C01D1/02

A CONTINUOUS PROCESS FOR SUSTAINABLE PRODUCTION OF HYDROGEN
20210261407 · 2021-08-26 ·

The disclosure provides a method of producing hydrogen. The method comprises conducting a thermochemical reaction by contacting a metal, or an alloy thereof, with steam to produce a metal oxide and/or a metal hydroxide and hydrogen. The method then comprises contacting the metal oxide and/or the metal hydroxide produced in the thermochemical reaction with water or a basic aqueous solution to produce a solution comprising a metal ion. Finally, the method comprises conducting an electrochemical reaction by applying a voltage across an anode and a cathode, whereby at least a portion of the cathode contacts the solution comprising the metal ion, to produce hydrogen, oxygen and the metal, or the alloy thereof.

Method of preparing metal oxide-silica composite aerogel and metal oxide-silica composite aerogel prepared by using the same
10941043 · 2021-03-09 · ·

Provided are a method of preparing a metal oxide-silica composite aerogel which includes preparing a silicate solution by dissolving water glass at a concentration of 0.125 M to 3.0 M, after adding and mixing a metal salt solution having a metal ion concentration of 0.125 M to 3.0 M to the silicate solution, precipitating metal oxide-silica composite precipitates by adjusting a pH of a resulting mixture to be in a range of 3 to 9, and separating and drying the metal oxide-silica composite precipitates, wherein the metal salt solution includes a magnesium (Mg)-containing metal salt in an amount such that an amount of magnesium ions is greater than 50 mol % based on a total mole of metal ions in the metal salt solution, and a metal oxide-silica composite aerogel having low tap density and high specific surface area prepared by the method.

Method of preparing metal oxide-silica composite aerogel and metal oxide-silica composite aerogel prepared by using the same
10941043 · 2021-03-09 · ·

Provided are a method of preparing a metal oxide-silica composite aerogel which includes preparing a silicate solution by dissolving water glass at a concentration of 0.125 M to 3.0 M, after adding and mixing a metal salt solution having a metal ion concentration of 0.125 M to 3.0 M to the silicate solution, precipitating metal oxide-silica composite precipitates by adjusting a pH of a resulting mixture to be in a range of 3 to 9, and separating and drying the metal oxide-silica composite precipitates, wherein the metal salt solution includes a magnesium (Mg)-containing metal salt in an amount such that an amount of magnesium ions is greater than 50 mol % based on a total mole of metal ions in the metal salt solution, and a metal oxide-silica composite aerogel having low tap density and high specific surface area prepared by the method.

Sodium-based electrode active material and secondary battery comprising same

A sodium-based electrode active material and a secondary battery comprising the same are provided. The electrode active material is represented by the following Chemical Formula 1, and has an orthorhombic crystal system and a space group of Cmcm. [Chemical Formula 1] Na.sub.x[Mn.sub.1-y-zM.sup.1.sub.yM.sup.2.sub.z]O.sub.2-A.sub.. In Chemical Formula 1, x may be 0.5 to 0.8. M.sup.1 and M.sup.2 may be, regardless of each other, Sc, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Y, Zr, Nd, Mo, Tc, Ru, Rh, Pd, Pb, Ag, Cd, Al, Ga, In, Sn, or Bi. y may be from 0 to 0.25. z may be from 0 to 0.25. A may be N, O, F, or S, and may be 0 to 0.1.

Sodium-based electrode active material and secondary battery comprising same

A sodium-based electrode active material and a secondary battery comprising the same are provided. The electrode active material is represented by the following Chemical Formula 1, and has an orthorhombic crystal system and a space group of Cmcm. [Chemical Formula 1] Na.sub.x[Mn.sub.1-y-zM.sup.1.sub.yM.sup.2.sub.z]O.sub.2-A.sub.. In Chemical Formula 1, x may be 0.5 to 0.8. M.sup.1 and M.sup.2 may be, regardless of each other, Sc, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Y, Zr, Nd, Mo, Tc, Ru, Rh, Pd, Pb, Ag, Cd, Al, Ga, In, Sn, or Bi. y may be from 0 to 0.25. z may be from 0 to 0.25. A may be N, O, F, or S, and may be 0 to 0.1.

Process for the synthesis of IZM-2 zeolite in the presence of a template, 1,6-bis(methylpiperidinium)hexane dihydroxide

A novel process is described for the preparation of a microporous crystalline solid, known as IZM-2 microporous solid or IZM-2 zeolite. This novel process consists of carrying out the synthesis of IZM-2 zeolite by conversion/transformation of a zeolite with structure type FAU in a fluorinated medium under hydrothermal conditions. In particular, said novel process consists of carrying out the synthesis of an IZM-2 zeolite in a fluorinated medium starting from a zeolite with structure type FAU used as the source of silicon and aluminium and a specific organic molecule or template comprising two quaternary ammonium functions, namely 1,6-bis(methylpiperidinium)hexane dihydroxide.

Epoxy resin composition with soda lime glass filler

Disclosed are compositions relating to optically clear epoxy resin formulations with filler compositions having superior regular transmission of light between 350 nm and 2500 nm, and a low coefficient of thermal expansion, along with optoelectronic devices sealed with the same.

Epoxy resin composition with soda lime glass filler

Disclosed are compositions relating to optically clear epoxy resin formulations with filler compositions having superior regular transmission of light between 350 nm and 2500 nm, and a low coefficient of thermal expansion, along with optoelectronic devices sealed with the same.

NITRATE PROCESS FOR MANUFACTURING TRANSITION METAL HYDROXIDE PRECURSORS

This invention relates to an industrial process of manufacturing hydroxide precursor for lithium transition metal oxide used in secondary lithium ion batteries. More particularly, this process utilizes highly concentrated nitrate salts and is designed to mitigate waste production.

METHOD OF STABILIZING IMINO-FUNCTIONAL SILANE
20200010490 · 2020-01-09 ·

A method of stabilizing imino-functional silane involving adding thereto at least one Brnsted-Lowry base to inhibit, suppress or prevent the addition reactions of the imino-functional silane with itself to form a imino- and amino-functional silane and the subsequent deamination reactions to form conjugated carbon-carbon double bond-containing imino-functional silanes and stabilized imino-functional silanes containing the at least one Brnsted-Lowry base.