A method for forming a sintered composition including providing a slurry precursor including a lithium-, sodium-, or magnesium-based compound; tape casting the slurry precursor to form a green tape; and sintering the green tape at a temperature in a range of 500° C. to 1350° C. for a time in a range of less than 60 min to form a sintered composition, such that the slurry precursor further includes a solvent and dispersant. The dispersant may include an amine compound, a carboxylic acid compound, or combinations, mixtures, or salts thereof.

A method for producing a lithium-transition metal composite oxide, including steps of: preparing a mixture including a lithium-containing compound and a transition metal compound; obtaining a molded body of the mixture; and sintering the molded bodies in a container having at least one vent hole, to obtain sintered bodies.

Embodiments relate to an improved hydroflux assisted densification process that introduces a transport phase (formed by the introduction of water during the process to suppress melting temperatures) for sintering, the transport phase being a non-aqueous solution. The process can facilitate sintering at low temperature ranges (at or below 300° C.) to yield densification>90% without the need for additional post-processing steps that otherwise would be needed if conventional processes were used. Control of the pressures and water content used during the process can enhance densification mechanisms related to dissolution-reprecipitation, allowing for a greater range of compositional spectra of materials that can be densified, a reduction of the amount of transport phase needed, a reduction of impurities and an improvement of properties in the densified material. Certain hydrated acetate powders can be used to generate a hydroxide mixture flux that is better for the low-temperature densification process.

Embodiments relate to an improved hydroflux assisted densification process that introduces a transport phase (formed by the introduction of water during the process to suppress melting temperatures) for sintering, the transport phase being a non-aqueous solution. The process can facilitate sintering at low temperature ranges (at or below 300° C.) to yield densification>90% without the need for additional post-processing steps that otherwise would be needed if conventional processes were used. Control of the pressures and water content used during the process can enhance densification mechanisms related to dissolution-reprecipitation, allowing for a greater range of compositional spectra of materials that can be densified, a reduction of the amount of transport phase needed, a reduction of impurities and an improvement of properties in the densified material. Certain hydrated acetate powders can be used to generate a hydroxide mixture flux that is better for the low-temperature densification process.

In an aspect, a Co.sub.2Z-type ferrite comprises oxides of at least Me, Co, Mo, Li, and Fe; wherein Me is at least one of Ba or Sr. In another aspect, the Co.sub.2Z-type ferrite comprises a Z-type hexaferrite an amount of lithium molybdate. In another aspect, the Co.sub.2Z-type ferrite has a formula Li.sub.2MoO.sub.4.Ba.sub.xSr.sub.3-xCo.sub.2+y−zMe′.sub.yMe″.sub.zFe.sub.24-2y-mO.sub.41, wherein Me′ is at least one of Ti, Mo, Ru, Ir, Zr, or Sn; Me″ is at least one of Zn, Mn, or Mg; x is 0 to 3; y is 0 to 1.8; z is 0 to 1.8; and m is −4 to 4. In yet another aspect, a method of making a Co.sub.2Z-type ferrite comprises milling an initial Co.sub.2Z-type ferrite and Li.sub.2MoO.sub.4 to form a mixed ferrite; and calcining the mixed ferrite to form the Co.sub.2Z-type ferrite.

In an aspect, a Co.sub.2Z-type ferrite comprises oxides of at least Me, Co, Mo, Li, and Fe; wherein Me is at least one of Ba or Sr. In another aspect, the Co.sub.2Z-type ferrite comprises a Z-type hexaferrite an amount of lithium molybdate. In another aspect, the Co.sub.2Z-type ferrite has a formula Li.sub.2MoO.sub.4.Ba.sub.xSr.sub.3-xCo.sub.2+y−zMe′.sub.yMe″.sub.zFe.sub.24-2y-mO.sub.41, wherein Me′ is at least one of Ti, Mo, Ru, Ir, Zr, or Sn; Me″ is at least one of Zn, Mn, or Mg; x is 0 to 3; y is 0 to 1.8; z is 0 to 1.8; and m is −4 to 4. In yet another aspect, a method of making a Co.sub.2Z-type ferrite comprises milling an initial Co.sub.2Z-type ferrite and Li.sub.2MoO.sub.4 to form a mixed ferrite; and calcining the mixed ferrite to form the Co.sub.2Z-type ferrite.

The present disclosure relates to the technical field of ceramic powder preparation, and discloses a zirconia/titania/cerium oxide doped rare earth tantalum/niobate RETa/NbO.sub.4 ceramic powder and a preparation method thereof. A general chemical formula of the ceramic powder is RE.sub.1-x(Ta/Nb).sub.1-x(Zr/Ce/Ti).sub.2xO.sub.4, 0<x<1, the crystal structure of the ceramic powder is orthorhombic, the lattice space group of the ceramic powder is C222.sub.1, the particle size of the ceramic powder ranges from 10 to 70 μm, and particles of the ceramic powder are spherical. During preparation, the raw materials are ball-milled before a high temperature solid phase reaction, then mixed with a solvent and an organic binder to obtain a slurry C, then centrifuged and atomized to obtain dry pellets, and finally sintered to obtain a zirconia/titanium oxide/cerium oxide doped rare earth tantalum/niobate RETa/NbO.sub.4 ceramic powder, which satisfies the requirements of APS technology for ceramic powders.

The present disclosure relates to the technical field of ceramic powder preparation, and discloses a zirconia/titania/cerium oxide doped rare earth tantalum/niobate RETa/NbO.sub.4 ceramic powder and a preparation method thereof. A general chemical formula of the ceramic powder is RE.sub.1-x(Ta/Nb).sub.1-x(Zr/Ce/Ti).sub.2xO.sub.4, 0<x<1, the crystal structure of the ceramic powder is orthorhombic, the lattice space group of the ceramic powder is C222.sub.1, the particle size of the ceramic powder ranges from 10 to 70 μm, and particles of the ceramic powder are spherical. During preparation, the raw materials are ball-milled before a high temperature solid phase reaction, then mixed with a solvent and an organic binder to obtain a slurry C, then centrifuged and atomized to obtain dry pellets, and finally sintered to obtain a zirconia/titanium oxide/cerium oxide doped rare earth tantalum/niobate RETa/NbO.sub.4 ceramic powder, which satisfies the requirements of APS technology for ceramic powders.

The present application discloses a method for fabricating a ceramic heating body with a porous heating film, which relates to technical field of fabricating method of heating body; the method including mixing, ball-milling, defoaming, molding and drying, sintering, paraffin filling, machining, coating, metalizing sintering, and electrode leading; the beneficial effects of the present application is simple in whole fabricating method, and by using a box furnace to sinter the green body under an oxidizing atmosphere and normal pressure, the fabricated ceramic heating body is heated uniformly and the heating efficiency is high.

The present application discloses a method for fabricating a ceramic heating body with a porous heating film, which relates to technical field of fabricating method of heating body; the method including mixing, ball-milling, defoaming, molding and drying, sintering, paraffin filling, machining, coating, metalizing sintering, and electrode leading; the beneficial effects of the present application is simple in whole fabricating method, and by using a box furnace to sinter the green body under an oxidizing atmosphere and normal pressure, the fabricated ceramic heating body is heated uniformly and the heating efficiency is high.