C04B2235/604

sp.SUP.2.-sp.SUP.3 .Hybrid crystalline boron nitride and its preparation process

The present disclosure relates to a novel sp.sup.2-sp.sup.3 hybrid crystalline boron nitride and its preparation process. A novel sp.sup.2-sp.sup.3 hybrid crystalline boron nitride allotrope, named Gradia BN, is synthesized using sp.sup.2 or sp.sup.3 hybridized boron nitride as raw materials under high-temperature and high-pressure. The basic structural units of Gradia BN are composed of sp.sup.2 hybridized graphite-like structural units and sp.sup.3 hybridized diamond-like structural units. Gradia BN disclosed in the present disclosure is a class of new sp.sup.2-sp.sup.3 hybrid boron nitride allotrope, whose crystal structure can vary with the widths and/or crystallographic orientation relationships of internal sp.sup.2 and/or sp.sup.3 structural units, and may have variable physical properties.

SHAPED AND FIRED ZIRCONIA REFRACTORY MATERIAL

A refractory lining in a combustion chamber operating in a reducing atmosphere. The lining includes at least one or more Zirconia (Zr)-based refractory lining members comprising one or more Zr-based parts. The Zr-based parts comprise at least 90 wt. %, preferably at least 95 wt. %, of monoclinic ZrO.sub.2 and/or partially stabilized ZrO.sub.2 and/or fully stabilized ZrO.sub.2, wherein the total content of tetragonal and cubic ZrO.sub.2 amounts to at least 20 wt. %, preferably more than 35 wt. %, as well as Zr based refractory lining members and methods for manufacturing the Zr based refractory lining members.

HIGH TEMPERATURE COMPOSITES AND METHODS FOR PREPARING HIGH TEMPERATURE COMPOSITES

A method for making a high temperature composite, which is a carbon carbon composite, carbon fiber reinforced ceramic matrix composite, ceramic fiber reinforced ceramic matrix composite, or a carbon silica composite, including: a) providing a precursor part including a resin comprising a poly(aryl ether ketone) (PAEK) and at least one reinforcing material, wherein the resin has a degree of crystallinity of 10% or more; b) pyrolyzing the precursor part to a pyrolyzed part; c) infusing a liquid second resin into the pyrolyzed part to make an infused part; and d) pyrolyzing the infused part to make the carbon carbon composite carbon fiber reinforced ceramic matrix composite, ceramic fiber reinforced ceramic matrix composite, or the carbon silica composite, optionally repeating steps c. through d. Also, a carbon carbon composite, carbon fiber reinforced ceramic matrix composite, ceramic fiber reinforced ceramic matrix composite, or carbon silica composite made by the method.

Systems, devices, and methods for manufacturing carbon ceramic brake discs
11702370 · 2023-07-18 · ·

Systems, devices, and methods are provided for manufacturing a carbon ceramic brake disc. Generally, a plurality of uncured or partially-cured bulk molding compound preforms or molding compound layers and ventilation cores are placed in a mold cavity and warm-pressed at a first temperature. The ventilation cores are removed from the resulting cured green body. The cured green body is then removed from the mold, and treated through a polymer infiltration and pyrolysis or reactive melt infiltration process. Certain steps can be repeated until a desired target density or weight is attained.

Dielectric ceramic composition and ceramic electronic component
11702368 · 2023-07-18 · ·

A dielectric ceramic composition including a first component and a second component. The first component comprises an oxide of Ca of 0.00 mol % to 35.85 mol % an oxide of Sr of 0.00 mol % to 47.12 mol %, an oxide of Ba of 0.00 mol % to 51.22 mol %, an oxide of Ti of 0.00 mol % to 17.36 mol %, an oxide of Zr of 0.00 mol % to 17.36 mol %, an oxide of Sn of 0.00 mol % to 2.60 mol %, an oxide of Nb of 0.00 mol % to 35.32 mol %, an oxide of Ta of 0.00 mol % to 35.32 mol %, and an oxide of V of 0.00 mol % to 2.65 mol %. The second component includes (by mass) at least (a) an oxide of Mn of 0.005% to 3.500% and (b) one or both of an oxide of Cu of 0.080% to 20.000% and an oxide of Ru of 0.300% to 45.000%.

SINTERED BODY WITH HIGH IMPACT RESISTANCE

To provide a sintered body with improved impact resistance due to impact absorption through plastic deformation before brittle fracture for an impact exceeding the fracture resistance of the sintered body, and/or a method for producing the sintered body.

A sintered body including: zirconia containing a stabilizer; and a region in which an impact mark is formed when an impact force is applied.

CUTTING TOOL

A cutting tool (1) formed of a silicon nitride-based sintered body (2) including a matrix phase (3), a hard phase (4), and a grain boundary phase (10) in which a glass phase (11) and a crystal phase (12) exist. The sintered body (2) contains yttrium in an amount of 5.0 wt % to 15.0 wt % in terms of an oxide, and contains titanium nitride as the hard phase (4) in an amount of 5.0 wt % to 25.0 wt %. In an X-ray diffraction peak, a halo pattern appears at 2θ ranging from 25° to 35° in an internal region of the sintered body (2). A ratio B/A of a maximum peak intensity B to a maximum peak intensity A satisfies 0.11≤B/A≤0.40 . . . Expression (1) in a surface region of the sintered body (2), and satisfies 0.00≤B/A≤0.10 . . . Expression (2) in the internal region of the sintered body (2).

COMPOSITE BODY, LITHIUM ION CONDUCTOR, ALL-SOLID STATE LITHIUM ION SECONDARY BATTERY, ELECTRODE SHEET FOR ALL-SOLID STATE LITHIUM ION SECONDARY BATTERY, AND LITHIUM TETRABORATE

According to the present invention, there are provided a composite body that enables the formation of a lithium ion conductor that exhibits good lithium ion conductivity by a pressurization treatment without sintering at a high temperature (about 1,000° C.) while using a lithium-containing oxide having excellent safety and stability, as well as a lithium ion conductor, an all-solid state lithium ion secondary battery, an electrode sheet for an all-solid state lithium ion secondary battery, and lithium tetraborate. The composite body according to the embodiment of the present invention contains a lithium compound having a lithium ion conductivity of 1.0×10.sup.−6 S/cm or more at 25° C. and lithium tetraborate that satisfies the following requirement 1.

The requirement 1: In a reduced two-body distribution function G(r) obtained from an X-ray total scattering measurement of the lithium tetraborate, a first peak in which a peak top is located in a range where r is 1.43±0.2 Å and a second peak in which a peak top is located in a range where r is 2.40±0.2 Å are present, G(r) of the peak top of the first peak and G(r) of the peak top of the second peak indicate more than 1.0, and an absolute value of G(r) is less than 1.0 in a range where r is more than 5 Å and 10 Å or less.

PRESSED SILICON CARBIDE CERAMIC (SIC) FLUIDIC MODULES WITH INTEGRATED HEAT EXCHANGE
20230219053 · 2023-07-13 ·

A silicon carbide flow reactor fluidic module comprises a monolithic closed-porosity silicon carbide body, a tortuous fluid passage extending through the silicon carbide body, the tortuous fluid passage having an interior surface, and one or more thermal control fluid passages also extending through the silicon carbide body, the interior surface having a surface roughness of less than 10 μm Ra. A process for forming such modules is also disclosed.

Filamentous organism-derived carbon-based materials, and methods of making and using same

The invention provides filamentous organism-derived carbonaceous materials doped with organic and/or inorganic compounds, and methods of making the same. In certain embodiments, these carbonaceous materials are used as electrodes in solid state batteries and/or lithium-ion batteries. In another aspect, these carbonaceous materials are used as a catalyst, catalyst support, adsorbent, filter and/or other carbon-based material or adsorbent. In yet another aspect, the invention provides battery devices incorporating the carbonaceous electrode materials.