C08B31/12

AMPHIPHILIC POLYSACCHARIDES, POLYSACCHARIDE-BASED HYDROGELS, AND METHODS OF MANUFACTURE

A method for the synthesis of alkyl -carboxy(hydroxyethyl) polysaccharides is described. The method includes methylating or ethylating a polysaccharide or providing a methylated or ethylated polysaccharide, hydroxyethylating the methylated or ethylated polysaccharide, and oxidizing the hydroxyethylated polysaccharide to form the -carboxy(hydroxyethyl) polysaccharide. A method for the synthesis of oxidized polysaccharides is also described. The method includes hydroxypropylating a polysaccharide and oxidizing the hydroxypropylated polysaccharides. A method for the production of a solid capable of forming a hydrogel is also described. The method includes combining a first solution comprising an oxidized oligo(hydroxypropyl) polysaccharide bearing one or more ketone groups with a second solution comprising an amine substituted polysaccharide to form a third solution, and removing solvent from the third solution to form the solid, or adding an additional solvent to the third solution to precipitate the solid. Novel polysaccharides and hydrogels prepared according to these methods are also described.

Leuco polymers as bluing agents in laundry care compositions

A leuco polymer comprising a polymeric carbohydrate and a leuco moiety. The polymeric carbohydrate and the leuco moiety are covalently bound. Methods of making the leuco polymer, laundry care compositions comprising the leuco polymer and methods of treating textiles with such laundry care compositions.

STARCH-CONTAINING MICROSPHERE AND PREPARATION METHOD AND USE THEREOF
20210032373 · 2021-02-04 ·

A starch-containing microsphere has a particle size that exhibits polydispersity with uniform distribution in a particle size concentrated distribution interval. The particle size distribution in the particle size concentrated distribution interval has the following features: equal division of the particle size concentrated distribution interval into n intervals, and a microsphere percentage in each interval is formula (I),

[00001] 100 n .Math. .Math. % 1 .Math. 0 n .Math. .Math. % , ( I )

where n is an integer greater than 1. The preparation method of the starch-containing microsphere includes: first reacting starch with a low concentration of epichlorohydrin, and then reacting the resultant product with a surfactant, followed by final crosslinking to give microspheres. The starch-containing microspheres thus prepared are polydisperse starch-containing microspheres with a uniform particle size distribution, with the particle size being in a range of 0.1-500 m.

STARCH-CONTAINING MICROSPHERE AND PREPARATION METHOD AND USE THEREOF
20210032373 · 2021-02-04 ·

A starch-containing microsphere has a particle size that exhibits polydispersity with uniform distribution in a particle size concentrated distribution interval. The particle size distribution in the particle size concentrated distribution interval has the following features: equal division of the particle size concentrated distribution interval into n intervals, and a microsphere percentage in each interval is formula (I),

[00001] 100 n .Math. .Math. % 1 .Math. 0 n .Math. .Math. % , ( I )

where n is an integer greater than 1. The preparation method of the starch-containing microsphere includes: first reacting starch with a low concentration of epichlorohydrin, and then reacting the resultant product with a surfactant, followed by final crosslinking to give microspheres. The starch-containing microspheres thus prepared are polydisperse starch-containing microspheres with a uniform particle size distribution, with the particle size being in a range of 0.1-500 m.

REACTIVE POLYSACCHARIDE-BASED HEMOSTATIC AGENT

Compositions and methods related to powdered hemostats that crosslink during and/or after application to a bleeding site are generally described.

METHOD FOR MODIFYING POLYSACCHARIDE MATERIAL BY SEQUENCED HOMOGENEOUS CHEMICAL FUNCTIONALISATION

The present invention concerns a method for modifying a polysaccharide material, preferably an amylaceous material, involving a first step of homogeneous solubilisation of said polysaccharide material in an aqueous solvent, followed by a step of homogeneous chemical functionalisation comprising at least one non-crosslinking chemical modification, or at least one crosslinking chemical modification, or a sequence of at least one non-crosslinking chemical modification and at least one crosslinking chemical modification. Secondly, the present invention concerns a modified polysaccharide material, in particular obtained by the method according to the invention, characterised in that it has a novel distribution of the chemical substituents attached to the hydroxyl functions of the anhydroglucose units of said polysaccharide material. The novel starches can be used as organic adjuvants for dry mortars made from cement or made from gypsum, in particular as a binder for a dry mortar made from cement or as a thickening agent for a mortar made from plaster.

METHOD FOR MODIFYING POLYSACCHARIDE MATERIAL BY SEQUENCED HOMOGENEOUS CHEMICAL FUNCTIONALISATION

The present invention concerns a method for modifying a polysaccharide material, preferably an amylaceous material, involving a first step of homogeneous solubilisation of said polysaccharide material in an aqueous solvent, followed by a step of homogeneous chemical functionalisation comprising at least one non-crosslinking chemical modification, or at least one crosslinking chemical modification, or a sequence of at least one non-crosslinking chemical modification and at least one crosslinking chemical modification. Secondly, the present invention concerns a modified polysaccharide material, in particular obtained by the method according to the invention, characterised in that it has a novel distribution of the chemical substituents attached to the hydroxyl functions of the anhydroglucose units of said polysaccharide material. The novel starches can be used as organic adjuvants for dry mortars made from cement or made from gypsum, in particular as a binder for a dry mortar made from cement or as a thickening agent for a mortar made from plaster.

MONOLITHIC COMPOSITION FOR DUAL-RATE RELEASE WITH HIGH DRUG LOADING
20240009313 · 2024-01-11 ·

The present document describes a process for the preparation of a low functionalization polysaccharide having carboxyl groups, comprising a) swelling of a polysaccharide granule in boiling water or a water/polyol mixture, to obtain a swollen polysaccharide; b) partial gelatinization of said swollen polysaccharide in an alkaline solvent mixture of water and alcohol and/or polyol, to obtain a partially gelatinized polysaccharide; and c) partial functionalization of said partially gelatinized polysaccharide with a functionalizing agent, to obtain the low functionalization polysaccharide.

MONOLITHIC COMPOSITION FOR DUAL-RATE RELEASE WITH HIGH DRUG LOADING
20240009313 · 2024-01-11 ·

The present document describes a process for the preparation of a low functionalization polysaccharide having carboxyl groups, comprising a) swelling of a polysaccharide granule in boiling water or a water/polyol mixture, to obtain a swollen polysaccharide; b) partial gelatinization of said swollen polysaccharide in an alkaline solvent mixture of water and alcohol and/or polyol, to obtain a partially gelatinized polysaccharide; and c) partial functionalization of said partially gelatinized polysaccharide with a functionalizing agent, to obtain the low functionalization polysaccharide.

Joint compound with sulfonated starch

Provided herein is a joint compound having a composition to allow tools to easily clean up, comprising water, at least one inert filler, and a binder comprising a sulfonated starch, and a method of preparing the joint compound.