C07C51/50

Water-based extraction and purification processes for cannabinoid acids

The present invention relates to methods of extracting cannabinoid acids from cannabis plant material by combining the plant material with an aqueous solution having a high pH to solubilize cannabinoid acid anions, followed by precipitation of the cannabinoid acids at low pH and filtration. The method provides yields of up to 97%, while high pH purification of ethanol extracted oils yielded purities up to 86%.

METHOD FOR PRODUCING EASILY POLYMERIZABLE COMPOUND
20230202960 · 2023-06-29 · ·

A method for producing an easily polymerizable compound, comprising a polymerization prevention step of supplying an oxygen-containing gas to an easily polymerizable compound-containing liquid through a gas supply means having one or more supply ports, wherein an area S (mm.sup.2) per one supply port is 0.1 or more and 20 or less, and a ratio V/S of a linear velocity V (m/s) of the gas at the supply port to the area S in the polymerization preventing step is 6.0 or more.

METHOD FOR PRODUCING EASILY POLYMERIZABLE COMPOUND
20230202960 · 2023-06-29 · ·

A method for producing an easily polymerizable compound, comprising a polymerization prevention step of supplying an oxygen-containing gas to an easily polymerizable compound-containing liquid through a gas supply means having one or more supply ports, wherein an area S (mm.sup.2) per one supply port is 0.1 or more and 20 or less, and a ratio V/S of a linear velocity V (m/s) of the gas at the supply port to the area S in the polymerization preventing step is 6.0 or more.

Process for producing acetic acid

A process for producing acetic acid including an acetic acid collection step for feeding a first distillation column with a volatile component at least containing acetic acid, methyl acetate, methyl iodide, water, and hydrogen iodide. Separating a first lower boiling point component as an overhead, and collecting a first liquid stream containing acetic acid. An acetic acid purification step for feeding a second distillation column with the first liquid stream, and separating a second lower boiling point component as an overhead. Collecting a second liquid stream containing acetic acid. An alkali component is added or mixed for distilling a mixture to be treated containing the first liquid stream and the alkali component in the second distillation column. In the mixture, at least one component (A) having a boiling point lower than acetic acid. The at least one component (A) having a concentration of 0.1 to 15% by weight.

Process for producing acetic acid

A process for producing acetic acid including an acetic acid collection step for feeding a first distillation column with a volatile component at least containing acetic acid, methyl acetate, methyl iodide, water, and hydrogen iodide. Separating a first lower boiling point component as an overhead, and collecting a first liquid stream containing acetic acid. An acetic acid purification step for feeding a second distillation column with the first liquid stream, and separating a second lower boiling point component as an overhead. Collecting a second liquid stream containing acetic acid. An alkali component is added or mixed for distilling a mixture to be treated containing the first liquid stream and the alkali component in the second distillation column. In the mixture, at least one component (A) having a boiling point lower than acetic acid. The at least one component (A) having a concentration of 0.1 to 15% by weight.

Process for producing acetic acid

A process for producing acetic acid including an acetic acid collection step for feeding a first distillation column with a volatile component at least containing acetic acid, methyl acetate, methyl iodide, water, and hydrogen iodide. Separating a first lower boiling point component as an overhead, and collecting a first liquid stream containing acetic acid. An acetic acid purification step for feeding a second distillation column with the first liquid stream, and separating a second lower boiling point component as an overhead. Collecting a second liquid stream containing acetic acid. An alkali component is added or mixed for distilling a mixture to be treated containing the first liquid stream and the alkali component in the second distillation column. In the mixture, at least one component (A) having a boiling point lower than acetic acid. The at least one component (A) having a concentration of 0.1 to 15% by weight.

ACRYLIC ACID PRODUCTION PROCESS

Provided herein are methods of producing acrylic acid from bPL. Such methods involve the use of a heterogeneous catalyst, such as a zeolite at vapor phase conditions. The method may use a fixed bed, moving bed or fluidized contacting zone as the reactor configurations.

ACRYLIC ACID PRODUCTION PROCESS

Provided herein are methods of producing acrylic acid from bPL. Such methods involve the use of a heterogeneous catalyst, such as a zeolite at vapor phase conditions. The method may use a fixed bed, moving bed or fluidized contacting zone as the reactor configurations.

METHOD FOR PRODUCING VAPOR COMPOSITION CONTAINING LACTIC ACID
20170253553 · 2017-09-07 ·

The method for producing a vapor composition containing lactic acid of the present invention is capable of suppressing the generation of by-products such as acetaldehyde and carbon monoxide due to pyrolysis of a lactic acid species during vaporization. Furthermore, a lactic acid oligomer generated can be effectively used without loss, and a vapor composition containing lactic acid can be industrially efficiently produced stably for a long time. The present invention relates to a method for producing a vapor composition containing lactic acid including: feeding a liquid composition containing lactic acid to a vaporizer; mixing the liquid composition with a liquid composition containing a lactic acid oligomer contained in the vaporizer to prepare a liquid mixture; and heating the liquid mixture to vaporize part of the liquid mixture, whereby a vapor composition containing lactic acid is produced.

METHOD FOR PRODUCING VAPOR COMPOSITION CONTAINING LACTIC ACID
20170253553 · 2017-09-07 ·

The method for producing a vapor composition containing lactic acid of the present invention is capable of suppressing the generation of by-products such as acetaldehyde and carbon monoxide due to pyrolysis of a lactic acid species during vaporization. Furthermore, a lactic acid oligomer generated can be effectively used without loss, and a vapor composition containing lactic acid can be industrially efficiently produced stably for a long time. The present invention relates to a method for producing a vapor composition containing lactic acid including: feeding a liquid composition containing lactic acid to a vaporizer; mixing the liquid composition with a liquid composition containing a lactic acid oligomer contained in the vaporizer to prepare a liquid mixture; and heating the liquid mixture to vaporize part of the liquid mixture, whereby a vapor composition containing lactic acid is produced.