Patent classifications
C07D303/04
Method of using biopolymer to synthesize titanium-containing silicon oxide material and applications thereof
A method of using biopolymer to synthesize titanium-containing silicon oxide material and applications thereof are disclosed. The method comprises steps: mixing a titanium source, a silicon source, an acid source, a base source, a biopolymer and a solvent to form an aqueous solution, and letting the aqueous solution react to form a semi-product; performing aging, solid-liquid separation and drying of the semi-product to obtain a dried solid; and performing calcination or extraction of the dried solid to obtain a titanium-containing silicon oxide material with a high specific surface area. The present invention adopts a biopolymer as the templating agent, which makes the fabrication process of titanium-containing silicon oxide material more environment-friendly. After calcination or extraction, the product still has superior catalytic activity, able to catalyze epoxidation of olefins and favorable for the production of epoxide.
Method of using biopolymer to synthesize titanium-containing silicon oxide material and applications thereof
A method of using biopolymer to synthesize titanium-containing silicon oxide material and applications thereof are disclosed. The method comprises steps: mixing a titanium source, a silicon source, an acid source, a base source, a biopolymer and a solvent to form an aqueous solution, and letting the aqueous solution react to form a semi-product; performing aging, solid-liquid separation and drying of the semi-product to obtain a dried solid; and performing calcination or extraction of the dried solid to obtain a titanium-containing silicon oxide material with a high specific surface area. The present invention adopts a biopolymer as the templating agent, which makes the fabrication process of titanium-containing silicon oxide material more environment-friendly. After calcination or extraction, the product still has superior catalytic activity, able to catalyze epoxidation of olefins and favorable for the production of epoxide.
System for Energy Regeneration Using Mechanical Vapor Recompression in Combined Chemical Process
The present disclosure provides a system for energy recycling using mechanical vapor recompression in combined chemical process, the system including a heat exchange reactor for generating an intermediate material by means of an exothermic reaction and discharging the generated intermediate material, and heat-exchanging heat generated in the exothermic reaction with water supplied from outside so as to generate water vapor; an absorption tank for receiving the intermediate material, and mixing the intermediate material with water, so as to generate an intermediate material aqueous solution; a stripper for receiving the intermediate material aqueous solution, and separating the intermediate material into an intermediate material gas and an intermediate material water-rich aqueous solution; an endothermic reactor for receiving the intermediate material water-rich aqueous solution, and reacting the intermediate material with water, so as to generate a final product aqueous solution; an evaporation concentrator for receiving the final product aqueous solution, and heat-exchanging heat of the water vapor from the heat exchange reactor with the final product aqueous solution so as to generate steam; a dehydrating distillation tower for receiving, dehydrating, and purifying the final product aqueous solution discharged from the evaporation concentrator; and a mechanical vapor recompressor for compressing the steam from the evaporation concentrator, and providing the compressed steam as a source of heat or a source of steam supply.
Preparation Method For Propylene Epoxidation Catalyst, And Application Thereof
A preparation method for a propylene epoxidation catalyst: pre-hydrolyzing a silicon source, adding a titanium source and reacting to form a sol, atomizing the sol and then spraying it into liquid ammonia for molding, implementing pore broadening, and performing drying, calcination, and silanization treatment to obtain a TiSiO.sub.2 composite oxide catalyst. The present catalyst can be used in the chemical process of preparing propylene oxide by epoxidation of propylene, the average propylene oxide selectivity being up to 97.5%, having prospects for industrial application.
Method of using biopolymer to synthesize titanium-containing silicon oxide material and applications thereof
A method of using biopolymer to synthesize titanium-containing silicon oxide material and applications includes mixing a titanium source, a silicon source, an acid source, a base source, a biopolymer and a solvent to form an aqueous solution, and letting the aqueous solution react to form a semi-product; performing aging, solid-liquid separation and drying of the semi-product to obtain a dried solid; and performing calcination or extraction of the dried solid to obtain a titanium-containing silicon oxide material with a high specific surface area. The present invention adopts a biopolymer as the templating agent, which makes the fabrication process of titanium-containing silicon oxide material more environment-friendly. After calcination or extraction, the product still has superior catalytic activity, able to catalyze epoxidation of olefins and favorable for the production of epoxide.
Method of using biopolymer to synthesize titanium-containing silicon oxide material and applications thereof
A method of using biopolymer to synthesize titanium-containing silicon oxide material and applications includes mixing a titanium source, a silicon source, an acid source, a base source, a biopolymer and a solvent to form an aqueous solution, and letting the aqueous solution react to form a semi-product; performing aging, solid-liquid separation and drying of the semi-product to obtain a dried solid; and performing calcination or extraction of the dried solid to obtain a titanium-containing silicon oxide material with a high specific surface area. The present invention adopts a biopolymer as the templating agent, which makes the fabrication process of titanium-containing silicon oxide material more environment-friendly. After calcination or extraction, the product still has superior catalytic activity, able to catalyze epoxidation of olefins and favorable for the production of epoxide.
Diesel Detergent Without A Low Molecular Weight Penalty
The composition of the present invention related to a quaternary ammonium salt detergent and the use of such quaternary ammonium salt detergents in a fuel composition to reduce diesel injector deposits and remove or clean up existing deposits on the diesel injectors.
Diesel Detergent Without A Low Molecular Weight Penalty
The composition of the present invention related to a quaternary ammonium salt detergent and the use of such quaternary ammonium salt detergents in a fuel composition to reduce diesel injector deposits and remove or clean up existing deposits on the diesel injectors.
Process for producing epoxy alcohol compound
A compound represented by formula (II): ##STR00001## (where Ar represents a phenyl group optionally substituted by 1 to 3 substituents selected from the group consisting of a halogen atom and a trifluoromethyl group, and R represents a hydrogen atom or an alkyl group having 1 to 12 carbon atoms) is produced by step A: reacting trimethyl oxosulfonium salt or trimethyl sulfonium salt with a base in a solvent, and removing the resulting solid to obtain a trimethyl oxosulfonium ylide solution or a trimethyl sulfonium ylide solution; and step B: reacting a compound represented by formula (I): ##STR00002## and the solution obtained in step A, and the compound represented by formula (II) can be derived to a compound represented by formula (V): ##STR00003## that is useful for production of an antifungal agent.
Process for producing epoxy alcohol compound
A compound represented by formula (II): ##STR00001## (where Ar represents a phenyl group optionally substituted by 1 to 3 substituents selected from the group consisting of a halogen atom and a trifluoromethyl group, and R represents a hydrogen atom or an alkyl group having 1 to 12 carbon atoms) is produced by step A: reacting trimethyl oxosulfonium salt or trimethyl sulfonium salt with a base in a solvent, and removing the resulting solid to obtain a trimethyl oxosulfonium ylide solution or a trimethyl sulfonium ylide solution; and step B: reacting a compound represented by formula (I): ##STR00002## and the solution obtained in step A, and the compound represented by formula (II) can be derived to a compound represented by formula (V): ##STR00003## that is useful for production of an antifungal agent.