C11C1/025

FISH OIL CHOLESTEROL

The present disclosure describes that high purity cholesterol is obtained by the processes of the invention without any further purification step, such as a crystallizing step from a solvent, but rather by distilling steps alone. The disclosures provides a process that includes the production of compositions having a cholesterol content over 75% in weight, from fish oil processing waste residues.

Potassium soaps that can be thickened with chloride salts
10793808 · 2020-10-06 · ·

Natural liquid potassium soap compositions and methods of manufacturing and using the same are provided with thickening by the addition of chloride salts, such as sodium chloride and potassium chloride. The natural liquid potassium soap compositions may contain one or more fatty acids with carbon length ranging from four (C4) to twenty-two (C22) or natural fatty acid mixtures with coconut oil, olive oil, tallow, sunflower oil, safflower oil, and/or tall oil fatty acids which are saponified with lye. The saponification lye is preferably potassium hydroxide. Preferred embodiments contain potassium salts of fatty acids comprising at least oleic acid (C18:1 cis-9), olive oils, coconut oils or mixtures thereof. The chloride salt is added in either solid or liquid form following saponification and neutralization.

METHODS FOR MAKING FREE FATTY ACIDS FROM SOAPS USING THERMAL HYDROLYSIS FOLLOWED BY ACIDIFICATION

Provided are methods, processes and systems for treating a soapstock. In alternative embodiments, provided are systems and methods for treating a soapstock to generate free fatty acids and/or fatty acid derivatives, e.g. fatty acid alkyl esters. In alternative embodiments, provided are systems and methods for realizing the full fatty acid yield of a soapstock by first converting substantially all of the saponifiable material in a soapstock to salts of fatty acids (soaps) and acidulating the soaps to generate free fatty acids and/or fatty acid derivatives, e.g. fatty acid alkyl esters, wherein the soapstock comprises soaps and saponifiable lipids, e.g. glycerides and/or phospholipids, and the generating of free fatty acids and/or fatty acid is achieved.

METHOD FOR PRODUCTION OF FATTY ACIDS

A process for production fatty acids comprising: adjusting pH of a saponifiable material to a value above pH 7 by adding alkaline material; saponifying all saponifiable material by passing alternate electrical current through the material, wherein the said step of saponification occurs in a saponification reactor; acidulating the saponified material by adding acid to pH value below 4; isolating obtained free fatty acids from aqueous layer.

Solvent extraction of oil from distillers dried grains and methods of using extraction products

A process for extraction of crude oil from distillers dried grain solubles and/or distillers dried grains and producing corn distillers meal that may be used as a livestock supplement is disclosed. For example, the corn distillers meal may be used as a crude protein supplement for use in a livestock feed diet or a poultry feed diet. The solvent extracted crude oil may be suitable for oleochemical processing for personal care and home care products, biodiesel production, and/or renewable diesel production from hydro-treating the extracted oil to make green diesel fuel.

Method for Reducing the Content of Saturated Monoglycerides in a Raw Biodiesel
20200199471 · 2020-06-25 ·

The invention relates to a method for reducing the content of monoglycerides (MG), in particular saturated monoglycerides (GMG), in a raw biodiesel (RB), which has a content of monoglycerides (MG) of between 0.4 and 0.7 wt % and a content of free fatty acids (FFA) of less than or equal to 0.25 wt %, comprising the following steps: A) providing the raw biodiesel (RB) having the constituents indicated above in the concentrations indicated above; B) adding (1) an alkaline aqueous solution (L) to the raw biodiesel (RB); C) mixing the alkaline aqueous solution (L), and thus glycerides in the biodiesel, preferably monoglycerides (MG), in particular saturated monoglycerides (GMG), being hydrolyzed; D) performing a first centrifugal separation (2) of a heavy phase (6) comprising the alkaline aqueous solution (L) with the hydrolyzed constituents from a light phase (7) comprising the biodiesel; E) drying (5) the light phase (7) or (9) in order to provide a processed biodiesel for use as a fuel having a content of monoglycerides of less than 0.4 wt %. The invention further relates to a use according to the invention.

Squalene extraction from seed oils

A method for squalene extraction from a seed oil includes converting fatty acids of the seed oil into soap by subjecting the seed oil to a saponification reaction to obtain a saponified product, and adsorbing the fatty acids of the seed oil on surfaces of iron oxide nanoparticles to obtain iron oxide nanoparticles coated with fatty acids. The method may further include washing the iron oxide nanoparticles coated with fatty acids with a polar solvent to obtain a third mixture including a polar phase and the iron oxide nanoparticles coated with fatty acids, separating the iron oxide nanoparticles coated with fatty acids from the third mixture by a magnetic field, mixing the polar phase with a non-polar solvent and distilled water to obtain a two-phase solution, the two-phase solution including a non-polar phase and an aqueous phase, and separating and drying the non-polar phase to obtain squalene.

SOLID/LIQUID EXTRACTION
20200069978 · 2020-03-05 ·

The present application relates to an oil extracted from a solid vegetable matter or a micro-organism comprising a high unsaponifiable content, the solid vegetable from which the oil has been extracted and the micro-organism from which the oil has been extracted.

Preparation of vegetable-based stearic acid
10508251 · 2019-12-17 · ·

One or more techniques are disclosed for a process of preparing a concentrated form of a vegetable-based stearic acid from a plant source. The process may comprise drying and deodorizing a vegetable based emulsion; and further concentrating the resulting fatty acid and triglyceride mix. The process may further comprise distillation of the resulting concentrated fatty acid and triglyceride mix, to separate the free fatty acids from the triglycerides. Additionally, the process may comprise fractional distillation of the free fatty acid distillate, to produce a concentrated from of the stearic acid, separating it from other fatty acids.

PARTIAL CALCIFICATION OF FREE FATTY ACID MIXTURES, LIVESTOCK FEED COMPOSITIONS INCLUDING THEM, AND METHODS OF MAKING SAME
20190373918 · 2019-12-12 ·

The present invention includes a nutritional supplement composition that may be used for livestock and the like, as well as to a livestock feed mixture containing same. Also included are methods of preparing the nutritional supplement composition, the livestock feed mixture, as well as methods of providing nutrition to livestock and the like. The livestock feed composition comprises: (a) a solid particulate livestock feed material and (b) a solidified particulate mixture of (i) free fatty acid and (ii) a calcium salt of a fatty acid, the calcium salt of a fatty acid being present in a molar ratio amount in the range of from about 25% to about 55% of the amount of the free fatty acid. The preferred mixture is a solid having an onset melt point of between about 140 and 170 degrees Fahrenheit, and a hardness of from about 5 to about 15 Shore A units at 170 degrees Fahrenheit.