C07C17/395

Method for producing 1-chloro-2,3,3-trifluoropropene

To provide a method for producing 1-chloro-2,3,3-trifluoropropene, whereby it is possible to efficiently remove 1-chloro-3,3-difluoro-1-propyne and/or an oxide from a composition comprising 1-chloro-2,3,3-trifluoropropene. A method for producing 1-chloro-2,3,3-trifluoropropene, in which a composition comprising 1-chloro-2,3,3-trifluoropropene and at least one member selected from 1-chloro-3,3-difluoro-1-propyne and an oxide, is brought into contact with a basic aqueous solution to remove said at least one member selected from 1-chloro-3,3-difluoro-1-propyne and an oxide, from the composition.

Method for producing 1-chloro-2,3,3-trifluoropropene

To provide a method for producing 1-chloro-2,3,3-trifluoropropene, whereby it is possible to efficiently remove 1-chloro-3,3-difluoro-1-propyne and/or an oxide from a composition comprising 1-chloro-2,3,3-trifluoropropene. A method for producing 1-chloro-2,3,3-trifluoropropene, in which a composition comprising 1-chloro-2,3,3-trifluoropropene and at least one member selected from 1-chloro-3,3-difluoro-1-propyne and an oxide, is brought into contact with a basic aqueous solution to remove said at least one member selected from 1-chloro-3,3-difluoro-1-propyne and an oxide, from the composition.

PROCESS FOR REDUCING 3,3,3-TRIFLUOROPROPYNE IN 2,3,3,3-TETRAFLUOROPROPENE

The invention relates to a process for reducing the concentration of a fluorinated alkyne impurity, such as 3,3,3-trifluoropropyne (TFPY), in 2,3,3,3-tetrafluoropropene (HFO-1234yf) which comprises contacting such a mixture with a caustic material, such as sodium hydroxide (NaOH), under conditions effective to reduce the concentration of the fluorinated alkyne impurity, including in some practices reducing the concentration by at least about 50%.

PROCESS FOR REDUCING 3,3,3-TRIFLUOROPROPYNE IN 2,3,3,3-TETRAFLUOROPROPENE

The invention relates to a process for reducing the concentration of a fluorinated alkyne impurity, such as 3,3,3-trifluoropropyne (TFPY), in 2,3,3,3-tetrafluoropropene (HFO-1234yf) which comprises contacting such a mixture with a caustic material, such as sodium hydroxide (NaOH), under conditions effective to reduce the concentration of the fluorinated alkyne impurity, including in some practices reducing the concentration by at least about 50%.

Process for purifying 1-chloro-3,3,3-trifluoropropene
11912640 · 2024-02-27 · ·

The present invention relates to a process for neutralizing a composition A comprising 1-chloro-3,3,3-trifluoropropene, 1,1-dichloro-1,3,3-trifluoropropane and one or more acid compound(s) of formula HX with XF or Cl; said process comprising the step a) of bringing said composition A into contact with a solution B under conditions capable of limiting the formation of 1-chloro-1,3,3-trifluoropropene.

Process for purifying 1-chloro-3,3,3-trifluoropropene
11912640 · 2024-02-27 · ·

The present invention relates to a process for neutralizing a composition A comprising 1-chloro-3,3,3-trifluoropropene, 1,1-dichloro-1,3,3-trifluoropropane and one or more acid compound(s) of formula HX with XF or Cl; said process comprising the step a) of bringing said composition A into contact with a solution B under conditions capable of limiting the formation of 1-chloro-1,3,3-trifluoropropene.

Process for purifying 1-chloro-3,3,3-trifluoropropene
11912640 · 2024-02-27 · ·

The present invention relates to a process for neutralizing a composition A comprising 1-chloro-3,3,3-trifluoropropene, 1,1-dichloro-1,3,3-trifluoropropane and one or more acid compound(s) of formula HX with XF or Cl; said process comprising the step a) of bringing said composition A into contact with a solution B under conditions capable of limiting the formation of 1-chloro-1,3,3-trifluoropropene.

PROCESS FOR THE REMOVAL OF HALOALKYNE IMPURITIES FROM (HYDRO)HALOCARBON COMPOSITIONS
20190367434 · 2019-12-05 · ·

The invention relates to a process comprising contacting a composition comprising a (hydro)halocarbon and a compound of formula R.sub.fCCX with a basic solution comprising an hydroxide, an alkoxide and/or an amide to reduce the concentration of R.sub.fCCX, wherein R.sub.f is a perfluorinated alkyl group and X is H, F, Cl, Br, or I. The invention further relates to process for preparing a (hydro)halocarbon comprising (i) converting a starting material, optionally in the presence of HF and/or a catalyst, to a composition comprising the (hydro)halocarbon and a compound of formula R.sub.fCCX, wherein R.sub.f is a perfluorinated alkyl group and X is H, F, Cl, Br, or I; (ii) contacting the composition with a basic solution comprising an hydroxide, an alkoxide and/or an amide to reduce the concentration of the compound of formula R.sub.fCCX; and (iii) recovering the (hydro)halocarbon.

PROCESS FOR THE REMOVAL OF HALOALKYNE IMPURITIES FROM (HYDRO)HALOCARBON COMPOSITIONS
20190367434 · 2019-12-05 · ·

The invention relates to a process comprising contacting a composition comprising a (hydro)halocarbon and a compound of formula R.sub.fCCX with a basic solution comprising an hydroxide, an alkoxide and/or an amide to reduce the concentration of R.sub.fCCX, wherein R.sub.f is a perfluorinated alkyl group and X is H, F, Cl, Br, or I. The invention further relates to process for preparing a (hydro)halocarbon comprising (i) converting a starting material, optionally in the presence of HF and/or a catalyst, to a composition comprising the (hydro)halocarbon and a compound of formula R.sub.fCCX, wherein R.sub.f is a perfluorinated alkyl group and X is H, F, Cl, Br, or I; (ii) contacting the composition with a basic solution comprising an hydroxide, an alkoxide and/or an amide to reduce the concentration of the compound of formula R.sub.fCCX; and (iii) recovering the (hydro)halocarbon.

PROCESS FOR THE REMOVAL OF HALOALKYNE IMPURITIES FROM (HYDRO)HALOCARBON COMPOSITIONS
20190367434 · 2019-12-05 · ·

The invention relates to a process comprising contacting a composition comprising a (hydro)halocarbon and a compound of formula R.sub.fCCX with a basic solution comprising an hydroxide, an alkoxide and/or an amide to reduce the concentration of R.sub.fCCX, wherein R.sub.f is a perfluorinated alkyl group and X is H, F, Cl, Br, or I. The invention further relates to process for preparing a (hydro)halocarbon comprising (i) converting a starting material, optionally in the presence of HF and/or a catalyst, to a composition comprising the (hydro)halocarbon and a compound of formula R.sub.fCCX, wherein R.sub.f is a perfluorinated alkyl group and X is H, F, Cl, Br, or I; (ii) contacting the composition with a basic solution comprising an hydroxide, an alkoxide and/or an amide to reduce the concentration of the compound of formula R.sub.fCCX; and (iii) recovering the (hydro)halocarbon.