Disclosed are methods of assistance and documentation of a filling of tubular reactors including recording of filling materials and fill levels of filling materials and documenting the filling materials used, fill levels and results of a catalysis process of tubular reactors produced in such a way.

The invention relates to a filling device (1) for filling a container with a particulate material (28). The filling device (1) comprises a supply container (2) that can be filled with the particulate material (28), wherein the supply container (2) has a lower opening (2.2). Moreover, the filling device (1) comprises a radial distribution unit (3), which can be supplied with the particulate material via the lower opening (2.2) of the supply container (2) and which is connected to the supply container (2) in such a way that it can rotate about a rotational axis (A), in order to distribute in the container the particulate material (28) supplied from the supply container (2) to the distribution unit (3). The filling device is characterized in that the distribution unit (3) can be driven by a drive unit (4) that is arranged outside the supply container (2).

A regenerator vessel for adsorbing halogen-containing material from a regenerator vent gas stream has a plurality of catalyst nozzles disposed at a top portion of the regenerator vessel. A first gas outlet is associated with a chlorination zone, and a second gas outlet associated with a combustion zone. A drying zone is in fluid communication with an air heater and the drying zone located in a bottom portion of the regenerator vessel. The first gas outlet is configured to withdraw a first gas stream from the chlorination zone and the second gas outlet is configured to withdraw a second gas stream from the combustion zone. The top portion of the regenerator vessel has an adsorption zone having a vent gas inlet port, a vent gas outlet port, and a portion of an annular catalyst bed.

The present invention relates to a device, a column and a method for radial separation or reaction, wherein the adsorption chamber (9) has a charging height (H3) greater than the height of the distribution duct (6) and the height of the collecting duct (8), and the upper wall (2) of the adsorption chamber (9) comprises at least one inlet (16) for washing solvent.

A fixed bed reactor system for the oxidative dehydrogenation of ethane, comprising a catalyst bed wherein the catalyst capacity profile increases along the length of catalyst bed from the upstream end to the downstream end. The catalyst bed may include one or more sections, across one or more fixed bed reactors, that are identified by a change in catalyst capacity. Catalyst capacity, or the ability to convert ethane into ethylene, may be altered by changing the dilution ratio, void fraction, and or the 35% conversion temperature. A method for loading a fixed bed reactor with an increasing catalyst capacity is also described.

A reactor and a process for fluid catalytic cracking (FCC) a hydrocarbon feed in the riser-reactor, the process including injecting the hydrocarbon feed into an evaporation zone of the riser-reactor, injecting a first catalyst into the evaporation zone, wherein the first catalyst mixes with the hydrocarbon feed to generate a hydrocarbons stream in the evaporation zone, and wherein the temperature in the evaporation zone is less than 625° C., and passing the hydrocarbons stream from the evaporation zone into a cracking zone of the riser-reactor to generate a cracked product in the cracking zone.

A catalytic reactor comprises a floating particle catcher unit and a particle catching surface which extracts particles from the fluid flow stream above the catalyst bed whereby at least a part of the particles settles on the particle catching surface instead of clogging the catalyst bed.

A method including a) polymerizing at least one monomer in a gas phase reactor in the presence of a supported multimodal catalyst system to form a multimodal polyethylene product having a reactor split equal to respective weight fractions of resin components in the polyethylene product; b) applying a predetermined formula for a product parameter of the multimodal polyethylene product; c) obtaining incorporation data and production rate data from the reaction based upon the predetermined formula; d) determining an actual hydrogen leading indicator; e) comparing the actual hydrogen leading indicator to a target value for a hydrogen leading indicator to determine a deviation of the actual hydrogen leading indicator from the target value; and f) adjusting an amount of a catalyst precursor being fed to the gas phase reactor to control reactor split and a product parameter.

The present disclosure relates to circulating fluidized bed apparatuses for dehydrogenation of alkanes to alkenes with higher yield and selectivity. The apparatus includes a riser-type reactor, a separator section, a regenerator and a withdrawal well disposed downstream to the regenerator. The apparatus includes a transfer line to receive hot regenerated catalyst free of oxygen from the withdrawal well, and to pre-treat the catalyst with a reducing gas to regulate-oxidation state of metals on the catalyst before reintroducing the catalyst to the riser-type reactor. The transfer line is formed in an elongated U-shaped pipe such that the oxidation state of the metals on the catalyst is regulated by the time the pre-treated catalyst reaches the bottom of the riser-type reactor.

The invention relates to an integrated process for assessing one or more properties of a catalyst. In the method, a standard chemical reactor or reactors is/are provided, and a bypass means is also provided, to transport a sample of whatever is added to the industrial reactor, to the test reactor. Both gases and liquids are transferred to the test reactor.