A method of manufacturing an elastic polymer aerogel material includes dissolving tire waste, the tire waste including natural rubber, synthetic polymers, steel, fillers, and curing systems, in a solvent to form a first mixture and dissolving a polymer having at least one double carbon-carbon bond in the solvent to form a second mixture. The first mixture and the second mixture are combined, wherein the tire waste reacts with the polymer having at least one double carbon-carbon bond to form a reactant gel. The reactant gel undergoes a solvent exchange followed by freeze drying to form the elastic polymer aerogel material, wherein the elastic polymer aerogel material defines a 3D porous structure.

A method of manufacturing an elastic polymer aerogel material includes dissolving tire waste, the tire waste including natural rubber, synthetic polymers, steel, fillers, and curing systems, in a solvent to form a first mixture and dissolving a polymer having at least one double carbon-carbon bond in the solvent to form a second mixture. The first mixture and the second mixture are combined, wherein the tire waste reacts with the polymer having at least one double carbon-carbon bond to form a reactant gel. The reactant gel undergoes a solvent exchange followed by freeze drying to form the elastic polymer aerogel material, wherein the elastic polymer aerogel material defines a 3D porous structure.

A functionally gradient material for guided periodontal hard and soft tissue regeneration includes a 3D printed scaffold layer and an electrospun fibrous membrane layer. The content of hydroxyapatite in the 3D printed scaffold layer is higher than the content of hydroxyapatite in the electrospun fibrous membrane layer. The pore size of the 3D printed scaffold layer is larger than the pore size of the electrospun fibrous membrane layer. The pore size of the 3D printed scaffold layer is 100-1000 μm, and the fiber diameter of the electrospun fibrous membrane layer is 300-5000 nm. The electrospun fibrous membrane layer is in a random distribution or an oriented arrangement or has a mesh structure. The thickness of the electrospun fibrous membrane layer is 0.08-1 mm.

A functionally gradient material for guided periodontal hard and soft tissue regeneration includes a 3D printed scaffold layer and an electrospun fibrous membrane layer. The content of hydroxyapatite in the 3D printed scaffold layer is higher than the content of hydroxyapatite in the electrospun fibrous membrane layer. The pore size of the 3D printed scaffold layer is larger than the pore size of the electrospun fibrous membrane layer. The pore size of the 3D printed scaffold layer is 100-1000 μm, and the fiber diameter of the electrospun fibrous membrane layer is 300-5000 nm. The electrospun fibrous membrane layer is in a random distribution or an oriented arrangement or has a mesh structure. The thickness of the electrospun fibrous membrane layer is 0.08-1 mm.

The present invention relates to electrospun fibers comprising i) a hydrophilic polymer that is soluble in a first solvent, ii) a bioadhesive substance that is slightly soluble in said first solvent, iii) optionally, a drug substance.

The invention relates to non-woven protein fibers and to methods for forming and producing the same. In certain embodiments, the invention provides a method of processing a protein comprising dissolving a protein in a solution, optionally removing any insoluble materials from the solution, and spraying the solution under an applied pressure. In other embodiments, the protein can be derived from a range of sources, including but not limited to arthropod silks, animal keratin (e.g. hair and wool), tissue elastin, collagen, resilin, and plant protein. In certain embodiments, the methods of the invention are an alternative to electrospinning methods known in the art.

MXene fibers and a preparation method thereof are provided. The method for preparation of a MXene fiber comprises preparing a dope solution in which MXene sheets are dispersed in a polar solvent, extruding the dope solution into a coagulating solution to coagulate the extruded dope solution to change into a MXene gel fiber, and drying the MXene gel fiber and converting it into the MXene fiber.

The present invention provides nanometer-sized fibers that are produced by an electrospinning method with use of a spinning solution for electrospinning, said spinning solution being environmentally friendly and taking the effects of an organic solvent on the human body into consideration. The fibers are formed from a resin that contains a silicone-modified polyurethane resin which is a reaction product of (A) a polyol, (B) a water dispersant, (C) an active hydrogen group-containing organopolysiloxane represented by formula (1)

R.sup.1R.sup.2R.sup.3SiO(SiR.sup.2R.sup.3O).sub.nSiR.sup.1R.sup.2R.sup.3  (1)

(wherein R.sup.1 represents a monovalent hydrocarbon group which may have an oxygen atom in the chain, while having from 1 to 10 carbon atoms and a hydroxyl group or a mercapto group, or a monovalent hydrocarbon group which has a primary amino group or a secondary amino group, while having from 1 to 10 carbon atoms; each of R.sup.2 and R.sup.3 represents a group that is selected from among an alkyl group having from 1 to 10 carbon atoms, an aralkyl group having from 7 to 10 carbon atoms, an aryl group having from 6 to 12 carbon atoms and a vinyl group; and n represents an integer from 1 to 200), and (D) a polyisocyanate.

Natural polymer-based fibrous elements including a modified polymer derived from a natural polymer and a surfactant, method for making such natural polymer-based fibrous elements and methods for making such fibrous structures are provided.

Provided herein are high throughput continuous or semi-continuous reactors and processes for manufacturing expanded graphite materials. Such processes are suitable for manufacturing expanded graphite materials with little batch-to-batch variation.