraction d.sub.50,coarse.

The present invention relates to a process for preparing zeolite crystals having a multimodal particle size distribution, and the sizes of which are between 0.02 μm and 20 μm, said process comprising a first introduction of one or more seeding agents into the tubular reactor or upstream of the tubular reactor, and at least one second introduction of one or more, identical or different, seeding agents into the tubular reactor.

The present application relates to aqueous slurries comprising precipitated calcium carbonates having a bimodal particle size distribution with a first maximum in particle size distribution and a second maximum in particle size distribution, as well as methods for making them and their uses.

Method for producing soluble potassium sulfate by recrystallization of crude potassium sulfate wherein the crude potassium sulfate contains an amount of potassium, calculated as K.sub.2O, of about 15 wt % or higher, and the resulting potassium sulfate crystalline material conforms with the following characteristics: the amount of insoluble material is less than about 0.05 wt %, a 1 wt % solution of the potassium sulfate has a pH below about 6, and/or 1 pH unit lower than the pH of the crude potassium sulfate, the fraction obtained after crystallization has an average particle size within the following parameters: (i) d90<about 0.6 mm, (ii) d10>about 0.02 mm, and (iii) dust amounts to about 0.4 wt % or less, whereby the resulting potassium sulfate contains more than 51% potassium, calculated as K.sub.2O.

A material synthesis method may comprise: adding at least one liquid precursor solution to an atomizer device; generating by the atomizer device an aerosol comprising liquid droplets; transporting the aerosol to a reactive zone for evaporating one or more solvents from the aerosol; and collecting particles synthesized from at least evaporating the aerosol.

An advantage is to provide a non-aqueous electrolyte secondary battery with improved heat resistance. A positive electrode active material contains a lithium-transition metal composite oxide containing 80 mol % or more of Ni and 0.1 mol % to 1.5 mol % of B on the basis of the total number of moles of metal elements excluding Li, and B and at least one element (M1) selected from Groups 4 to 6 are present on at least the surfaces of particles of the composite oxide. When particles having a volume-based particle size larger than 70% particle size (D70) are first particles, and particles having a volume-based particle size smaller than 30% particle size (D30) are second particles, the molar fraction of M1 on the basis of the total number of moles of metallic elements excluding Li on the surfaces of the second particles is greater than that of the first particles.

A lithium complex oxide includes a mixture of first particles of n1 (n1>40) aggregated primary particles and second particles of n2 (n2≤20) aggregated primary particles, the lithium complex oxide represented by Chemical Formula 1 and having FWHM (deg., 2θ) of 104 peak in XRD, defined by a hexagonal lattice having R-3m space group, in a range of Formula 1:

Li.sub.aNi.sub.xCo.sub.yMn.sub.zM.sub.1-x-y-zO.sub.2,  [Chemical Formula 1] where M is selected from: B, Ba, Ce, Cr, F, Mg, Al, Cr, V, Ti, Fe, Zr, Zn, Si, Y, Nb, Ga, Sn, Mo, W, P, Sr, and any combination thereof, 0.9≤a≤1.3, 0.6≤x≤1.0, 0.0≤y≤=0.4, 0.0≤z≤0.4, and 0.0≤1−x−y−z≤0.4,

−0.025≤FWHM.sub.(104)−{0.04+(x.sub.first particle−0.6)×0.25}≤0.025,  [Formula 1] where FWHM.sub.(104) is represented by Formula 2,

FWHM.sub.(104)={(FWHM.sub.Chemical Formula 1 powder(104)−0.1×mass ratio of second particles)/mass ratio of first particles}−FWHM.sub.Si powder(220).  [Formula 2]