B01J2208/0007

PROCESS AND REACTOR ASSEMBLY FOR THE ENHANCEMENT OF HYDRODYNAMICS IN A GAS-SOLIDS FLUIDIZED BED REACTOR

A process for polymerizing olefin monomer(s) in a gas-solids olefin polymerization reactor comprising a top zone; a middle zone, which comprises a top end in direct contact with said top zone and which is located below said top zone, the middle zone having a generally cylindrical shape; and a bottom zone, which is in direct contact with a bottom end of the middle zone and which is located below the middle zone; comprising the following steps: introducing a fluidization gas stream into the bottom zone; polymerizing olefin monomer(s) in the presence of a polymerization catalyst in a dense phase formed by particles of a polymer of the olefin monomer(s) suspended in an upwards flowing stream of the fluidization gas in the middle zone; introducing a jet gas stream through one or more jet gas feeding ports in a jet gas feeding area of the middle zone at the dense phase in the middle zone of the gas-solids olefin polymerization reactor; wherein the kinetic energy (E.sub.JG) input in the reactor by the jet stream is between 1.5 and 50 times higher than the kinetic energy (E.sub.FG) input in the reactor by the fluidization gas stream (FG).

Efficient in-situ catalyst sulfiding methods and systems

A system and method is disclosed for efficiently sulfiding metal catalyst resident in a reactor vessel comprises a sulfiding module and a hydrogen sulfide detection module and a remote computer all arranged and configured to communicate wirelessly and to allow remote control and monitoring of the modules and sulfiding process.

Method of producing carbon nanotubes in fluidized bed reactor

A method of producing carbon nanotubes in a fluidized bed reactor includes preparing a carbon nanotube by supplying a catalyst and a carbon source to an interior of the fluidized bed reactor having an internal pressure of 0.5 barg to 1.2 barg (gauge pressure), thereby improving the yield and purity of carbon nanotubes.

Fluidized Bed Reactor Apparatus and a Method for Processing Organic Material Using a Fluidized Bed Reactor Apparatus
20220152569 · 2022-05-19 ·

Fluidized bed reactor apparatus, comprising a cylindrical reactor chamber (10), and a rotating shaft (14) equipped with radially extending fluidization units (16) disposed in the reactor chamber (10), said rotating shaft (14) being connected to a drive unit (42). The apparatus further comprising means for feeding fluidizing bed material into the rector chamber (10), creating a fluidized bed (28) in the reactor chamber (10), means for feeding organic material that shall be processed into the fluidized bed (28) in the reactor chamber (10), and one or more outlets (22,24) for discharge of material, gases and vapors, wherein the process in the reactor chamber (10) is controlled by a control system (40) connected to at least the drive unit (42). The invention also relates to a method for processing organic material using a fluidized bed reactor apparatus.

Detection of polymer concentration in polymerization process using refractive index measurement

A method for determining polymer concentration can include synthesizing a polymer in a reactor under a set of parameters, wherein the reactor comprises a solution mixture having a refractive index, and wherein the solution mixture comprises a solvent, a polymer, and optionally a monomer, wherein the solution mixture has a polymer concentration; measuring the refractive index of the solution mixture; comparing the refractive index of the solution mixture with a calibration curve; and identifying the polymer concentration in the solution mixture. A system for determining polymer concentration can include a reactor containing a solution mixture comprising a solvent, a polymer, and optionally a monomer; a flash vessel fluidly coupled to the reactor to receive the solution mixture from the reactor; and a first refractometer fluidly coupled to the reactor, placed between the reactor and the flash vessel, and configured to measure a refractive index of the solution mixture.

System for energy regeneration using mechanical vapor recompression in combined chemical process
11141676 · 2021-10-12 · ·

The present disclosure provides a system for energy recycling using mechanical vapor recompression in combined chemical process, the system including a heat exchange reactor for generating an intermediate material by means of an exothermic reaction and discharging the generated intermediate material, and heat-exchanging heat generated in the exothermic reaction with water supplied from outside so as to generate water vapor; an absorption tank for receiving the intermediate material, and mixing the intermediate material with water, so as to generate an intermediate material aqueous solution; a stripper for receiving the intermediate material aqueous solution, and separating the intermediate material into an intermediate material gas and an intermediate material water-rich aqueous solution; an endothermic reactor for receiving the intermediate material water-rich aqueous solution, and reacting the intermediate material with water, so as to generate a final product aqueous solution; an evaporation concentrator for receiving the final product aqueous solution, and heat-exchanging heat of the water vapor from the heat exchange reactor with the final product aqueous solution so as to generate steam; a dehydrating distillation tower for receiving, dehydrating, and purifying the final product aqueous solution discharged from the evaporation concentrator; and a mechanical vapor recompressor for compressing the steam from the evaporation concentrator, and providing the compressed steam as a source of heat or a source of steam supply.

Temperature-controlling measure for the hydrogenation slurry bed reactor and its design method and use

A temperature-controlling measure for a hydrogenation slurry bed reactor has three control points that are set from low to high: cold hydrogen is injected automatically when the system reaches control point 1; cold oil in injected automatically when the system reaches control point 2; each pressure relief is opened automatically when the system reaches control point 3. The pressure relief point is set before and/or after the circulation pump of the reactor if internal circulation is set in the reactor; the pressure relief point is set at the reactor bottom if the internal circulation is not set; at least one pressure relief valve is set at each pressure relief point.

SYSTEM FOR GENERATING H2S IN AN ALKALINE MEDIUM AND METHOD OF USING THE SAME
20210276864 · 2021-09-09 ·

Method of producing hydrogen sulfide in an alkaline environment. A mixture having a sodium salt, elemental sulfur (S) and water is added to a reactor for the purpose of generating hydrogen sulfide (H.sub.2S) gas as the main product and sodium sulfate (Na.sub.2SO.sub.4) as a byproduct.

Fluid Catalytic Cracking of Petroleum Oil with Reduced Emissions
20210189259 · 2021-06-24 ·

A method for fluid catalytic cracking (FCC) of petroleum oil feedstock includes reacting the petroleum oil feedstock with a catalyst mixture in a reaction zone of an FCC unit to obtain a product stream including desulfurized hydrocarbon product, unreacted petroleum oil feedstock, and spent catalyst. During the reacting a process control system develops a process model based on data collected during the reacting, the process model characterizing a relationship among the feed rate of the base cracking catalyst, the feed rate of the FCC additive, the operating conditions, the composition of the product stream, and emissions from the reaction; and one or more of (i) a target feed rate of the base cracking catalyst, (ii) a target feed rate of the FCC additive, and (iii) one or more target operating conditions of the reaction in the reaction zone to reduce the emissions from the FCC unit and to increase a yield of the desulfurized hydrocarbon product in the product stream are determined.

System for generating H.SUB.2.S in an alkaline medium and method of using the same
11014808 · 2021-05-25 · ·

Method of producing hydrogen sulfide in an alkaline environment. A mixture having a sodium salt, elemental sulfur (S) and water is added to a reactor for the purpose of generating hydrogen sulfide (H.sub.2S) gas as the main product and sodium sulfate (Na.sub.2SO.sub.4) as a byproduct.