Patent classifications
C01G45/22
HEXAFLUOROMANGANATE (IV), COMPLEX FLUORIDE PHOSPHOR, AND METHODS RESPECTIVELY FOR PRODUCING SAID PRODUCTS
The present invention relates to a method for producing a hexafluoromanganate(IV), said method being characterized by comprising: inserting an anode and a cathode into a reaction solution that contains a compound containing manganese having an atomic valence of less than 4 and/or manganese having an atomic valence of more than 4 and hydrogen fluoride; and then applying an electric current having an electric current density of 100 to 1000 A/m.sup.2 between the anode and the cathode. According to the present invention, it becomes possible to produce a hexafluoromanganate(IV) in which the content ratio of manganese having an atomic valence of 4 is high and the contamination with oxygen is reduced and which has high purity. When a complex fluoride red phosphor is produced using the hexafluoromanganate(IV) as a raw material, the phosphor produced has high luminescence properties, particularly high internal quantum efficiency.
POSITIVE ELECTRODE ACTIVE MATERIAL PRECURSOR, POSITIVE ELECTRODE ACTIVE MATERIAL, PREPARATION METHOD, AND SECONDARY BATTERY
A preparation method includes the following steps: S1, preparing an aqueous solution of a metal salt and an aqueous solution of a precipitant, where the precipitant includes one or more selected from oxalic acid and a water-soluble oxalate; S2, mixing the aqueous solution of the precipitant and the aqueous solution of the metal salt at a shear speed of 10000 r/min or more for co-precipitation reaction; and S3, after the reaction is completed, obtaining the positive electrode active material precursor via washing and drying.
POSITIVE ELECTRODE ACTIVE MATERIAL PRECURSOR, POSITIVE ELECTRODE ACTIVE MATERIAL, PREPARATION METHOD, AND SECONDARY BATTERY
A preparation method includes the following steps: S1, preparing an aqueous solution of a metal salt and an aqueous solution of a precipitant, where the precipitant includes one or more selected from oxalic acid and a water-soluble oxalate; S2, mixing the aqueous solution of the precipitant and the aqueous solution of the metal salt at a shear speed of 10000 r/min or more for co-precipitation reaction; and S3, after the reaction is completed, obtaining the positive electrode active material precursor via washing and drying.
ALKALI METAL METALATE COMPOUNDS WITH MAGNETIC EXCHANGE BIAS AND IONIC CONDUCTIVITY PROPERTIES
Please cancel the abstract of this application and replace it with the following amended abstract presented in clean form according to the procedures outlines in MPEP 714(II)(B): It is provided an alkali metal metalate compound with high magnetic exchange bias and ionic conductivity properties having the general formulae (I) A.sub.2[M.sup.1.sub.3-x M.sup.2.sub.x Z.sub.4] with A being one of Li, Na, K; M.sup.1, M.sup.2 being one or more of Cr, Mn, Fe, Co, Ni, Cu, Zn; Z being S or Se; x being 0-3, preferably 0, 0.01, 0.1, 0.5, 1, 1.5, 2, 3; whereby the compounds K.sub.2[Ni.sub.3S.sub.4], K.sub.2[Zn.sub.3S.sub.4], K.sub.2[Mn.sub.3S.sub.4], Na.sub.2[Mn.sub.3Se.sub.4] and K.sub.2[Ni.sub.3Se.sub.4] are exempted.
Process for the preparation of nanocrystalline metal oxides
The present invention relates to a process for the preparation of nanocrystalline metal oxide particles comprising the steps of a) the introduction of a starting compound into a reaction chamber by means of a carrier fluid, b) the subjecting of the starting compound in a treatment zone to a pulsating thermal treatment, c) the forming of nanocrystalline metal oxide particles, d) the removal of the nanocrystalline metal oxide particles obtained in steps b) and c) from the reactor, wherein the starting compound is introduced into the reaction chamber in the form of a solution, slurry, suspension or in solid aggregate state. Further, the present compound relates to a catalyst material, obtainable by the process according to the invention, in particular a catalyst material for use in the preparation of methanol from carbon monoxide and hydrogen.
Lithium-manganese rich material, preparation method therefor and use thereof
The present disclosure discloses a lithium-manganese rich material and a preparation method and a use thereof.
DISORDERED ROCKSALT MATERIAL AND METHOD OF FORMING IT
A disordered rocksalt (DRS) having improved characteristic has a cation comprised of lithium and one other metal and an anion comprised of oxygen and fluorine, and one or more of phosphorous, sulfur, and nitrogen. The substitution of one or more of P, S, and N on the oxygen anion site may realize improved cycle life of the battery and/or may be useful to make safer batteries.
DISORDERED ROCKSALT MATERIAL AND METHOD OF FORMING IT
A disordered rocksalt (DRS) having improved characteristic has a cation comprised of lithium and one other metal and an anion comprised of oxygen and fluorine, and one or more of phosphorous, sulfur, and nitrogen. The substitution of one or more of P, S, and N on the oxygen anion site may realize improved cycle life of the battery and/or may be useful to make safer batteries.
Process for making precursors for cathode active materials, precursors, and cathode active materials
Process for making a manganese composite (oxy)hydroxide with a mean particle diameter D50 in the range from 2 to 16 m comprising the step(s) of combining (a) an aqueous solution containing salts of nickel and of manganese, and, optionally, at least one of Al, Mg, or transition metals other than nickel and manganese wherein at least 50 mole-% of the metal is manganese, (b) with an aqueous solution of an alkali metal hydroxide and (c) an organic acid or its alkali or ammonium salt wherein said organic acid bears at least two functional groups per molecule and at least one of the functional groups is a carboxylate group.
Process for making precursors for cathode active materials, precursors, and cathode active materials
Process for making a manganese composite (oxy)hydroxide with a mean particle diameter D50 in the range from 2 to 16 m comprising the step(s) of combining (a) an aqueous solution containing salts of nickel and of manganese, and, optionally, at least one of Al, Mg, or transition metals other than nickel and manganese wherein at least 50 mole-% of the metal is manganese, (b) with an aqueous solution of an alkali metal hydroxide and (c) an organic acid or its alkali or ammonium salt wherein said organic acid bears at least two functional groups per molecule and at least one of the functional groups is a carboxylate group.