Provided is a method of producing a sulfide solid electrolyte which brings low costs, and large sulfur reducing effect, the method comprising heat-treating material for a sulfide solid electrolyte at a temperature no less than a melting point of elemental sulfur while vibrating the material.

A method for producing sulfide-based glass ceramics including crystallizing a glass solid electrolyte, wherein the glass solid electrolyte includes: sulfide-based glass comprising at least a sulfur element and a lithium element; and a nitrile compound incorporated into the sulfide-based glass.

Provided is a glass production method with which oxidation can be suppressed and productivity can be increased. A glass production method according to the present invention includes the steps of: turning a raw material 6 placed in a container 1 into a melt 11; homogenizing the melt 11; removing a gas from the melt 11, wherein at least one of the step of turning the raw material 6 into the melt 11 and the step of homogenizing the melt 11 is performed in an atmosphere of an inert gas or a reducing gas, and in the step of the removing the gas from the melt 11, the inert gas or the reducing gas is removed by setting the temperature of the melt 11 to be lower than the temperature in the step of homogenizing the melt 11.

A method of making an optical fiber with multiple openings comprising the steps of fabricating an extrusion die using additive manufacturing such that the extrusion die has a plurality of channels that combine inside the die into another set of channels, extruding a glass, forming a fiber optic preform having a plurality of longitudinal openings that run the entire length, attaching a barrier layer for pressure application, and stretching the preform into an optical fiber with multiple openings. An extrusion die comprising an additive manufactured material, having a proximal side having openings and having a distal side having openings, wherein the openings of the proximal side are of feed channels, wherein the openings of the distal side are of forming channels, and wherein in side the body of the die, two of the feed channels combine the forming channels.

The present invention is generally directed to a photonic bad gap fiber and/or fiber preform with a central structured region comprising a first non-silica based glass and a jacket comprising a second non-silica based glass surrounding the central structured region, where the Littleton softening temperature of the second glass is at least one but no more than ten degrees Celsius lower than the Littleton softening temperature of the first glass, or where the base ten logarithm of the glass viscosity in poise of the second glass is at least 0.01 but no more than 2 lower than the base ten logarithm of the glass viscosity in poise of the first glass at a fiber draw temperature. Also disclosed is a method of making a photonic bad gap fiber and/or fiber preform.

Disclosed herein are methods for producing glass articles by hot-melt processing techniques. The methods involve the use of arsenic-free chalcogenide glasses. Despite the absence of arsenic, the chalcogenide glasses have low characteristic temperatures and are stable against crystallization. The low characteristic temperatures render the glasses capable of being hot-melt processed using conventional equipment. The glasses disclosed herein are suitable for the fabrication of optical devices, including but not limited to IR-transmitting optical devices.

A sulfide solid electrolyte for use in an all-solid-state battery has a composition represented by (100x) [yLi.sub.2S.Math.(1y)P.sub.2S.sub.5].Math.xLiBH.sub.4. In the formula, x is a value satisfying 50<x<75, and y is a value satisfying 0.72y0.78. The sulfide solid electrolyte has an ionic conductivity of 5.0 mS/cm or more at 25 C.

A striae-free chalcogenide glass with uniform refractive index.

A method to synthesize striae-free chalcogenide glass using melt processing. A striae-free chalcogenide glass with uniform refractive index.

Disclosed is a method of manufacturing a crystallized glass for a secondary battery. The secondary battery include a solid electrolyte comprising sulfide, which can be prepared by synthesizing sulfides using thermal energy and vapor pressure as energy sources. The method of the present invention is suitable for manufacturing a crystallized glass for use as the electrolyte comprising sulfide of the secondary battery. The method includes dispersing two or more kinds of sulfides in a solvent and synthesizing the sulfides under conditions of a temperature equal to or greater than a boiling point of the solvent and high pressure greater than standard atmospheric pressure.