Patent classifications
C01P2006/82
METHOD FOR PREPARING BASIC COPPER CARBONATE
A method for preparing a basic copper carbonate is provided. The method includes: mixing a copper hydroxide with water to obtain a precursor slurry; adding an accelerator to the precursor slurry and mixing the two to obtain a first mixture; introducing gaseous carbon dioxide into the first mixture for reaction whereby obtaining a crude basic copper carbonate; and purifying the crude basic copper carbonate whereby obtaining the basic copper carbonate. The accelerator is at least one selected from the group consisting of an ammonia water and an ammonium salt.
SOLID-STATE LITHIUM-ION CONDUCTOR MATERIALS, POWDER MADE OF SOLID-STATE ION CONDUCTOR MATERIALS, AND METHOD FOR PRODUCING SAME
A powder with particulates of a lithium ion-conducting material has a conductivity of at least 10.sup.−5 S/cm. The powder has an inorganic carbon content (Total Inorganic Carbon Content (TIC)) of less than 0.4 wt % and/or an organic carbon content (Total Organic Carbon Content (TOC)) of less than 0.1 wt %. The particulates have a d50 particle size in a range from 0.05 μm to 10 μm. The particulates have a particle size distribution log (d90/d10) of less than 4.
METHOD FOR PRODUCING POSITIVE ELECTRODE ACTIVE MATERIAL FOR NON-AQUEOUS ELECTROLYTE SECONDARY BATTERY
By a method including at least a spraying/mixing step of: mixing a precursor compound of a positive electrode active material with a lithium compound to prepare a mixture; and simultaneously spraying a spraying agent containing at least one element onto the mixture, there can be produced a positive electrode active material for non-aqueous electrolyte secondary batteries, which does not adversely affect battery properties of non-aqueous electrolyte secondary batteries, without reducing production efficiency.
LITHIUM SULFIDE PRODUCTION METHOD
A process for producing a low-cost water-reactive sulfide material includes reacting a substantially anhydrous first alkali metal salt, a substantially anhydrous first sulfide compound, and a substantially anhydrous first alkali metal hydrosulfide compound in a substantially anhydrous polar solvent, providing differential solubility for a substantially high solubility second sulfide and a substantially low solubility second alkali metal salt, and forming a mixture of the high solubility second sulfide, a second alkali metal hydrosulfide, and the low solubility second alkali metal salt; removing the low solubility second alkali metal salt to isolate the supernatant including the second sulfide, and separating the polar solvent from the second sulfide and the second alkali metal hydrosulfide followed by heating to produce the second sulfide. The present disclosure provides a scalable process for production of a high purity alkali metal sulfide that is essentially free of undesired contaminants.
LITHIUM-STUFFED GARNET THIN FILMS AND PELLETS HAVING AN OXYFLUORINATED AND/OR FLUORINATED SURFACE AND METHODS OF MAKING AND USING THE THIN FILMS AND PELLETS
Set forth herein are processes for making lithium-stuffed garnet oxides (e.g., Li.sub.7La.sub.3Zr.sub.2O.sub.12, also known as LLZO) that have passivated surfaces comprising a fluorinate and/or an oxyfluorinate species. These surfaces resist the formation of oxides, carbonates, hydroxides, peroxides, and organics that spontaneously form on LLZO surfaces under ambient conditions. Also set forth herein are new materials made by these processes.
Hydrated lime product
A hydrated lime product exhibiting superior reactivity towards HCl and SO.sub.2 in air pollution control applications. Also disclosed is a method of providing highly reactive hydrated lime and the resultant lime hydrate where an initial lime feed comprising calcium and impurities is first ground to a particle-size distribution with relatively course particles. Smaller particles are then removed from this ground lime and the smaller particles are hydrated and flash dried to form a hydrated lime, which is then milled to a significantly smaller particle size than that of the relatively course particles. The resultant lime hydrate product has available CaOH of greater than 92%, a citric acid reactivity of less than 20 seconds, a BET surface area greater than 18, a D90 less than 10 μm, a D50 less than 4 μm, a D90/D50 less than 3, and a large pore volume of greater than 0.2 BJH.
Countercurrent process for recovering high purity copper sulfate values from low grade ores
A method for extracting copper values from a low grade copper ore feedstock is provided. The method includes (a) providing an ore feedstock of a copper oxide ore; (b) subjecting the ore to at least one process selected from the group consisting of primary crushing processes and secondary crushing processes; (c) subjecting the ore feedstock to high pressure grinding roll crushing, thereby obtaining a crushed ore; (d) subjecting the crushed ore to acid curing, thereby obtaining a cured ore; (e) subjecting the cured ore to vat or heap leaching, thus yielding a leachate; (f) passing the leachate through a first ion exchange resin which is selective to base metals plus copper, thereby removing a portion of the copper values from the leachate and yielding a first loaded resin and a first treated leachate; (g) stripping base metals plus copper values from the first loaded resin with a first stripping solution, thereby yielding a base metals plus copper-loaded stripping solution; (h) selectively extracting copper values from the copper-loaded stripping solution via solvent extraction, thereby obtaining an extract and a raffinate; and (i) crystallizing a copper salt from the extract, thereby obtaining a crystallized copper salt.
Drying process
The present invention refers to a process for making a calcium carbonate containing material, wherein the process includes a specific drying procedure and allows for the provision of calcium carbonate materials with reduced moisture pick-up and low porosity.
PROCESS TO PREPARE AN ACTIVATED CARBON PRODUCT AND A SYNGAS MIXTURE
The invention is directed to a process to prepare an activated carbon product and a gaseous fraction comprising hydrogen, carbon monoxide and a mixture of gaseous organic compounds from a solid torrefied biomass feed comprising the following steps. (i) subjecting the solid biomass feed to a pyrolysis reaction thereby obtaining a gaseous fraction comprising hydrogen, carbon monoxide and a mixture of gaseous organic compounds and a solid fraction comprising of char particles. (ii) separating the solids fraction from the gaseous fraction. and (iii) activating the char particles as obtained in step (ii) to obtain the activated carbon product.
POSITIVE ELECTRODE ACTIVE MATERIAL FOR NONAQUEOUS ELECTROLYTE SECONDARY BATTERIES, METHOD FOR PRODUCING SAME, AND NONAQUEOUS ELECTROLYTE SECONDARY BATTERY
Provided is a positive electrode active material for a nonaqueous electrolyte secondary battery including a LiNi composite oxide having low internal resistance and excellent thermal stability. The positive electrode active material is obtained by performing a water washing process using a water spray on a LiNi composite oxide powder obtained by a firing step until the filtrate has an electric conductivity of 30 to 60 mS/cm, and then dried, where the LiNi composite oxide is represented by the composition formula (1): Li.sub.bNi.sub.1-aM1.sub.aO.sub.2, where M1 represents at least one kind of element selected from transition metal elements other than Ni, group 2 elements, and group 13 elements, and 0.01≤a≤0.5, and 0.85≤b≤1.05.