Patent classifications
C07C51/47
PROCESS FOR INHIBITING THE UNDESIRED FREE-RADICAL POLYMERIZATION OF ACRYLIC ACID PRESENT IN A LIQUID PHASE P
Process for inhibiting the undesired free-radical polymerization of acrylic acid present in a liquid phase P, wherein the acrylic acid content of P is at least 10% by weight, the liquid phase P comprises in the range from 25 to 1000 ppmw of glyoxal based on the weight of the acrylic acid present in P and the liquid phase P is admixed with protoanemonine in an amount that results in a protoanemonine content in the range from 0.5 to 100 ppmw based on the weight of the acrylic acid present in P, and a liquid phase P, wherein the acrylic acid content of P is at least 10% by weight and the liquid phase P comprises in the range from 25 to 1000 ppmw of glyoxal and in the range from 0.5 to 100 ppmw of protoanemonine, in each case based on the weight of the acrylic acid present in P.
PROCESS FOR INHIBITING THE UNDESIRED FREE-RADICAL POLYMERIZATION OF ACRYLIC ACID PRESENT IN A LIQUID PHASE P
Process for inhibiting the undesired free-radical polymerization of acrylic acid present in a liquid phase P, wherein the acrylic acid content of P is at least 10% by weight, the liquid phase P comprises in the range from 25 to 1000 ppmw of glyoxal based on the weight of the acrylic acid present in P and the liquid phase P is admixed with protoanemonine in an amount that results in a protoanemonine content in the range from 0.5 to 100 ppmw based on the weight of the acrylic acid present in P, and a liquid phase P, wherein the acrylic acid content of P is at least 10% by weight and the liquid phase P comprises in the range from 25 to 1000 ppmw of glyoxal and in the range from 0.5 to 100 ppmw of protoanemonine, in each case based on the weight of the acrylic acid present in P.
Processes Producing Alkali Hydroxides, Alkali Carbonates, Alkali Bicarbonates, and/or Alkaline Earth Sulfates
The present application pertains to methods for making alkali hydroxide, or alkali carbonates, or alkali bicarbonates, or alkaline-earth sulfates. In one embodiment, a material comprising an alkaline earth is converted to an alkaline earth sulfite or bisulfite and reacted with an alkali sulfate to form an alkaline earth sulfate and alkali sulfite or bisulfite. The alkali sulfite or bisulfite is converted into an alkali hydroxide, or an alkali carbonate, or an alkali bicarbonate. In another embodiment, ammonium carbonate or ammonium bicarbonate is reacted with an alkali sulfate, to form ammonium sulfate and an alkali carbonate or alkali bicarbonate. A material comprising an alkaline earth is converted to an alkaline earth sulfite or bisulfite and reacted with the ammonium sulfate to form an alkaline earth sulfate and ammonium sulfite or ammonium bisulfite. The ammonium sulfite or bisulfite is regenerated into ammonia, or ammonium hydroxide, or ammonium carbonate, or ammonium bicarbonate.
Processes Producing Alkali Hydroxides, Alkali Carbonates, Alkali Bicarbonates, and/or Alkaline Earth Sulfates
The present application pertains to methods for making alkali hydroxide, or alkali carbonates, or alkali bicarbonates, or alkaline-earth sulfates. In one embodiment, a material comprising an alkaline earth is converted to an alkaline earth sulfite or bisulfite and reacted with an alkali sulfate to form an alkaline earth sulfate and alkali sulfite or bisulfite. The alkali sulfite or bisulfite is converted into an alkali hydroxide, or an alkali carbonate, or an alkali bicarbonate. In another embodiment, ammonium carbonate or ammonium bicarbonate is reacted with an alkali sulfate, to form ammonium sulfate and an alkali carbonate or alkali bicarbonate. A material comprising an alkaline earth is converted to an alkaline earth sulfite or bisulfite and reacted with the ammonium sulfate to form an alkaline earth sulfate and ammonium sulfite or ammonium bisulfite. The ammonium sulfite or bisulfite is regenerated into ammonia, or ammonium hydroxide, or ammonium carbonate, or ammonium bicarbonate.
Processes Producing Alkali Hydroxides, Alkali Carbonates, Alkali Bicarbonates, and/or Alkaline Earth Sulfates
The present application pertains to methods for making alkali hydroxide, or alkali carbonates, or alkali bicarbonates, or alkaline-earth sulfates. In one embodiment, a material comprising an alkaline earth is converted to an alkaline earth sulfite or bisulfite and reacted with an alkali sulfate to form an alkaline earth sulfate and alkali sulfite or bisulfite. The alkali sulfite or bisulfite is converted into an alkali hydroxide, or an alkali carbonate, or an alkali bicarbonate. In another embodiment, ammonium carbonate or ammonium bicarbonate is reacted with an alkali sulfate, to form ammonium sulfate and an alkali carbonate or alkali bicarbonate. A material comprising an alkaline earth is converted to an alkaline earth sulfite or bisulfite and reacted with the ammonium sulfate to form an alkaline earth sulfate and ammonium sulfite or ammonium bisulfite. The ammonium sulfite or bisulfite is regenerated into ammonia, or ammonium hydroxide, or ammonium carbonate, or ammonium bicarbonate.
Process for purification of tetrahydrocannabinolic- and cannabidiolic acid from plant material extract
The present invention relates to a highly economic process for the purification of a cannabinoid acid, more specifically THCA or CBDA, from either a crude cannabis plant material or a cell culture of said cannabis plant, using ion exchange resins. The purified cannabinoid acid obtained may then be decarboxylated to yield the corresponding cannabinoid, i.e., THC or CBD, respectively.
Process for purification of tetrahydrocannabinolic- and cannabidiolic acid from plant material extract
The present invention relates to a highly economic process for the purification of a cannabinoid acid, more specifically THCA or CBDA, from either a crude cannabis plant material or a cell culture of said cannabis plant, using ion exchange resins. The purified cannabinoid acid obtained may then be decarboxylated to yield the corresponding cannabinoid, i.e., THC or CBD, respectively.
Process for purification of tetrahydrocannabinolic- and cannabidiolic acid from plant material extract
The present invention relates to a highly economic process for the purification of a cannabinoid acid, more specifically THCA or CBDA, from either a crude cannabis plant material or a cell culture of said cannabis plant, using ion exchange resins. The purified cannabinoid acid obtained may then be decarboxylated to yield the corresponding cannabinoid, i.e., THC or CBD, respectively.
METHOD FOR PRODUCING PURIFIED ACETIC ACID
Provided is a method for producing purified acetic acid with a good hue. A method for producing purified acetic acid, including treating acetic acid having a poor hue with a synthetic adsorbent to obtain acetic acid with an improved hue. The acetic acid to be treated is, for example, acetic acid having an absorbance of 0.01 or greater at a wavelength of 430 nm. The acetic acid to be treated may be acetic acid recovered from an acetic acid-containing solution that is discharged in a cellulose acetate production process. The synthetic adsorbent may have a cation exchange group on a resin surface. The synthetic adsorbent may have a pore structure.
METHOD FOR PRODUCING PURIFIED ACETIC ACID
Provided is a method for producing purified acetic acid with a good hue. A method for producing purified acetic acid, including treating acetic acid having a poor hue with a synthetic adsorbent to obtain acetic acid with an improved hue. The acetic acid to be treated is, for example, acetic acid having an absorbance of 0.01 or greater at a wavelength of 430 nm. The acetic acid to be treated may be acetic acid recovered from an acetic acid-containing solution that is discharged in a cellulose acetate production process. The synthetic adsorbent may have a cation exchange group on a resin surface. The synthetic adsorbent may have a pore structure.