The invention pertains to a process for modifying gypsum, wherein a continuous feed of raw gypsum is provided; the water content of the raw gypsum is determined in the continuous feed by near infrared spectroscopy (NIR) measurement; the raw gypsum is calcined in a calcination unit at a fire rate to remove water from the raw gypsum and to obtain a continuous feed of calcined gypsum having a water content within a selected range; a water content of the calcined gypsum is determined by near infrared spectroscopy, and the fire rate is adjusted based on the water content of the raw gypsum and of the calcined gypsum. Further, the invention pertains to an apparatus for performing said process.

The invention pertains to a process for modifying gypsum, wherein a continuous feed of raw gypsum is provided; the water content of the raw gypsum is determined in the continuous feed by near infrared spectroscopy (NIR) measurement; the raw gypsum is calcined in a calcination unit at a fire rate to remove water from the raw gypsum and to obtain a continuous feed of calcined gypsum having a water content within a selected range; a water content of the calcined gypsum is determined by near infrared spectroscopy, and the fire rate is adjusted based on the water content of the raw gypsum and of the calcined gypsum. Further, the invention pertains to an apparatus for performing said process.

The present disclosure relates generally to processes for phase analysis of calcium sulfate materials useful in making gypsum products. In various aspects, the disclosure provides processes for providing a computer-implemented system for determining a phase content of a test calcium sulfate material; processes for determining the phase content of a test calcium sulfate material; processes for providing stucco feedstocks; and production processes for gypsum products.

A method for heat treatment of a grain-shaped feed material using a calcination device to remove carbonate or water of crystallization from the feed material are provided. To continuously check the quality of the heat treatment process, the bulk density of the heat-treated material is measured continuously, wherein upon detection of a deviation of the determined bulk density from the at least one desired bulk density at least one heat treatment parameter of the heat treatment is adapted automatically or manually.

A system for conditioning stucco particulate material includes a vessel having separation chamber in communication with a holding chamber having a holding volume therein. The conditioning system includes the holding volume sufficient to condition the stucco particulate material therein and/or a control system configured to delay discharge of the stucco particulate material from the holding chamber. The system for conditioning stucco particulate material is configured to increase residence time of the stucco particulate material in the holding chamber to promote calcining conditioning therein.

The invention pertains to a process for modifying gypsum, wherein a continuous feed of raw gypsum is provided; the water content of the raw gypsum is determined in the continuous feed by near infrared spectroscopy (NIR) measurement; the raw gypsum is calcined in a calcination unit at a fire rate to remove water from the raw gypsum and to obtain a continuous feed of calcined gypsum having a water content within a selected range; a water content of the calcined gypsum is determined by near infrared spectroscopy, and the fire rate is adjusted based on the water content of the raw gypsum and of the calcined gypsum.

Further, the invention pertains to an apparatus for performing said process.

The invention pertains to a process for modifying gypsum, wherein a continuous feed of raw gypsum is provided; the water content of the raw gypsum is determined in the continuous feed by near infrared spectroscopy (NIR) measurement; the raw gypsum is calcined in a calcination unit at a fire rate to remove water from the raw gypsum and to obtain a continuous feed of calcined gypsum having a water content within a selected range; a water content of the calcined gypsum is determined by near infrared spectroscopy, and the fire rate is adjusted based on the water content of the raw gypsum and of the calcined gypsum.

Further, the invention pertains to an apparatus for performing said process.

The invention pertains to a process for modifying gypsum, wherein a continuous feed of raw gypsum is provided; the water content of the raw gypsum is determined in the continuous feed by near infrared spectroscopy (NIR) measurement; the raw gypsum is calcined in a calcination unit at a fire rate to remove water from the raw gypsum and to obtain a continuous feed of calcined gypsum having a water content within a selected range; a water content of the calcined gypsum is determined by near infrared spectroscopy, and the fire rate is adjusted based on the water content of the raw gypsum and of the calcined gypsum.

Further, the invention pertains to an apparatus for performing said process.

A calcining kettle includes an outer kettle shell, an inner kettle shell, an interior heat exchanger assembly defining at least one tortuous path inside a volume defined by the inner kettle shell, and an agitator within the inner kettle shell. The inner kettle shell is disposed within the outer kettle shell such that the inner kettle shell and the outer kettle shell together at least partially define a jacket adjacent the inner kettle shell. The inner kettle shell and the interior heat exchanger assembly at least partially define a processing volume. The agitator is configured to rotate at least one paddle to cause movement of a feedstock material within the processing volume. A heating device may be structured and adapted to circulate a heat transfer fluid in the at least one tortuous path and the jacket. Calcining methods are also disclosed.

The invention relates to a method for the expansion of sand grain-shaped raw material (1) in which the raw material (1) drops downwards through a substantially vertical heated shaft (4) provided with means (2) for forming a temperature profile (3), in which a shaft flow (5) prevails wherein the raw material (1) expands as a result of heat transfer in the shaft (4) to form expanded granulate (6) and the granulate formed (6) is passed into a pneumatic conveying line (7) with a conveying flow (8) for further transport. In order to continuously check the quality of the expansion process, the bulk density of the expanded granulate (6) is measured continuously, wherein upon detecting a deviation from at least one defined bulk density, the temperature profile (3) in the shaft (4) is adapted automatically or manually and/or the feeding of raw material (1) into the shaft (4) is reduced automatically or manually.