Patent classifications
C01P2006/37
METHODS FOR PREPARING AMMONIUM TETRATHIOMOLYBDATE
This disclosure relates to crystalline ammonium tetrathiomolybdate having pharmaceutical grade purity and processes for manufacturing crystalline ammonium tetrathiomolybdate. This disclosure also relates to processes for manufacturing bis-choline tetrathiomolybdate having pharmaceutical grade purity.
Thermal Insulation
The present invention relates to inorganic fibres having a composition comprising: 61.0 to 70.8 wt% SiO.sub.2; 28.0 to 39.0 wt% CaO; 0.10 to 0.85 wt% MgO other components, if any, providing the balance up to 100 wt %,
The sum of SiO.sub.2 and CaO is greater than or equal to 98.8 wt % and the other components comprise less than 0.70 wt % Al.sub.2O.sub.3, if any.
METHOD FOR MECHANOCHEMICAL PREPARATION OF HIGH TEMPERATURE-RESISTANT BISMUTH YELLOW PIGMENT
The present disclosure relates to a method for preparation of a high temperature-resistant bismuth yellow pigment. The method comprises: mixing an oxide which served as a matrix and dopan with a bismuth source, a vanadium source, or a molybdenum source, and then placing the mixture into a mill for grinding to obtain a precursor; further calcining and crushing the precursor to obtain the high temperature-resistant bismuth yellow pigment powder. The bismuth yellow pigment has a bright color, a b* value greater than 90, a stable performance, and a high heat-resistance above 800° C. The method is environmentally friendly without waste, and reaction conditions are simple. Doping of BiVO.sub.4 crystal lattices by incorporation of oxides can be achieved, so that the particle size and distribution of the bismuth yellow pigment can be effectively controlled while the color performance of the bismuth yellow pigment is greatly improved.
AEROGEL COMPOSITIONS AND METHODS
The present disclosure provides an aerogel composition which is intrinsically hydrophobic without surface modification by a hydrophobizing agent, is durable and easy to handle, which has favorable performance in aqueous environments, and which also has favorable combustion and self-heating properties. Also provided is a method of preparing an aerogel composition which is intrinsically hydrophobic without surface modification by a hydrophobizing agent, is durable and easy to handle, which has favorable performance in aqueous environments, and which has favorable combustion and self-heating properties.
PREPARATION METHOD FOR INSOLUBLE SULFUR AND ANTI-REVERSION STABILIZER USED THEREBY
Provided are a preparation method for insoluble sulfur and an anti-reversion stabilizer used thereby. Methane is used as the anti-reversion stabilizer. The methane is added to liquid sulfur at sulfur gasification stage, and is cracked into active free radicals under the action of sulfur vapor active free radicals; in the quenching process of sulfur vapor mixed with methane, the active free radicals generated by methane cracking carry out end capping on insoluble sulfur end groups generated by sulfur vapor polymerization, thus completing insoluble sulfur stabilization. The methane is added at liquid sulfur gasification stage, and after sulfur gasification, the methane is mixed with sulfur vapor in a gaseous form, rather than being added to the product in a solid or liquid manner at a later stage, so that the insoluble sulfur and the stabilizer can be uniformly contacted and mixed to the greatest extent.
DOPED BEO COMPOUNDS FOR OPTICALLY STIMULATED LUMINESCENCE (OSL) AND THERMOLUMINESCENCE (TL) RADIATION DOSIMETRY
The present invention relates generally in part to BeO-based compounds that are capable of storing at least part of the energy of incident ionizing radiation and releasing at least part of the stored energy upon optical stimulation and heating. BeO-based compounds dosimetry was also developed in instrumentation, application and fundamental investigations. The present disclosure further relates the to the investigation of a BeO-based optically stimulated luminescence (OSL) dosimeter together with an OSL reader, and discusses the design and operation of an OSL reader, suitable to measure OSL emission of BeO-based dosimeters, for example beryllium oxide doped with sodium, dysprosium and erbium. The present disclosure further relates to the use of BeO-based compounds comprising BeO and at least one dopant selected from the group consisting of sodium, dysprosium and erbium as a fiber-coupled OSL dosimeter.
Aerogel precursor and aerogel prepared using the same
The present disclosure provides an aerogel precursor including an alkoxydisiloxane-based prepolymer and having a functional group derived from a hydrophobic sol-gel forming agent of the following Chemical Formula 1 on a surface thereof, and therefore, capable of enhancing high temperature thermal stability of an aerogel providing hydrophobic pores having uniform pore size distribution when preparing an aerogel, and an aerogel prepared using the same: ##STR00001## (in Chemical Formula 1, M, R, R.sup.1 to R.sup.4 are the same as defined in the specification.)
Environment-Friendly Heat Shielding Film Using Non-radioactive Stable Isotope and Manufacturing Method Thereof
Disclosed are an environment-friendly heat shielding film using a non-radioactive stable isotope and a manufacturing method therefor and, more specifically, an environment-friendly heat shielding film using a non-radioactive stable isotope and a manufacturing method therefor, wherein a heat shielding layer is formed on one surface of a substrate layer; the heat shielding layer is composed of stable isotopes as elements constituting a precursor and contains a non-radioactive stable isotope tungsten bronze compound having an oxygen-deficient .sup.(Y)A.sub.x.sup.(182,183,184,186)W.sub.1O.sub.(3-n) type hexagonal structure, thereby preventing the generation of radioactive materials, fundamentally blocking haze, and improving the visible light transmittance and the infrared light blocking rate; and the heat resistance and durability problems that may occur when the heat shielding layer is formed of the non-radioactive stable isotope tungsten bronze compound are solved by a passivation film.
SILICA AEROGEL PREPARATION METHOD AND AEROGEL PREPARED USING SAID METHOD
A preparation method for a silica aerogel, comprising the following steps: A) raw material containing a solid silicon source and an alkaline solution is used to produce an aerogel precursor after mixing; and B) the aerogel precursor is dried to obtain a silica aerogel. An improved silica aerogel preparation method, comprising the following steps: A) a cation exchange resin and a silicate solution are used as raw materials and mixed; B) the mixed material is allowed to stand to obtain an aerogel precursor; and C) the aerogel precursor is dried to obtain a silica aerogel.
Low-silica chabazite zeolites with high acidity
A microporous crystalline material having a molar silica to alumina ratio (SAR) ranging from 10 to 15 and a fraction of Al in the zeolite framework of 0.63 or greater is disclosed. A method of selective catalytic reduction of nitrogen oxides in exhaust gas that comprises contacting exhaust gases, typically in the presence of ammonia, urea, an ammonia generating compound, or a hydrocarbon compound, with an article comprising the disclosed microporous crystalline is also disclosed. Further, a method of making the disclosed microporous crystalline material is disclosed.