An operation method of a copper-smelting furnace is characterized by including supplying an Fe metal source into a copper-smelting furnace together with a feeding material including copper concentrate and a flux, the copper concentrate including Al, the Fe metal source including an Fe metal of 40 mass % to 100 mass %.

The invention provides a method for the recovery of a metal-containing product (M.sub.Prod) comprising: providing a composite material comprising a matrix of oxidised reductant (R.sub.o), a product metal (M.sub.P) dispersed in the matrix of oxidised reductant (R.sub.o), and one or more metal compounds (M.sub.PC.sub.R) of the product metal (M.sub.P) in one or more oxidation states dispersed in the matrix of oxidised reductant (R.sub.o); and treating the composite material to at least partially remove the one or more metal compounds (M.sub.PC.sub.R) from the matrix of oxidised reductant (Ro) to form the metal-containing product (M.sub.Prod).

The invention provides a method for the recovery of a metal-containing product (M.sub.Prod) comprising: providing a composite material comprising a matrix of oxidised reductant (R.sub.o), a product metal (M.sub.P) dispersed in the matrix of oxidised reductant (R.sub.o), and one or more metal compounds (M.sub.PC.sub.R) of the product metal (M.sub.P) in one or more oxidation states dispersed in the matrix of oxidised reductant (R.sub.o); and treating the composite material to at least partially remove the one or more metal compounds (M.sub.PC.sub.R) from the matrix of oxidised reductant (Ro) to form the metal-containing product (M.sub.Prod).

A calcium, aluminum, and silicon alloy is provided. The alloy includes about 15 to 45% calcium, 20 to 40% aluminum, and 20 to 40% silicon.

A calcium, aluminum, and silicon alloy is provided. The alloy includes about 15 to 45% calcium, 20 to 40% aluminum, and 20 to 40% silicon.

A method of producing a composite material comprising: supplying a metal compound (M.sub.PC) of a product metal (M.sub.P) and a reductant (R) capable of reducing the metal compound (M.sub.PC) of the product metal (MP) to a reactor; forming a composite material comprising a matrix of oxidised reductant (R.sub.0) of the reductant (R), the product metal (M.sub.P) dispersed in the matrix of oxidised reductant (R.sub.0), and at least one of (i) one or more metal compounds (M.sub.PC.sub.R) of the metal compound (M.sub.PC) in one or more oxidation states and (ii) the reductant (R); and recovering the composite material from the reactor, wherein the metal compound (M.sub.PC) of the product metal (M.sub.P) is fed to the reactor such that it is in excess relative to the reductant (R).

A method of producing a composite material comprising: supplying a metal compound (M.sub.PC) of a product metal (M.sub.P) and a reductant (R) capable of reducing the metal compound (M.sub.PC) of the product metal (MP) to a reactor; forming a composite material comprising a matrix of oxidised reductant (R.sub.0) of the reductant (R), the product metal (M.sub.P) dispersed in the matrix of oxidised reductant (R.sub.0), and at least one of (i) one or more metal compounds (M.sub.PC.sub.R) of the metal compound (M.sub.PC) in one or more oxidation states and (ii) the reductant (R); and recovering the composite material from the reactor, wherein the metal compound (M.sub.PC) of the product metal (M.sub.P) is fed to the reactor such that it is in excess relative to the reductant (R).

The invention relates to a method for preparing high-melting-point metal powder through multi-stage deep reduction, and belongs to the technical field of preparation of powder. The method includes the following steps of mixing dried high-melting-point metal oxide powder with magnesium powder and performing a self-propagating reaction, placing an intermediate product into a closed reaction kettle, leaching the intermediate product with hydrochloric acid as a leaching solution so as to obtain a low-valence oxide Me.sub.xO precursor of the low-valence high-melting-point metal; uniformly mixing the precursor with calcium powder, pressing the mixture, placing the pressed mixture into a vacuum reduction furnace, heating the vacuum reduction furnace to 700-1200° C., performing deep reduction for 1-6 h, leaching a deep reduction product with hydrochloric acid as a leaching solution and performing treatment, so as to obtain the high-melting-point metal powder.

A method for preparing a high-purity metal lithium by a vacuum thermal reduction method includes the following steps: obtaining Li.sub.2O.(2-x)CaO by carrying a vacuum thermal decomposition process on a lithium-containing raw material in the presence of a refractory agent and a catalyst; mixing the obtained oxide with the fluxing agent, the catalyst and a reducing agent according to a certain ratio, and then briquetting; carrying out vacuum thermal reduction in a vacuum reduction furnace, and performing centrifugal sedimentation and micron ceramic dust removal on lithium vapor obtained by the thermal reduction to obtain a high-purity metal gas; and removing metal impurities from the gas by controlling a condensation temperature and a condensation speed of the gas so as to purify the lithium vapor, and obtaining a high-purity metal lithium with a rapid cooling technology.

A method for preparing a high-purity metal lithium by a vacuum thermal reduction method includes the following steps: obtaining Li.sub.2O.(2-x)CaO by carrying a vacuum thermal decomposition process on a lithium-containing raw material in the presence of a refractory agent and a catalyst; mixing the obtained oxide with the fluxing agent, the catalyst and a reducing agent according to a certain ratio, and then briquetting; carrying out vacuum thermal reduction in a vacuum reduction furnace, and performing centrifugal sedimentation and micron ceramic dust removal on lithium vapor obtained by the thermal reduction to obtain a high-purity metal gas; and removing metal impurities from the gas by controlling a condensation temperature and a condensation speed of the gas so as to purify the lithium vapor, and obtaining a high-purity metal lithium with a rapid cooling technology.