Patent classifications
C04B2235/606
GLASS
The present invention relates to a glass including, represented by mole percent based on oxides: from 52% to 80% of SiO.sub.2; from 5% to 30% of B.sub.2O.sub.3; from 2% to 30% of Al.sub.2O.sub.3; from 0.1% to 11% of P.sub.2O.sub.5; and from 0.0001% to 5% of Na.sub.2O, in which the glass has an average thermal expansion coefficient α at from 50° C. to 350° C. of from 5×10.sup.−7/° C. or more and 33×10.sup.−7/° C. or less.
MICROWAVE DIELECTRIC CERAMIC MATERIAL AND PREPARATION METHOD THEREOF
A temperature-stable modified NiO—Ta.sub.2O.sub.5-based microwave dielectric ceramic material and a preparation method thereof are provided. Using ion doping modification to form solid solution structure is an important measure to adjust microwave dielectric properties, especially the temperature stability. Based on formation rules of the solid solution, ion replacement methods are designed including Ni.sup.2+ ions are replaced by Cu.sup.2+ ions, and (Ni.sub.1/3Ta.sub.2/3).sup.4+ composite ions are replaced by [(Al.sub.1/2Nb.sub.1/2).sub.ySn.sub.1-y].sup.4+ composite ions, which considers that cations with similar ionic radii to Ni.sup.2+ and Ta.sup.5+ ions can be introduced into the NiTa.sub.2O.sub.6 ceramic for doping under the same coordination environment (coordination number=6), and therefore a ceramic material with the NiTa.sub.2O.sub.6 solid solution structure can be obtained. The microwave dielectric ceramic material with excellent temperature stability and low loss is finally prepared by adjusting molar contents of each of doped ions, and its microwave dielectric properties are excellent.
FREEZE DRYING OF COMPOSITES FOR FILAMENT SPREADING
A method of spreading fiber tows includes assembling a fibrous composite from a plurality of tows, applying an aqueous solution to the fibrous composite, freezing the fibrous composite after applying the aqueous solution, freeze drying the fibrous composite to remove water from the fibrous composite, and heating the fibrous composite after freeze drying to remove a cryoprotectant from the fibrous composite. The aqueous solution comprises water and the cryoprotectant and freezing the fibrous composite spreads filaments within the plurality of fiber tows.
Titanium-containing calcium hexaaluminate material and preparation method thereof
A titanium-containing calcium hexaaluminate material and preparation method thereof is disclosed. The technical solution is: using 60˜80 wt % alumina micro powder, 5˜20 wt % calcium-containing micro powder, 10˜20 wt % titania micro powder and 1˜10 wt % manganese oxide micro powder as raw materials, blending the raw materials evenly in a planetary ball mill to obtain a blend, machine pressing the blend at 100˜200 MPa to obtain a green body, drying the green body at 110˜200° C. for 12˜36 h, and incubating the dried green body at 1500˜1800° C. for 1˜8 h to obtain the titanium-containing calcium hexaaluminate material. The present disclosure has low cost and simple process, and the prepared titanium-containing calcium hexaaluminate material has the characteristics of good chemical stability, high thermal shock resistance and strong melt resistance to titanium-aluminum alloy.
ULTRA-HIGH TEMPERATURE CARBIDE FOAMS AND METHODS OF FABRICATING THE SAME
Ultra-high temperature carbide (UHTC) foams and methods of fabricating and using the same are provided. The UHTC foams are produced in a three-step process, including UHTC slurry preparation, freeze-drying, and spark plasma sintering (SPS). The fabrication methods allow for the production of any kind of single- or multi-component UHTC foam, while also providing flexibility in the shape and size of the UHTC foams to produce near-net-shape components.
Honeycomb structure
A honeycomb structure includes a honeycomb segment bonded member including; a plurality of prismatic columnar shaped honeycomb segments; and a bonding layer bonding the segments, wherein one honeycomb segment has a bulge on one side face, extending in an axial direction, another honeycomb segment has a recess on one side face, extending in the axial direction, the one honeycomb segment and the another are disposed adjacent and bonded to each other via the bonding layer with the bulge inserted in the recess, length of the bulge is smaller than length of the one side face of the one honeycomb segment, length of the recess is smaller than length of the one side face of the another honeycomb segment, a base part of the bulge is defined with a bent side face, an angle between an imaginary bottom face and the bent side face of the bulge being 60° or more.
Ten-membered fergusonite structure high-entropy oxide ceramic and preparation method thereof
Disclosed are a ten-membered fergusonite structure high-entropy oxide ceramic and a preparation method thereof, where the high-entropy oxide ceramic has a monoclinic structure, with a chemical formula of RENbO.sub.4, and the RE is any ten rare-earth cations selected from a group consisting of La.sup.3+, Ce.sup.3+, Pr.sup.3+, Nd.sup.3+, Sm.sup.3+, Eu.sup.3+, Gd.sup.3+, Dy.sup.3+, Ho.sup.3+, Er.sup.3+, Tm.sup.3+, Yb.sup.3+, Lu.sup.3+ and Y.sup.3+. The ten rare-earth cations have a molar ratio of 1:1:1:1:1:1:1:1:1:1 and equal share of RE position. According to the application, by adopting solid state reaction, the fergusonite structure high-entropy oxide ceramic with single-phase structure, uniform element distribution and stable phase is obtained. The high-entropy oxide ceramic prepared by the application is simple in process, uniform in chemical composition and microstructure, and convenient to realize on-demand regulation on properties through a combination of different elements.
Alumina-based fibrous mass, process for producing same, and use
To provide an alumina-based fibrous mass having a high areal pressure and is usable as a holding material for an exhaust gas cleaners and a production process thereof; the alumina-based fibrous mass has a chemical composition containing an Al.sub.2O.sub.3 in an amount of 70% or more and less than 90% and having a total pore volume of 0.0055 mL/g or less.
Plugged honeycomb structure and manufacturing method of the same
There is disclosed a plugged honeycomb structure. A plugged honeycomb structure includes a tubular honeycomb structure body having partition walls including a porous partition wall base material defining a plurality of cells which become through channels for a fluid and extend from a first end face to a second end face, and a porous trapping layer disposed on the surface of the partition wall base material; and plugging portions disposed in open ends of predetermined cells in the first end face and open ends of residual cells in the second end face, and the partition wall base material is constituted of a porous body including α-Al.sub.2O.sub.3 as a main phase and further including aluminum titanate and glass.
HONEYCOMB STRUCTURE
A honeycomb structure includes a pillar-shaped honeycomb structure body including porous partition walls defining and forming a plurality of cells which extend from an inflow end face to an outflow end face, and a porous outer wall surrounding the partition walls, a porous supporting bulge disposed to extend out from a circumference of the outer wall so that at least a part of the outer wall is exposed, and plugging portions arranged in open ends of the cells, and the supporting bulge has support portions and a side wall portion, and the partition walls and the outer wall of the honeycomb structure body and the support portions and the side wall portion of the supporting bulge are all formed monolithically by formation of a ceramic raw material.