A process for preparing roofing granules includes forming kaolin clay into green granules and sintering the green granules at a temperature of at least 900 degrees Celsius to cure the green granules until the crystalline content of the sintered granules is at least ten percent as determined by x-ray diffraction.

The present invention provides a high alumina fused cast refractory that is easily produced and has low porosity and high corrosion resistance, and a method of producing the same. The high alumina fused cast refractory of the present invention has the following chemical composition: 95.0 mass % to 99.5 mass % Al.sub.2O.sub.3, 0.20 mass % to 1.50 mass % SiO.sub.2, 0.05 mass % to 1.50 mass % B.sub.2O.sub.3, 0.05 mass % to 1.20 mass % MgO and balance. The method of producing the high alumina fused cast refractory of the present invention includes obtaining a mixture by mixing an Al.sub.2O.sub.3 source material, a SiO.sub.2 source material, a B.sub.2O.sub.3 source material and an MgO source material, and fusing the mixture.

The present invention provides a high alumina fused cast refractory that is easily produced and has low porosity and high corrosion resistance, and a method of producing the same. The high alumina fused cast refractory of the present invention has the following chemical composition: 95.0 mass % to 99.5 mass % Al.sub.2O.sub.3, 0.20 mass % to 1.50 mass % SiO.sub.2, 0.05 mass % to 1.50 mass % B.sub.2O.sub.3, 0.05 mass % to 1.20 mass % MgO and balance. The method of producing the high alumina fused cast refractory of the present invention includes obtaining a mixture by mixing an Al.sub.2O.sub.3 source material, a SiO.sub.2 source material, a B.sub.2O.sub.3 source material and an MgO source material, and fusing the mixture.

A gas nozzle having a fired surface excellent in particle reduction effect is provided. The gas nozzle 1 is a columnar gas nozzle made of sintered ceramics, provided with at least one through-hole 2 through which gas flows. The entire inner surface 2a of the through-hole 2 and the end face 1A on which outlet 2b of the through-hole 2 is provided are both fired surfaces. The inner surface 2a of the through-hole 2 has a first region A in the vicinity of the outlet 2b and a second region B which is located at a further position than the first region A. The average crystal grain size in the first region A is formed to be smaller than the average crystal grain size in the second region B.

A method for improving the Bs of an MnZn power ferrite material by moving the valley point includes the following steps: 1) mixing Fe.sub.2O.sub.3, MnO and ZnO, and performing primary sanding; 2) adding glue, performing spraying and granulating, and then performing pre-sintering to obtain a pre-sintered material; 3) adding additives to the pre-sintered material, and performing secondary sanding; and 4) adding glue to the secondary sanded material, performing spraying and granulating, pressing into a standard ring, and then performing sintering. The method controls and moves the valley point, reduces loss and improves the Bs of a material by controlling the Fe.sub.2O.sub.3 content and the Co.sub.2O.sub.3 content, and the method is relatively simple and suitable for industrialization.

A method for improving the Bs of an MnZn power ferrite material by moving the valley point includes the following steps: 1) mixing Fe.sub.2O.sub.3, MnO and ZnO, and performing primary sanding; 2) adding glue, performing spraying and granulating, and then performing pre-sintering to obtain a pre-sintered material; 3) adding additives to the pre-sintered material, and performing secondary sanding; and 4) adding glue to the secondary sanded material, performing spraying and granulating, pressing into a standard ring, and then performing sintering. The method controls and moves the valley point, reduces loss and improves the Bs of a material by controlling the Fe.sub.2O.sub.3 content and the Co.sub.2O.sub.3 content, and the method is relatively simple and suitable for industrialization.

A heat dissipation member includes a thermal radiation ceramic material, and the thermal radiation ceramic material contains silicon nitride and boron nitride as main components. The ratio of the mass of boron nitride to the mass of silicon nitride and boron nitride is 10 mass % to 40 mass %.

The invention relates to a method for producing a metal-ceramic substrate and to a furnace suitable for carrying out the method. With the method, a metal-ceramic substrate with increased thermal and current conductivity can be obtained. The method comprises the steps of providing a stack containing a ceramic body, a metal foil, and a solder material in contact with the ceramic body and the metal foil, the solder material comprising a metal having a melting point of at least 700° C., a metal having a melting point of less than 700° C., and an active metal, and heating the stack, the stack passing through a heating zone for heating.

The present invention relates to a method for producing a metal-ceramic substrate. The method has the following steps: providing a stack containing a ceramic body, a metal foil, and a solder material in contact with the ceramic body and the metal foil, wherein the solder material has: a metal having a melting point of at least 700° C., a metal having a melting point of less than 700° C., and an active metal; and heating the stack, wherein at least one of the following conditions is satisfied: the high temperature heating duration is no more than 60 min; the peak temperature heating duration is no more than 30 min; the heating duration is no more than 60 min.

A ceramic subassembly manufactured by a 3D-printing process is described. The ceramic subassembly comprises a ceramic substrate having a sidewall extending to spaced apart first and second end surfaces. At least one via extends through the substrate from the ceramic substrate first end surface to the ceramic substrate second end surface. In cross-section, the via has a square-shape with rounded corners.