This invention relates to a process for determining the suitability of pyrolysis tar, such as steam cracker tar, for upgrading using hydroprocessing without excessive fouling of the hydroprocessing reactor. A pyrolysis tar is sampled, the sample is analyzed to determine one or more characteristics of the tar related to tar reactivity, and the analysis is used to determine conditions under which the tar can be blended, pre-treated, and/or hydroprocessed.

A process for producing isotropic and mesophase pitch with reduced solids contamination from aromatic liquids contaminated with solids, such as catalyst fines or semi-coke. Contaminated feed is charged through one or more pitch forming reactors which discharge a pitch rich liquid and a vapor phase with reduced solids contamination. The vapor phase is cooled, condensed and may be charged continuously to another pitch forming reactor in parallel or used intermittently as a total or partial replacement for solids contaminated feed.

A method of producing biofuels, based on pyrolysis of biomass from macrophytes, includes: pre-treatment of biomass, including processes of drying and crushing the biomass, followed by injection of pre-treated biomass into a pyrolysis reactor; biomass pyrolysis in pyrolysis reactor; a first separation of products; a second separation of products; a third separation of products; burning or collecting gases, wherein the method produces at least four different types of products, including: biochar, pyroligneous extract, vegetable tar and synthesis gas; whereby, the biochar product is collected in the first product separation through the use of a cyclone, the pyroligneous extract product is collected in the second product separation through the use of a condenser, the vegetable tar product is collected in the third product separation through the use of a centrifuge, and the synthesis gas product is collected in the gas burning or collecting step.

A method of producing biofuels, based on pyrolysis of biomass from macrophytes, includes: pre-treatment of biomass, including processes of drying and crushing the biomass, followed by injection of pre-treated biomass into a pyrolysis reactor; biomass pyrolysis in pyrolysis reactor; a first separation of products; a second separation of products; a third separation of products; burning or collecting gases, wherein the method produces at least four different types of products, including: biochar, pyroligneous extract, vegetable tar and synthesis gas; whereby, the biochar product is collected in the first product separation through the use of a cyclone, the pyroligneous extract product is collected in the second product separation through the use of a condenser, the vegetable tar product is collected in the third product separation through the use of a centrifuge, and the synthesis gas product is collected in the gas burning or collecting step.

This invention relates to a process for determining the suitability of pyrolysis tar, such as steam cracker tar, for upgrading using hydroprocessing without excessive fouling of the hydroprocessing reactor. A pyrolysis tar is sampled, the sample is analyzed to determine one or more characteristics of the tar related to tar reactivity, and the analysis is used to determine conditions under which the tar can be blended, pre-treated, and/or hydroprocessed.

This invention relates to a process for determining the suitability of pyrolysis tar, such as steam cracker tar, for upgrading using hydroprocessing without excessive fouling of the hydroprocessing reactor. A pyrolysis tar is sampled, the sample is analyzed to determine one or more characteristics of the tar related to tar reactivity, and the analysis is used to determine conditions under which the tar can be blended, pre-treated, and/or hydroprocessed.

A method for forming mesophase pitch can include applying a stimulus to a first amount of coal tar to form a first amount of mesophase pitch. The stimulus can include one or more of an electromagnetic field (“EMF”) or a magnetic field. The method can further include evaluating a characteristic of the first amount of mesophase pitch, changing a parameter of the stimulus in response to evaluating the characteristic of the first amount of mesophase pitch, and applying the stimulus exhibiting the changed parameters to a second amount of coal tar to form mesophase pitch.

Pitch production systems utilizing coal tar or decant oil for coal. or petroleum based pitch are disclosed. Total pitch production yields are increased by heat treating distillate fractions from the pitch production process. A heat treatment system and process are disclosed in embodiments. The heaviest distillates having the highest molecular weights are subjected to heat treatment, though other embodiments contemplate heat treating a variety of combined distillate fractions. The heat treatment systems require heat soaking the distillate(s) at elevated temperatures of 459-535 C. at a near-constant temperature with near-uniform flow. A fraction of the heat-treated distillate may be reintroduced to the pitch production system as part of a continuous process.

An asphalt processing system is formed from a heating drum and an induction heating system. Flights move asphalt through the heating drum, which concurrently heat the asphalt along with the heating drum wall. A mixing drum can be connected to the heating drum, and include paddles or flights to move the asphalt, while concurrently mixing the material to ensure consistent temperatures through the asphalt cement. The asphalt is heating using one or more induction heating systems to quickly heat the asphalt to between 275 F. and 750 F., followed by moving the asphalt to between 275 F. and 350 F. The system can include a convection system that heats recirculated air through the heating drum. A water condenser can be employed to remove moisture during air recirculation, and reduce asphalt moisture content. The asphalt cement is optionally modified by addition of one or more rejuvenation oils. This system is particularly useful for recycled asphalt pavement, but can be used for all asphalt products.

An asphalt processing system is formed from a heating drum and an induction heating system. Flights move asphalt through the heating drum, which concurrently heat the asphalt along with the heating drum wall. A mixing drum can be connected to the heating drum, and include paddles or flights to move the asphalt, while concurrently mixing the material to ensure consistent temperatures through the asphalt cement. The asphalt is heating using one or more induction heating systems to quickly heat the asphalt to between 275 F. and 750 F., followed by moving the asphalt to between 275 F. and 350 F. The system can include a convection system that heats recirculated air through the heating drum. A water condenser can be employed to remove moisture during air recirculation, and reduce asphalt moisture content. The asphalt cement is optionally modified by addition of one or more rejuvenation oils. This system is particularly useful for recycled asphalt pavement, but can be used for all asphalt products.