C04B35/10

GRAIN-GRADE ZIRCONIA TOUGHENED ALUMINA CERAMIC SUBSTRATE AND METHOD FOR PREPARING THE SAME
20220402821 · 2022-12-22 ·

A grain-grade zirconia toughened alumina ceramic substrate and a method for preparing the same. The ceramic substrate is prepared from alumina power (main phase) and zirconia powder (secondary phase) in a binary azeotrope of anhydrous ethanol and butanone in the presence of magnesia-alumina spinel powder (as sintering aid), phosphate ester (as dispersant), polyvinyl butyral (as binder) and dibutyl phthalate (as plasticizer). In a mixture of the alumina power and the zirconia powder, a volume percentage of the alumina power is 82.44-96.7%, and a volume percentage of the zirconia powder is 3.30-17.56%. The magnesia-alumina spinel powder is 0.1-4.0% by weight of the mixture of the alumina power and the zirconia powder. A particle size ratio of the alumina powder to the zirconia powder is 2.415-4.444.

GRAIN-GRADE ZIRCONIA TOUGHENED ALUMINA CERAMIC SUBSTRATE AND METHOD FOR PREPARING THE SAME
20220402821 · 2022-12-22 ·

A grain-grade zirconia toughened alumina ceramic substrate and a method for preparing the same. The ceramic substrate is prepared from alumina power (main phase) and zirconia powder (secondary phase) in a binary azeotrope of anhydrous ethanol and butanone in the presence of magnesia-alumina spinel powder (as sintering aid), phosphate ester (as dispersant), polyvinyl butyral (as binder) and dibutyl phthalate (as plasticizer). In a mixture of the alumina power and the zirconia powder, a volume percentage of the alumina power is 82.44-96.7%, and a volume percentage of the zirconia powder is 3.30-17.56%. The magnesia-alumina spinel powder is 0.1-4.0% by weight of the mixture of the alumina power and the zirconia powder. A particle size ratio of the alumina powder to the zirconia powder is 2.415-4.444.

Coating method, coating layer, and turbine shroud

A coating method includes depositing a slurry including a coarsely particulate ceramic and a finely particulate ceramic on a base material configured with an oxide-based ceramics matrix composite such that a proportion of coarse particles decreases towards a surface of the base material; forming a bond coating by performing a heat treatment on the base material on which the slurry has been deposited; and forming a top coating by thermally spraying a ceramic onto the bond coating. The oxide-based ceramics matrix composite is an alumina silica type oxide-based ceramics matrix composite. The coarsely particulate ceramic and the finely particulate ceramic are alumina-based powder.

Coating method, coating layer, and turbine shroud

A coating method includes depositing a slurry including a coarsely particulate ceramic and a finely particulate ceramic on a base material configured with an oxide-based ceramics matrix composite such that a proportion of coarse particles decreases towards a surface of the base material; forming a bond coating by performing a heat treatment on the base material on which the slurry has been deposited; and forming a top coating by thermally spraying a ceramic onto the bond coating. The oxide-based ceramics matrix composite is an alumina silica type oxide-based ceramics matrix composite. The coarsely particulate ceramic and the finely particulate ceramic are alumina-based powder.

EFFECTIVE LEACHING OF ALUMINA-BASED CASTING CORES
20220388056 · 2022-12-08 ·

A ceramic core (40) for an investment casting process (80) including a subsurface internal channel (50) for the introduction of leachate (98) to improve the effectiveness of a leaching process used to remove the core (94) from a cast alloy component (100). The subsurface internal channel may be completely hollow, or it may include one or more ribs (54). The core may be formed (82) using a 3D printing process wherein a carrier material (68) is deposited in a central region of the channel for the purpose of supporting an overlying layer (62) of core material, with the carrier material later being removed to reveal the hollow internal channel (52).

EFFECTIVE LEACHING OF ALUMINA-BASED CASTING CORES
20220388056 · 2022-12-08 ·

A ceramic core (40) for an investment casting process (80) including a subsurface internal channel (50) for the introduction of leachate (98) to improve the effectiveness of a leaching process used to remove the core (94) from a cast alloy component (100). The subsurface internal channel may be completely hollow, or it may include one or more ribs (54). The core may be formed (82) using a 3D printing process wherein a carrier material (68) is deposited in a central region of the channel for the purpose of supporting an overlying layer (62) of core material, with the carrier material later being removed to reveal the hollow internal channel (52).

Plasma processing device member and plasma processing device provided with same

A plasma processing device member according to the disclosure includes a base material and a film formed of a rare-earth element oxide, or a rare-earth element fluoride, or a rare-earth element oxyfluoride, or a rare-earth element nitride, the film being disposed on at least part of the base material. The film includes a surface to be exposed to plasma, the surface having an arithmetic mean roughness Ra of 0.01 μm or more and 0.1 μm or less, the surface being provided with a plurality of pores, and a value obtained by subtracting an average equivalent circle diameter of the pores from an average distance between centroids of adjacent pores is 28 μm or more and 48 μm or less. A plasma processing device according to the disclosure includes the plasma processing device member described above.

Plasma processing device member and plasma processing device provided with same

A plasma processing device member according to the disclosure includes a base material and a film formed of a rare-earth element oxide, or a rare-earth element fluoride, or a rare-earth element oxyfluoride, or a rare-earth element nitride, the film being disposed on at least part of the base material. The film includes a surface to be exposed to plasma, the surface having an arithmetic mean roughness Ra of 0.01 μm or more and 0.1 μm or less, the surface being provided with a plurality of pores, and a value obtained by subtracting an average equivalent circle diameter of the pores from an average distance between centroids of adjacent pores is 28 μm or more and 48 μm or less. A plasma processing device according to the disclosure includes the plasma processing device member described above.

AL2O3-BASED CERAMIC WELDING SEALING COMPONENT AND PREPARATION METHOD THEREOF

The present invention discloses an Al.sub.2O.sub.3-based ceramic welding sealing component and a preparation method thereof, and relates to the technical field of metalized ceramic processing. The Al.sub.2O.sub.3-based ceramic welding sealing component disclosed in the present invention comprises a ceramic matrix and a metallized layer. The ceramic matrix is made from raw materials such as an inorganic fiber-aluminum oxide 3D network matrix, yttrium oxide, silicon oxide, titanium oxide, an additive, a binder and a dispersant, through steps such as preparation of the inorganic fiber-aluminum oxide 3D network matrix, mixing, pelletizing, primary sintering and secondary sintering; and the raw materials of the metallized layer comprise titanium powder, tungsten powder, molybdenum oxide, boron oxide, yttrium oxide and an organic binder. Al.sub.2O.sub.3-based ceramic welding sealing component provided by the present invention has high efficiency of space filling and tensile strength, excellent tensile strength, toughness and high-temperature resistance.

AL2O3-BASED CERAMIC WELDING SEALING COMPONENT AND PREPARATION METHOD THEREOF

The present invention discloses an Al.sub.2O.sub.3-based ceramic welding sealing component and a preparation method thereof, and relates to the technical field of metalized ceramic processing. The Al.sub.2O.sub.3-based ceramic welding sealing component disclosed in the present invention comprises a ceramic matrix and a metallized layer. The ceramic matrix is made from raw materials such as an inorganic fiber-aluminum oxide 3D network matrix, yttrium oxide, silicon oxide, titanium oxide, an additive, a binder and a dispersant, through steps such as preparation of the inorganic fiber-aluminum oxide 3D network matrix, mixing, pelletizing, primary sintering and secondary sintering; and the raw materials of the metallized layer comprise titanium powder, tungsten powder, molybdenum oxide, boron oxide, yttrium oxide and an organic binder. Al.sub.2O.sub.3-based ceramic welding sealing component provided by the present invention has high efficiency of space filling and tensile strength, excellent tensile strength, toughness and high-temperature resistance.