Used Oil Recycling Filtration Assembly
20170232394 · 2017-08-17
Inventors
Cpc classification
B01D2311/06
PERFORMING OPERATIONS; TRANSPORTING
B01D2311/04
PERFORMING OPERATIONS; TRANSPORTING
B01D2311/04
PERFORMING OPERATIONS; TRANSPORTING
B01D2311/2642
PERFORMING OPERATIONS; TRANSPORTING
B01D2313/08
PERFORMING OPERATIONS; TRANSPORTING
B01D2311/2642
PERFORMING OPERATIONS; TRANSPORTING
B01D2311/06
PERFORMING OPERATIONS; TRANSPORTING
International classification
Abstract
A filtration system suitable for recovering base stock from used lubricating oil and other applications pass feedstock over nano-filtration membranes assembled as a stack of membranes all experiencing parallel flow. On exiting a first stack of membranes the feedstock passes through an opening in a pressure-sustaining separator plate to flow in the reverse direction past a second stack of membranes and subsequently establish a serpentine flow of feedstock through multiple stacks of membranes. The stacks of membranes all share a common pressure containment vessel. Pressure boosters installed in the flow-through openings of separator plates separating consecutive stacks can serve to restore lost pressure of the feedstock and maintain effective permeation of permeate through the membranes. A pressure control valve at the outlet to the permeate-receiving cavities of a stack can be used to adjust the trans-membrane pressure.
Claims
1-19. (canceled)
20. A filtration system to produce a permeate from a liquid feedstock comprising multiple permeable membrane support panels assemblies assembled in stacks, each membrane panel assembly carrying respective permeable filter membranes, each membrane panel assembly having a receiving space within to serve as a permeate-receiving cavity for accepting permeate driven through the membranes by pressure applied to the feedstock and a permeate-receiving cavity outlet to drain-off permeate, wherein a) the multiple membrane panels assemblies are mounted in a common pressure-containment vessel, such vessel having walls, a feedstock inlet and outlets for permeate and concentrate, and b) the pressure containment vessel contains at least one pressure-sustaining separator plate positioned between at least two otherwise adjacent stacks of membrane panel-assemblies, the separator plate having a flow-through opening at one end only to allow liquid to flow from one stack of membrane panels assemblies to the next and wherein the at least one separator plate: i) is positioned between the two otherwise adjacent stacks of membrane panels assemblies with its outer periphery serving as part of the walls of the pressure containment vessel, ii) provides a separator permeate inlet connected through a manifold to the permeate-receiving cavity outlets of at least one of the two stacks of otherwise adjacent membrane panels assemblies to receive permeate therefrom, and iii) comprises a passageway positioned along the periphery of the separator plate to convey permeate outside the pressure containment vessel through a separator permeate outlet.
21. A filtration system as in claim 20 comprising respective frames within which each membrane panel assembly is mounted, the frames each having outer peripheries that serve, when the membrane panel supports are combined to form stacks, as part of the walls of the pressure containment vessel, wherein the frames of the at least one of the two otherwise adjacent stacks of membrane panels assemblies comprise tabs that provide the manifold liar delivery of permeate to the separator permeate inlet.
22. A filtration system as in claim 21 wherein the separator permeate outlet is connected to deliver permeate to a back-pressure control valve having an associated pressure sensor and valve control system for establishing the pressure within the permeate-receiving cavity.
23. A filtration system to produce a permeate from a liquid feedstock comprising multiple permeable membrane support panels assemblies assembled in stacks, each membrane panel assembly carrying respective permeable filter membranes, each membrane panel assembly having a permeate-receiving cavity within to serve as a cavity for accepting permeate driven through the membranes by pressure applied to the feedstock and a permeate-receiving cavity outlet to drain-off permeate, wherein: a) the stacks of multiple membrane panels assemblies are mounted in a common pressure-containment vessel, such vessel having walls, a feedstock inlet and outlets for permeate and concentrate, and b) the pressure containment vessel contains at least one pressure-sustaining separator plate positioned between at least two otherwise adjacent stacks of membrane support panels, the separator plate having a flow-through opening at one end only to allow liquid to flow from one stack of membrane support panels assemblies to the next, and wherein the permeate-receiving cavity outlets of the membrane panels assemblies are connected to deliver permeate to a back-pressure control valve having an associated pressure sensor and valve control system for establishing the pressure within the permeate-receiving cavities.
24. The filtration system as in claim 23 wherein: a) the membrane panels assemblies comprise two permeable panels mounted back-to-back with two respective membranes located on their outer-facing surfaces, and b) the two panels define between them the receiving space there within to serve as the permeate-receiving cavity for accepting permeate driven through the two membranes by pressure applied to the feedstock, thereby constituting the “panel assemblies”, and wherein, between the at least one pressure sustaining separator plate, groups of membrane panel assemblies are arrayed in a parallel configuration so that feedstock will flow in the same direction on both sides of the panel assemblies within the group, collectively the membrane panel assemblies in a group constituting the “stack” of membrane panel assemblies separated by the separator plate.
25. A filtration system to produce a permeate from a liquid feedstock comprising multiple permeable filter membrane support panels wherein: a) the support panels comprise two permeable panels mounted back-to-back with two respective filter membranes located on their outer-facing surfaces, b) the two panels define between them a receiving space there within to serve as a permeate-receiving cavity for accepting permeate driven through the two membranes by pressure applied to the feedstock, and c) each permeate-receiving cavity is provided with a permeate-receiving cavity outlet to drain-off permeate, thereby constituting “panel assemblies”, the panel assemblies being combined into at least two stacks of such panels assemblies wherein: d) the at least two stacks of panels assemblies are mounted in a common pressure-containment vessel, such vessel having walls, a feedstock inlet and outlets for permeate and concentrate, e) the pressure containment vessel contains at least one pressure-sustaining separator plate positioned between at least two otherwise adjacent stacks of panels assemblies, the separator plate having a flow-through opening at one end only to allow liquid to flow from one stack of panels assemblies to the next, and f) a pressure booster is mounted in the at least one separator plate flow-through opening to restore lost pressure between consecutive stacks of panel assemblies.
26. A filter system as in claim 25 wherein the pressure containment vessel comprises at least three pressure-sustaining separator plates and pressure boosters are respectively mounted in the flow-through openings in every other separator plate.
27. A filter system as in claim 26 comprising pressure boosters respectively mounted in the flow-through openings in every separator plate.
28. A filter system as in claim 25 wherein the pressure booster is actuated by an electric motor.
29. A filter system as in claim 26 wherein the pressure boosters are actuated by respective electric motors.
30. A filter system as in claim 27 wherein the pressure boosters are actuated by respective electric motors.
31. A filter system as in claim 25 wherein the pressure booster is actuated by a rotating shaft driven from outside the pressure vessel.
32. A filtration system as in claim 26 wherein the pressure boosters are actuated by a common rotating shaft driven from outside the pressure vessel.
33. A filtration system as in claim 27 wherein the pressure boosters are actuated by a common rotating shall driven from outside the pressure vessel.
34. A filtration system as in claim 32 wherein the common shaft penetrates every other intervening separator plate through a pressure seal.
35. A filtration system as in claim 25 comprising respective frames within which each membrane support panel assembly is mounted, the peripheries of the frames, when the membrane panel assemblies are combined to form stacks, serving as part of the walls of the pressure containment vessel, wherein the frames comprise tabs assembled to provide a manifold connected to the permeate outlets of the permeate receiving cavities of each panel assembly for collection of permeate from each stack for delivery to an external storage vessel.
36. A filtration system as in claim 35 wherein the separator plates interspersed between the stacks of panels are respectively provided with conduits connected to the manifolds of the respective stacks to receive and convey permeate out of the pressure containment vessel.
37. A filtration system as in claim 25 wherein the permeate-receiving cavity outlets of each panel assembly in a stack are connected to a stack manifold that is connected to deliver permeate to a back-pressure control valve having an associated pressure sensor and valve control system for establishing the pressure within the permeate-receiving cavity.
38. A filtration system as in claim 25 wherein the permeate-receiving cavity outlets of each panel assembly in a stack are connected to a stack manifold that is connected through a passageway positioned along, the periphery of the separator plate at the end of the stack to deliver permeate to a hack-pressure control valve having an associated pressure sensor and valve control system for establishing the pressure within the permeate-receiving cavity.
Description
SUMMARY OF THE FIGURES
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DESCRIPTION OF THE PREFERRED EMBODIMENTS
[0065] In
[0066] The cavity 26 may contain a permeable cavity propping structure 61 (shown in
[0067] Membranes suitable for use with the invention in a used lubricating oil application are believed to be available from:
[0068] Koch Membrane Systems, Inc.
850 Main Street
Wilmington, Mass.
[0069] 01887-3388
USA
[0070] EMD Millipore Corporation
290 Concord Road
Billerica
Mass. 01821
United States of America
[0071] U.S. Pat. No. 4,818,088 also describes a nano-membrane for use with aliphatic hydrocarbon liquids suitable for incorporation into the invention described herein in such application.
[0072] System Layout
[0073] In
[0074] Feedstock 11 enters the containment vessel 35 bounded by end plates 38 at an inlet 13. This inlet 13 is fitted with an inlet diffuser 42 to distribute the flow amongst the membrane panel assemblies 41 within the containment vessel 35. Initially the hot feedstock 11 heats the apparatus while being circulated at low speed. Then the circulation rate and pressure within the loop 33 can be increased to process the feedstock 11 more rapidly.
[0075] The containment vessel 35 includes a series of individual membrane panel assemblies 41 (depicted schematically as lines 41 in
[0076] At the outlet collector 42 partially concentrated feedstock 11A exits from containment 35 to flow around the loop 33. Eventually a loop outlet pump 43 extracts more fully depleted concentrate 15 from the loop 33 through a back-pressure control valve 43 for delivery to a processed-concentrate holding tank 44.
[0077] As shown in
[0078] As best shown in
[0079] In
[0080] Permeate conduits 58 can run adjacent to the inner portion of the frame 52 to carry permeate 25 to the ends of the membrane panel assemblies 41.
[0081] In
[0082] Individual panel assemblies 41 have passageway openings 50, also shown in plan view in
[0083] The height of the headspace provided by the gaps 53 has an important effect on the operation of the system. As this headspace 53 gets narrower, the pressure drop along a given length of membrane 20 will increase. If higher feedstock pressures are used, then, for a given gap height 53, the feedstock 11 flow rate will be higher. This flow rate will help “scrub” non-passing feedstock matter off the surface of the membrane 20, reducing membrane blockage. At the same time, such over-pressure can affect “concentration polarization” on the surface of the membrane. This has the consequence of thickening the boundary layer of fluid flow over the membrane, which will reduce permeate flow. For this reason trans-membrane pressure should not be allowed to become excessive.
[0084]
[0085] In
[0086] Serpentine Flow
[0087] In
[0088] In
[0089] Pressure Boost
[0090] In
[0091] The shaft 64 is turned through a transmission 67 by an external electric motor 66. Thus, as the feedstock 11 passes from stack 45 to stack 45 in the bank of stacks, its pressure is boosted, making-up for the pressure loss incurred by flowing in a cross-flow over the surface of the membranes 20. The motor 66 may be a variable speed motor to control the amount of the pressure boost. Although a common shaft 64 is shown as actuating the pressure boosters 65, each pressure booster 65 could have its own individual electric motor.
[0092] As depicted in some of the Figures so far for the individual membrane support panel assemblies 41 and separator plates 46, reference has been made to an opening, (in the form of a passageway 50 (in
[0093] In
[0094] In configurations where the pressure drop within the flow of feedstock 11 is significant, e.g. the length of cross-flow along the membranes 20 in one or more stacks 45 is considerably extended or the feedstock 11 is viscous as in the case of heavy oil, a second set of pressure boosters 65 may be installed at the other end of the separator plate 46. Thus further multiple impellers 65 may be positioned at the top of the second, fourth and all even numbered separator plates 46. In this separate array of pressure boosters 65, all odd numbered separator plates 46 would have appropriately aligned pressure-tight bearings 69. This second shaft, or set of shafts, would have its own drive mechanism 66, 67 and speed control. For such long panels, the unit could beneficially be positioned on its side.
[0095] Trans-Membrane Pressure Control
[0096] To dispose of permeate 25 each stack 45 is provided with a first permeate outlet manifold 27A (in
[0097] By providing each back-pressure valve 71 (in
[0098] Drain tabs 93 (in
[0099] The permeate back-pressure control system as described is suitable for providing a preferred trans-membrane pressure when feedstock 11 is delivered to the containment vessel inlet 13 at a significantly elevated inlet pressure level 12. The consecutive pressure-boosting provisions for the individual consecutive stacks 45 described previously as part of this invention can obviate the need to deliver feedstock 11 to the container inlet 13 at an elevated inlet pressure 12. Nevertheless, in order to maintain trans-membrane pressures at reasonable values in either such cases, the permeate back-pressure control system as described can be used to set or fine-tune the trans-membrane pressure for individual stacks by adjusting the pressure of the associated membrane collection cavities 26.
[0100] Hybrid Separator Plate
[0101] The separator plate 46 need not be an independent component.
[0102] In this variant the lightly built perforated metal panel 47 is supported and stiffened by the pressure-sustaining modified separation plate 46A providing effectively a stiffened membrane panel support assembly 41 with a separator plate 46 embedded therein. If desired the modified separator plate 46A may also be perforated although this may prove costly for a thickened plate.
[0103] Number of Panels in Each Stack
[0104] As the feedstock 11 passes through a series of stacks 45, its pressure will be progressively reduced. At the same time, a portion of its volume will be carried-away in the permeate 25 that passes through the membranes 20. This loss of volume, after a number of stacks 45 have been passed-through will reduce the rate of feedstock 11 flow across membrane 20 surfaces.
[0105] To maintain the cross-flow fluid velocity at a desired level, the number of membrane support panels 41 in later stacks 45 in the series can be reduced. Thus, for example, where the initial stack count includes twenty membrane panels, then after, say, ten stacks in the series, the twenty first stack may have its panel count reduced to nineteen. This process can be repeated if the number of stacks in the series is extended substantially. The values in the example given will vary with the viscosity of the feedstock 11, the length of panel assemblies 41, the number of stacks in the system and other parameters.
[0106] Mounting of Membrane Support Panels
[0107] When finally assembled, the membrane support panels 41 and separator plates 46 which provide a portion of the boundaries of the pressure containment vessel 35 are held rigidly in place by the compressive force of the end plates 38 that are drawn towards each other by tightening the peripheral arrangement of bolts 56. This compressive force is high and the integrity of the arrangement once assembled is secure.
[0108] During initial assembly, temporary rails may be provided between the two end plates 38 to align individual panels being positioned there between in respect of their vertical position. Spacers located alongside side bolts 56 can ensure proper alignment in the horizontal direction.
[0109] In most applications where a pure base stock is required for producing fresh lubricating oil, the permeate 25 may be subject to a final treatment by passing it through a commercially available Polishing Unit that relies on activated clays. It is not represented that the output from the filtration system as describe is absolutely ready for use as a base stock for preparing lubricating oil.
[0110] While the above description has focused on an apparatus for recovering base lube oil stock from used lubricating oil, the invention and the apparatus hereinafter claimed is equally applicable to any suitable liquid filtration process that relies on a membrane as the filtering medium.
CONCLUSION
[0111] The foregoing has constituted a description of specific embodiments showing how the invention may be applied and put into use. These embodiments are only exemplary. The invention in its broadest, and more specific aspects, is further described and defined in the claims which now follow.
[0112] These claims, and the language used therein, are to be understood in terms of the variants of the invention which have been described. They are not to be restricted to such variants, but are to be read as covering the full scope of the invention as is implicit within the invention and the disclosure that has been provided herein.