C01B21/0646

Method, system and injection subsystem for producing nanotubes

A floating catalyst chemical vapor deposition system produces nanotubes. The system includes a reaction chamber, a heater for heating a nanotube-material precursor and a catalyst precursor, and an injector for injecting the precursors into the chamber. In the chamber, the catalyst precursor is pyrolysed to produce catalyst particles, and the nanotube-material precursor is pyrolysed in the presence of the catalyst particles in order to produce nanotubes. A controller controls at least one operational parameter, e.g., injection temperatures of the precursors, flow rates of carrier gases of the precursors, and a reaction temperature of the chamber and of the precursors. An injection pipe extends into the chamber to an adjustable extent in order to control the injection temperature of the catalyst precursor and/or the nanotube-material precursor.

Continuous boron nitride nanotube yarns and methods of production

A method and apparatus for producing boron nitride nanotubes and continuous boron nitride nanotube yarn or tapes is provided. The apparatus includes rotating reaction tubes that allow for continuous chemical vapor deposition of boron nitride nanotubes. The rotation of the reaction tubes allows the boron nitride nanotubes to be spun into yarns or made into tapes, without post process or external rotation or spinning of the gathered nanotubes. Boron nitride nanotube yarns or tapes of great length can be produced as a result, thereby providing industry with a readily useable format for this type of material. Dopants such as carbon can be added to engineer the band gap of the nanotubes. Catalysts may be formed outside or inside the reactor.

Spherical boron nitride fine powder, method for manufacturing same and thermally conductive resin composition using same

The present invention provides a spherical boron nitride fine powder and the other superior in filling property into resin. The present invention relates to a spherical boron nitride fine powder having the following characteristics (A) to (C): (A) the spherical boron nitride fine particles have any one or more of Si, Ti, Zr, Ce, Al, Mg, Ge, Ga, and V in an amount of 0.1 atm % or more and 3.0 atm % or less in its composition on the surface of 10 nm; (B) the spherical boron nitride fine powder has an average particle diameter of 0.05 m or more and 1 m or less; and (C) the spherical boron nitride fine powder has an average circularity of 0.8 or more.

CONTINUOUS BORON NITRIDE NANOTUBE YARNS AND METHODS OF PRODUCTION

A method and apparatus for producing boron nitride nanotubes and continuous boron nitride nanotube yarn or tapes is provided. The apparatus includes rotating reaction tubes that allow for continuous chemical vapor deposition of boron nitride nanotubes. The rotation of the reaction tubes allows the boron nitride nanotubes to be spun into yarns or made into tapes, without post process or external rotation or spinning of the gathered nanotubes. Boron nitride nanotube yarns or tapes of great length can be produced as a result, thereby providing industry with a readily useable format for this type of material. Dopants such as carbon can be added to engineer the band gap of the nanotubes. Catalysts may be formed outside or inside the reactor.

BORON NITRIDE POWDER, METHOD FOR PRODUCING SAME, AND HEAT-DISSIPATING MEMBER PRODUCED USING SAME

To provide a boron nitride powder having excellent heat conductivity and high particle strength. Provided is a boron nitride powder which comprises bulky boron nitride formed such that scaly primary particles of hexagonal boron nitride are aggregated to form bulky particles, and which has the following characteristics (A) to (C): (A) a particle strength of the bulky particles at a cumulative breakdown rate of 63.2% is 5.0 MPa or more; (B) an average particle size of the boron nitride powder is 2 m or more and 20 m or less; and (C) an orientation index of the boron nitride powder as determined from X-ray diffraction is 20 or less.

BORON NITRIDE NANOTUBE (BNNT)-NANOPARTICLE COMPOSITES, METHODS FOR THE PREPARATION THEREOF AND THEIR MACROSCOPIC ASSEMBLIES

The present application relates to boron nitride nanotube (BNNT)-nanoparticle composites, to methods of preparing such composites and their use, for example, in metal/ceramic matrix composites and/or macroscopic assemblies. For example, the methods comprise subjecting a source of hydrogen, a source of boron, a source of nitrogen and a nanoparticle precursor to a stable induction thermal plasma and cooling the reaction mixture to obtain the composite.

POROUS BORON NITRIDE
20200206715 · 2020-07-02 ·

A method for producing a porous boron nitride material. The method comprises providing a mixture comprising a first nitrogen-containing organic compound, a second nitrogen-containing organic compound and a boron-containing compound. The method further comprises heating the mixture to cause thermal degradation of the mixture and form a porous boron nitride material.

HEXAGONAL BORON NITRIDE POWDER, METHOD FOR PRODUCING SAME, RESIN COMPOSITION AND RESIN SHEET
20200148537 · 2020-05-14 · ·

A hexagonal boron nitride powder having an average longer diameter (L) of primary particles in the hexagonal boron nitride powder of more than 10.0 m and 30.0 m or less, an average thickness (D) of the primary particles in the hexagonal boron nitride powder of 1.0 m or more, a ratio of the average longer diameter (L) to the average thickness (D), [L/D], of 3.0 or more and 5.0 or less, and a content of primary particles having a ratio of a longer diameter (1) to a thickness (d), [l/d], of 3.0 or more and 5.0 or less of 25% or more, a method for producing the hexagonal boron nitride powder, and a resin composition and a resin sheet each containing the hexagonal boron nitride powder.

Process for the production of two-dimensional nanomaterials

The present invention provides a process for producing a two-dimensional nanomaterial, the process comprising forming the two-dimensional nanomaterial on a surface of a substrate by CVD, wherein said surface is a liquid surface which comprises a molten eutectic compound. Substrates and substrate precursors for use in said process are also provided.

SPHERICAL BORON NITRIDE FINE POWDER, METHOD FOR MANUFACTURING SAME AND THERMALLY CONDUCTIVE RESIN COMPOSITION USING SAME
20200048091 · 2020-02-13 ·

The present invention provides a spherical boron nitride fine powder and the other superior in filling property into resin. The present invention relates to a spherical boron nitride fine powder having the following characteristics (A) to (C): (A) the spherical boron nitride fine particles have any one or more of Si, Ti, Zr, Ce, Al, Mg, Ge, Ga, and V in an amount of 0.1 atm % or more and 3.0 atm % or less in its composition on the surface of 10 nm; (B) the spherical boron nitride fine powder has an average particle diameter of 0.05 m or more and 1 m or less; and (C) the spherical boron nitride fine powder has an average circularity of 0.8 or more.