C07C51/412

Process for the preparation of a polyamide

The invention relates to a process for preparing a semi-aromatic polyamide from diamine and dicarboxylic acid, comprising steps of •(i) dosing a liquid diamine to an agitated powder comprising an aromatic dicarboxylic acid thereby forming a powder comprising a diamine/dicarboxylic acid salt (DD-salt), and •(ii) solid-state polymerizing the DD-salt to obtain the polyamide.

MULTIPLE-COMPONENT SOLID PHASES CONTAINING AT LEAST ONE ACTIVE PHARMACEUTICAL INGREDIENT

The subject invention concerns a method for identifying complementary chemical functionalities to form a desired supramolecular synthon. The subject invention also pertains to multiple-component phase compositions comprising one or more pharmaceutical entities and methods for producing such compositions.

MULTIPLE-COMPONENT SOLID PHASES CONTAINING AT LEAST ONE ACTIVE PHARMACEUTICAL INGREDIENT

The subject invention concerns a method for identifying complementary chemical functionalities to form a desired supramolecular synthon. The subject invention also pertains to multiple-component phase compositions comprising one or more pharmaceutical entities and methods for producing such compositions.

PROCESS FOR MAKING ACRYLIC ACID FROM DEXTROSE

A process is described for making acrylic acid from dextrose, which comprises fermenting dextrose; removing solids from the resulting fermentation broth; removing lactic acid from the clarified broth by extraction into an organic solvent; separating out the lactic acid-loaded organic solvent while recycling at least a portion of the remainder back to the fermentation step; reacting the lactic acid with ammonia to provide a dehydration feed comprising ammonium lactate while preferably recycling the organic solvent; carrying out a vapor phase dehydration of the ammonium lactate to produce a crude acrylic acid product; and purifying the crude acrylic acid by distillation followed by melt crystallization, chromatography or both melt crystallization and chromatography.

PROCESS FOR MAKING ACRYLIC ACID FROM DEXTROSE

A process is described for making acrylic acid from dextrose, which comprises fermenting dextrose; removing solids from the resulting fermentation broth; removing lactic acid from the clarified broth by extraction into an organic solvent; separating out the lactic acid-loaded organic solvent while recycling at least a portion of the remainder back to the fermentation step; reacting the lactic acid with ammonia to provide a dehydration feed comprising ammonium lactate while preferably recycling the organic solvent; carrying out a vapor phase dehydration of the ammonium lactate to produce a crude acrylic acid product; and purifying the crude acrylic acid by distillation followed by melt crystallization, chromatography or both melt crystallization and chromatography.

Sodium diacetate crystal and solid dialysis preparation comprising said crystal

A novel highly stable sodium diacetate crystal, in which the volatilization of acetic acid can be suppressed for a long period. More specifically, a sodium diacetate crystal having a median diameter in the range of 300 to 3000 μm.

Sodium diacetate crystal and solid dialysis preparation comprising said crystal

A novel highly stable sodium diacetate crystal, in which the volatilization of acetic acid can be suppressed for a long period. More specifically, a sodium diacetate crystal having a median diameter in the range of 300 to 3000 μm.

CERIUM CITRATE, METHOD OF MAKING AND CORROSION INHIBITOR COMPRISING CERIUM CITRATE

A method of making cerium citrate includes combining cerium carbonate and citric acid to produce cerium citrate and carbon dioxide. The cerium citrate is substantially free of negative ions other than citrate. The cerium citrate can be used in a corrosion inhibitor composition.

CERIUM CITRATE, METHOD OF MAKING AND CORROSION INHIBITOR COMPRISING CERIUM CITRATE

A method of making cerium citrate includes combining cerium carbonate and citric acid to produce cerium citrate and carbon dioxide. The cerium citrate is substantially free of negative ions other than citrate. The cerium citrate can be used in a corrosion inhibitor composition.

ZINC CARBOXYLIC ACID SALT AND ZINC CARBOXYLATE SOLUTION CONTAINING SAME
20230183162 · 2023-06-15 · ·

A composition of zinc salts of carboxylic acids. The carboxylic acids of the zinc salts include 0.5 to 6.0 mass % of a component (A), 0.05 to 1.2 mass % of a component (B) and 88.0 to 98.0 mass % of a component (C) described below. A ratio [(A)/(B)] of a mass of the component (A) with respect to a mass of the component (B) is 99/1 to 75/25, where (A) is a straight chain and saturated carboxylic acid having a carbon number of 12 to 22; (B) is a strait chain and unsaturated carboxylic acid having one unsaturated bond and a carbon number of 18, said unsaturated bond comprising a trans-form double bond; and (C) is a straight-chain and unsaturated carboxylic acid having one unsaturated bond and a carbon number of 18, said unsaturated bond comprising a cis-form double bond.