Patent classifications
C07C303/14
HIGH-EFFICIENCY CYCLIC PREPARATION METHOD FOR COLUMNAR TAURINE
Disclosed is a high-efficiency cyclic preparation method for a columnar taurine finished product, including: preparing an aqueous taurine solution with a certain concentration; introducing the aqueous taurine solution into a basic resin for treatment to remove an alkali metal isethionate and an isethionic acid derivative; monitoring an effluent liquid at an outlet of the basic resin and collecting the effluent liquid that is monitored to be qualified; and crystallizing taurine of the collected effluent liquid to obtain a taurine crystal. The method of the present disclosure has the advantages of process innovation, and high efficiency, and the obtained taurine crystal has the advantages of good quality, good fluidity, no caking, low production cost and high efficiency, and has good prospects for industrial production.
UNSATURATED FATTY ALCOHOL DERIVATIVES FROM NATURAL OIL METATHESIS
- David R. Allen ,
- Marcos Alonso ,
- Mary Beddaoui ,
- Randal J. Bernhardt ,
- Aaron Brown ,
- Scott Dillavou ,
- Xue Min Dong ,
- Wilma Gorman ,
- John C. Hutchison ,
- Gary Luebke ,
- Renee Luka ,
- Franz Luxem ,
- Andrew D. Malec ,
- Ronald A. Masters ,
- Dennis S. Murphy ,
- Nicholas Pendleton ,
- Irma Ryklin ,
- Patti Skelton ,
- Brian Sook ,
- Chris SPAULDING ,
- Krista Turpin ,
- Gregory Wallace ,
- Michael Wiester ,
- Patrick Shane Wolfe
Sulfate and sulfonate derivatives of unsaturated fatty alcohols, processes for making them, and methods of using them are disclosed. In one aspect, a monounsaturated fatty alcohol composition is made by reducing a metathesis-derived monounsaturated alkyl ester. The fatty alcohol composition is then converted to a sulfate or sulfonate derivative by one or more of alkoxylation, sulfation, sulfonation, and sulfitation. Of particular interest are the sulfate and ether sulfate derivatives. Microscopy studies indicate that the unsaturated sodium sulfates in particular have a lamellar phase that should enable formulation at high actives levels. Sulfate compositions comprising 40 to 60 wt. % of a monounsaturated fatty primary alcohol sulfate and 40 to 60 wt. % of a secondary hydroxyalkyl primary alcohol sulfate are also disclosed. The derivatives and sulfate compositions are valuable for many end-use applications, including, for example, agricultural dispersants, water-soluble herbicides, anionic emulsifiers for agricultural use, hard surface cleaners, light-duty liquid detergents, personal cleansers, gas well foamers for oilfield applications, laundry detergents, enhanced oil recovery compositions, latex paints, and specialty foams.
UNSATURATED FATTY ALCOHOL DERIVATIVES FROM NATURAL OIL METATHESIS
- David R. Allen ,
- Marcos Alonso ,
- Mary Beddaoui ,
- Randal J. Bernhardt ,
- Aaron Brown ,
- Scott Dillavou ,
- Xue Min Dong ,
- Wilma Gorman ,
- John C. Hutchison ,
- Gary Luebke ,
- Renee Luka ,
- Franz Luxem ,
- Andrew D. Malec ,
- Ronald A. Masters ,
- Dennis S. Murphy ,
- Nicholas Pendleton ,
- Irma Ryklin ,
- Patti Skelton ,
- Brian Sook ,
- Chris SPAULDING ,
- Krista Turpin ,
- Gregory Wallace ,
- Michael Wiester ,
- Patrick Shane Wolfe
Sulfate and sulfonate derivatives of unsaturated fatty alcohols, processes for making them, and methods of using them are disclosed. In one aspect, a monounsaturated fatty alcohol composition is made by reducing a metathesis-derived monounsaturated alkyl ester. The fatty alcohol composition is then converted to a sulfate or sulfonate derivative by one or more of alkoxylation, sulfation, sulfonation, and sulfitation. Of particular interest are the sulfate and ether sulfate derivatives. Microscopy studies indicate that the unsaturated sodium sulfates in particular have a lamellar phase that should enable formulation at high actives levels. Sulfate compositions comprising 40 to 60 wt. % of a monounsaturated fatty primary alcohol sulfate and 40 to 60 wt. % of a secondary hydroxyalkyl primary alcohol sulfate are also disclosed. The derivatives and sulfate compositions are valuable for many end-use applications, including, for example, agricultural dispersants, water-soluble herbicides, anionic emulsifiers for agricultural use, hard surface cleaners, light-duty liquid detergents, personal cleansers, gas well foamers for oilfield applications, laundry detergents, enhanced oil recovery compositions, latex paints, and specialty foams.
Process for making renewable surfactant intermediates and surfactants from fats and oils and products thereof
The present invention relates generally to methods for producing renewable detergent compounds. More specifically, the invention relates to methods for producing detergent intermediates, including bio-linear alkylbenzene (LAB), bio-alcohols, and long chain bio-paraffins, from natural oils.
Process for making renewable surfactant intermediates and surfactants from fats and oils and products thereof
The present invention relates generally to methods for producing renewable detergent compounds. More specifically, the invention relates to methods for producing detergent intermediates, including bio-linear alkylbenzene (LAB), bio-alcohols, and long chain bio-paraffins, from natural oils.
Process for making renewable surfactant intermediates and surfactants from fats and oils and products thereof
The present invention relates generally to methods for producing renewable detergent compounds. More specifically, the invention relates to methods for producing detergent intermediates, including bio-linear alkylbenzene (LAB), bio-alcohols, and long chain bio-paraffins, from natural oils.
Unsaturated fatty alcohol derivatives from natural oil metathesis
- David R. Allen ,
- Marcos Alonso ,
- Mary Beddaoui ,
- Randal J. Bernhardt ,
- Aaron Brown ,
- Scott Dillavou ,
- Xue Min Dong ,
- Wilma Gorman ,
- John C. Hutchison ,
- Gary Luebke ,
- Renee Luka ,
- Franz Luxem ,
- Andrew D Malec ,
- Ronald A. Masters ,
- Dennis S. Murphy ,
- Nicholas Pendleton ,
- Irma Ryklin ,
- Patti Skelton ,
- Brian Sook ,
- Chris SPAULDING ,
- Krista Turpin ,
- Gregory Wallace ,
- Michael Wiester ,
- Patrick Shane Wolfe
Sulfate and sulfonate derivatives of unsaturated fatty alcohols, processes for making them, and methods of using them are disclosed. In one aspect, a monounsaturated fatty alcohol composition is made by reducing a metathesis-derived monounsaturated alkyl ester. The fatty alcohol composition is then converted to a sulfate or sulfonate derivative by one or more of alkoxylation, sulfation, sulfonation, and sulfitation. Of particular interest are the sulfate and ether sulfate derivatives.
Unsaturated fatty alcohol derivatives from natural oil metathesis
- David R. Allen ,
- Marcos Alonso ,
- Mary Beddaoui ,
- Randal J. Bernhardt ,
- Aaron Brown ,
- Scott Dillavou ,
- Xue Min Dong ,
- Wilma Gorman ,
- John C. Hutchison ,
- Gary Luebke ,
- Renee Luka ,
- Franz Luxem ,
- Andrew D Malec ,
- Ronald A. Masters ,
- Dennis S. Murphy ,
- Nicholas Pendleton ,
- Irma Ryklin ,
- Patti Skelton ,
- Brian Sook ,
- Chris SPAULDING ,
- Krista Turpin ,
- Gregory Wallace ,
- Michael Wiester ,
- Patrick Shane Wolfe
Sulfate and sulfonate derivatives of unsaturated fatty alcohols, processes for making them, and methods of using them are disclosed. In one aspect, a monounsaturated fatty alcohol composition is made by reducing a metathesis-derived monounsaturated alkyl ester. The fatty alcohol composition is then converted to a sulfate or sulfonate derivative by one or more of alkoxylation, sulfation, sulfonation, and sulfitation. Of particular interest are the sulfate and ether sulfate derivatives.
NOVEL PROCESS FOR THE PREPARATION OF BELINOSTAT
The present invention provides a novel and commercially viable process with high yield for the preparation of (E)-N-hydroxy-3-(3-phenylsulfamoyl-phenyl)-acrylamide, also known as Belinostat (I). The invention also provides process for purification and novel crystalline form of Belinostat in substantially pure form.
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NOVEL PROCESS FOR THE PREPARATION OF BELINOSTAT
The present invention provides a novel and commercially viable process with high yield for the preparation of (E)-N-hydroxy-3-(3-phenylsulfamoyl-phenyl)-acrylamide, also known as Belinostat (I). The invention also provides process for purification and novel crystalline form of Belinostat in substantially pure form.
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