Patent classifications
C07C17/395
METHOD OF REMOVING 2-CHLORO-1,3,3,3-TETRAFLUOROPROPENE AND METHOD OF PRODUCING 1-CHLORO-2,3,3,3-TETRAFLUOROPROPENE
Provided are: a method of removing 2-chloro-1,3,3,3-tetrafluoropropene (1224xe), the method including bringing a mixture containing 1224xe and 1224yd into contact with an alkali optionally in the presence of a phase transfer catalyst; and a method of producing 1-chloro-2,3,3,3-tetrafluoropropene (1224yd), the method including bringing a mixture containing 1224xe and 1224yd into contact with an alkali optionally in the presence of a phase transfer catalyst.
METHOD OF REMOVING 2-CHLORO-1,3,3,3-TETRAFLUOROPROPENE AND METHOD OF PRODUCING 1-CHLORO-2,3,3,3-TETRAFLUOROPROPENE
Provided are: a method of removing 2-chloro-1,3,3,3-tetrafluoropropene (1224xe), the method including bringing a mixture containing 1224xe and 1224yd into contact with an alkali optionally in the presence of a phase transfer catalyst; and a method of producing 1-chloro-2,3,3,3-tetrafluoropropene (1224yd), the method including bringing a mixture containing 1224xe and 1224yd into contact with an alkali optionally in the presence of a phase transfer catalyst.
Composition containing C.SUB.8.F.SUB.17.Br and method for producing C.SUB.8.F.SUB.17.Br
This invention provides a composition that contains PFOB with a PFOA content lower than that of known PFOB, and that is less likely to have an adverse effect on the environment; and provides a method for producing PFOB. The composition contains C.sub.8F.sub.17Brand further contains C.sub.7F.sub.15COOH, wherein C.sub.7F.sub.15COOH is present in a concentration of 25 ppb or less based on the total weight of C.sub.8F.sub.17Br. The method for producing C.sub.8F.sub.17Br comprises reacting C.sub.8F.sub.17I and a brominating agent to obtain C.sub.8F.sub.17Br, and alkali-washing the obtained C.sub.8F.sub.17Br to reduce the C.sub.7F.sub.15COOH content to 25 ppb or less based on the total weight of C.sub.8F.sub.17Br.
Composition containing C.SUB.8.F.SUB.17.Br and method for producing C.SUB.8.F.SUB.17.Br
This invention provides a composition that contains PFOB with a PFOA content lower than that of known PFOB, and that is less likely to have an adverse effect on the environment; and provides a method for producing PFOB. The composition contains C.sub.8F.sub.17Brand further contains C.sub.7F.sub.15COOH, wherein C.sub.7F.sub.15COOH is present in a concentration of 25 ppb or less based on the total weight of C.sub.8F.sub.17Br. The method for producing C.sub.8F.sub.17Br comprises reacting C.sub.8F.sub.17I and a brominating agent to obtain C.sub.8F.sub.17Br, and alkali-washing the obtained C.sub.8F.sub.17Br to reduce the C.sub.7F.sub.15COOH content to 25 ppb or less based on the total weight of C.sub.8F.sub.17Br.
PROCESSES FOR PRODUCING HIGH-PURITY TRIFLUOROIODOMETHANE
The present disclosure provides a method for purifying trifluoroiodomethane. The method includes providing a process stream comprising trifluoroiodomethane, organic impurities, and acid impurities; reacting the process stream with a basic aqueous solution, the basic aqueous solution comprising water and at least one base selected from the group of an alkali metal carbonate and an alkali metal hydroxide; and separating at least some of the organic impurities from the process stream.
PROCESSES FOR PRODUCING HIGH-PURITY TRIFLUOROIODOMETHANE
The present disclosure provides a method for purifying trifluoroiodomethane. The method includes providing a process stream comprising trifluoroiodomethane, organic impurities, and acid impurities; reacting the process stream with a basic aqueous solution, the basic aqueous solution comprising water and at least one base selected from the group of an alkali metal carbonate and an alkali metal hydroxide; and separating at least some of the organic impurities from the process stream.
HIGH-PURITY 1,1,1,2,3,3-HEXAFLUOROPROPANE, METHOD FOR PRODUCING SAME AND USE THEREOF
The present invention relates to a method for producing high-purity 1,1,1,2,3,3-hexafluoropropane and a composition containing mainly 1,1,1,2,3,3-hexafluoropropane, suitable for use as a cleaning agent in the semiconductor industry.
HIGH-PURITY 1,1,1,2,3,3-HEXAFLUOROPROPANE, METHOD FOR PRODUCING SAME AND USE THEREOF
The present invention relates to a method for producing high-purity 1,1,1,2,3,3-hexafluoropropane and a composition containing mainly 1,1,1,2,3,3-hexafluoropropane, suitable for use as a cleaning agent in the semiconductor industry.
COMPOSITION CONTAINING C8F17Br AND METHOD FOR PRODUCING C8F17Br
This invention provides a composition that contains PFOB with a PFOA content lower than that of known PFOB, and that is less likely to have an adverse effect on the environment; and provides a method for producing PFOB. The composition contains C.sub.8F.sub.17Brand further contains C.sub.7F.sub.15COOH, wherein C.sub.7F.sub.15COOH is present in a concentration of 25 ppb or less based on the total weight of C.sub.8F.sub.17Br. The method for producing C.sub.8F.sub.17Br comprises reacting C.sub.8F.sub.17I and a brominating agent to obtain C.sub.8F.sub.17Br, and alkali-washing the obtained C.sub.8F.sub.17Br to reduce the C.sub.7F.sub.15COOH content to 25 ppb or less based on the total weight of C.sub.8F.sub.17Br.
COMPOSITION CONTAINING C8F17Br AND METHOD FOR PRODUCING C8F17Br
This invention provides a composition that contains PFOB with a PFOA content lower than that of known PFOB, and that is less likely to have an adverse effect on the environment; and provides a method for producing PFOB. The composition contains C.sub.8F.sub.17Brand further contains C.sub.7F.sub.15COOH, wherein C.sub.7F.sub.15COOH is present in a concentration of 25 ppb or less based on the total weight of C.sub.8F.sub.17Br. The method for producing C.sub.8F.sub.17Br comprises reacting C.sub.8F.sub.17I and a brominating agent to obtain C.sub.8F.sub.17Br, and alkali-washing the obtained C.sub.8F.sub.17Br to reduce the C.sub.7F.sub.15COOH content to 25 ppb or less based on the total weight of C.sub.8F.sub.17Br.