Electron microscope and method of operating the same
09772976 · 2017-09-26
Assignee
Inventors
Cpc classification
H01J37/285
ELECTRICITY
H01J2237/24507
ELECTRICITY
G06F17/18
PHYSICS
International classification
G06F17/18
PHYSICS
Abstract
An electron microscope and method of operating an electron microscope (1) has an electron beam source (11) for producing an electron beam, a noise canceling aperture (12) for detecting a part of the beam, an amplifier (42), an effective value calculating circuit (44) for extracting DC components of the output signal from the amplifier (42), a detector (15) for detecting a signal obtained in response to impingement of the beam on a sample (A), a preamplifier circuit (20), an amplifier circuit (30), a dividing circuit (54) for performing a division based on the output signal from the amplifier circuit (30) and on the output signal from the amplifier (42), and a multiplier circuit (58) for performing multiplication of the output signal from the dividing circuit (54) and the output from the effective value calculating circuit (44).
Claims
1. An electron microscope comprising: an electron beam source for producing an electron beam; an electron beam detecting portion for detecting a part of the electron beam; a DC component extracting portion for extracting DC components of an output signal from the electron beam detecting portion; an image detecting portion for detecting a signal obtained in response to impingement of the electron beam on a sample; a division portion for performing a division based on an output signal from the image detecting portion and on an output signal from the electron beam detecting portion; and a multiplication portion for performing a multiplication of a signal indicative of the result of the division performed by the division portion and a signal extracted by the DC component extracting portion.
2. The electron microscope as set forth in claim 1, wherein said DC component extracting portion calculates an effective value of the output signal from said electron beam detecting portion, taken over a given period of time.
3. The electron microscope as set forth in claim 2, wherein said given period of time is set to be long enough to obtain one frame of image containing an image of the sample based on the signal obtained in response to impingement of the electron beam on the sample.
4. The electron microscope as set forth in claim 1, wherein said DC component extracting portion integrates an output signal from said electron beam detecting portion, removes DC components of the integral output signal to thereby produce a second integral signal, produces a third integral signal opposite in polarity to the second integral signal, and sums up the second and third integral signals.
5. The electron microscope as set forth in claim 1, wherein processing performed by said DC component extracting portion, said division portion, and said multiplication portion is performed by digital computations.
6. The electron microscope as set forth in claim 2, wherein processing performed by said DC component extracting portion, said division portion, and said multiplication portion is performed by digital computations.
7. The electron microscope as set forth in claim 3, wherein processing performed by said DC component extracting portion, said division portion, and said multiplication portion is performed by digital computations.
8. The electron microscope as set forth in claim 4, wherein processing performed by said DC component extracting portion, said division portion, and said multiplication portion is performed by digital computations.
9. A method of operating an electron microscope, comprising the steps of: detecting a part of an electron beam generated by an electron beam source to thereby produce a first signal; extracting DC components of the first signal to produce a second signal; detecting a signal obtained by impingement of the electron beam on a sample to produce an image signal; performing a division based on the image signal and on the first signal; multiplying a signal indicative of the result of the division by the second signal; and displaying an electron microscope image based upon the product of the multiplication in the previous step.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
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DESCRIPTION OF THE INVENTION
(18) The preferred embodiments of the present invention are hereinafter described in detail with reference to the drawings. It is to be understood that the embodiments described below do not unduly restrict the contents of the present invention delineated by the claims and that not all the configurations described below are essential constituent components of the invention.
(19) In the following, a scanning transmission electron microscope (STEM) is taken as one example of electron microscope associated with the present invention. The present invention can also be applied to other electron microscopes such as a scanning electron microscope (SEM).
1. First Embodiment
(20)
(21) The electron beam released from the electron beam source 11 is partially cut off by the noise canceling aperture 12 and then converged onto a sample A by the lens 13. A well-known electron gun such as a CFEG (cold-field emission gun) can be used as the electron beam source 11.
(22) The electron beam transmitted through the sample A passes through the lens 14 and is partially detected by the detector 15. An image signal detected by the detector 15 is the product of the emission current I1 hitting the sample A and the brightness component S of the sample A, i.e., I1×S.
(23) The noise canceling aperture 12 detects the emission current (noise signal). For example, any illumination aperture disposed between the electron beam source 11 and the sample A such as a condenser aperture may also be used as the noise canceling aperture 12 in the electron optical column 10. Apart from the illumination aperture, a dedicated noise canceling aperture 12 may also be mounted. The emission current I2 detected by the noise canceling aperture 12 is amplified by the noise detecting circuit 40.
(24) Utilizing that the emission current I1 hitting the sample A and the emission current I2 detected by the noise canceling aperture 12 are in a proportional relationship (I1=n×I2), the noise canceling circuit 50 removes (or correctly, reduces) the noise signal superimposed on the output signal from the amplifier circuit 30. The signal free of the noise signal is arithmetically processed in a given manner by the processing section 60 and then sent to the personal computer (PC) 2. An STEM image of the sample A is displayed on the display screen of the PC 2 and stored.
(25)
(26) In the present embodiment, as shown in
(27) When the noise canceling function is inactive, the output signal from the amplifier circuit 30 is applied to the processing section 60 via the switch circuit 59. Accordingly, where the noise canceling function is inactive, STEM imaging is performed fundamentally using only two adjustments, i.e., contrast and brightness. The contrast is a gain applied to the image signal for adjusting the degree of lightness or darkness. In the present embodiment, contrast is set into the detector 15. The brightness is a DC voltage applied to cancel the offset component of the image signal. In the present embodiment, brightness is set into the preamplifier circuit 20.
(28) In the present embodiment, the preamplifier circuit 20 is configured including an adder 22 and an amplifier 24. Brightness B is added by the adder 22 to an image signal S×I1 (see
V.sub.1=Gp×(S×I1+B) (1)
(29) In the present embodiment, the amplifier circuit 30 is configured including an amplifier 32. The output signal V.sub.1 from the preamplifier circuit 20 is amplified by a factor of Ga by the amplifier 32. Using Eq. (1), the output signal V.sub.2 (see
V.sub.2=Ga×Gp×(S×I1+B) (2)
(30) The processing section 60 converts the analog output signal from the amplifier circuit 30 into digital form by means of an A/D converter 62, then creates image data by performing arithmetic processing such as averaging, and sends the created data to the PC 2 shown in
(31) On the other hand, when the noise canceling function is active, the output signal V.sub.2 from the amplifier circuit 30 is noise-canceled by the noise canceling circuit 50 and then applied to the processing section 60 via the switch circuit 59.
(32) In the present embodiment, the noise canceling circuit 50 is configured including a subtractor 52, a divider circuit 54, an adder 56, an amplifier 57, a multiplier circuit 58, and the switch circuit 59. The amplifier 57 gives a gain (Gp×Ga) equal to the product of the gain Gp of the amplifier 24 and the gain Ga of the amplifier 32 to the brightness B. The subtractor 52 subtracts the output signal (Gp×Ga×B) from the amplifier 57 from the output signal V.sub.2 from the amplifier circuit 30. Even when the noise canceling function is active, the output signal V.sub.2 from the amplifier circuit 30 is given by Eq. (2) and so the output signal V.sub.3 (see
(33)
(34) As is obvious from Eq. (3), the brightness added by the preamplifier circuit 20 is canceled out in the output signal V.sub.3 from the subtractor 52. The output signal V.sub.3 from the subtractor 52 is applied to the input (X) of the numerator side of the divider circuit 54. The noise signal detected by the noise detecting circuit 40 is applied to the input (Y) on the denominator side of the divider circuit 54.
(35) In the present embodiment, the noise detecting circuit 40 is configured including an amplifier 42 and an effective value calculating circuit 44. The amplifier 42 converts the emission current I2 (see
V.sub.4=Gn×I2 (4)
(36) The effective value calculating circuit 44 calculates the effective value (RMS) of the output signal V.sub.4 from the amplifier 42 over a preset time on a real-time basis. For example, a general-purpose IC may be used as the effective value calculating circuit 44.
(37) The output signal V.sub.3 from the subtractor 52 and the output signal V.sub.4 from the amplifier 42 are applied to the input (X) on the numerator side and the input (Y) on the denominator side, respectively, of the divider circuit 54 and divides the signal V.sub.3 by the signal V.sub.4. Therefore, using Eqs. (3) and (4), the output signal V.sub.5 (see
(38)
(39) The multiplier circuit 58 multiplies the output signal V.sub.5 (see
(40)
(41) where the emission current I2 is given by
I2=I2.sub.DC+N (7)
where I2.sub.DC is the DC component and N is the noise component.
(42) The output signal (Gn×I2).sub.RMS from the effective value calculating circuit 44 can be approximated by
(Gn×I2).sub.RMS=Gn×(I2).sub.RMS≅Gn×I2.sub.DC (8)
(43) The equation I1=I2×n is substituted into Eq. (6). Eqs. (7) and (8) are also substituted. The output signal V.sub.6 from the multiplier circuit 58 is approximated by
(44)
(45) In Eq. (9), I2.sub.DC is an ideal DC current obtained by removing the noise component N from the emission current I2, and is an emission current detected by the noise detecting circuit 40 when there is no emission noise. The equation I1=I2×n indicates that I2.sub.DC×n is equivalent to an ideal DC current I1.sub.DC obtained by removing the emission current from I1.
(46) Therefore, by substituting the equation I2.sub.DC×n=I1.sub.DC into Eq. (9), the output signal V.sub.6 from the multiplier circuit 58 is approximated by
V.sub.6≅Ga×Gp×S×I1.sub.DC (10)
(47) The adder 56 adds up the output signal V.sub.6 from the multiplier circuit 58 and the output signal (Gp×Ga×B) from the amplifier 57. Therefore, the output signal V.sub.7 (see
(48)
(49) The output signal V.sub.7 from the adder 56 is applied to the processing section 60 via the switch circuit 59. The processing section 60 converts the analog output signal from the adder 56 into digital form by the A/D converter 62, then averages or otherwise arithmetically processes the digital signal to create image data, and sends the image data to the PC 2 shown in
(50) I1.sub.DC of Eq. (11) is nearly equal in value to the emission current hitting the sample A when there is no emission noise. Consequently, STEM imaging is enabled only with adjustments of the contrast and brightness while Ga, Gp, Gn, and gain given to the brightness that is removed or re-added are kept constant at all times in the same way as when the noise canceling function is inactive.
(51) If the emission current varies with time, a signal obtained by removing only noise from the output signal V.sub.2 from the amplifier circuit 30 given by Eq. (2) can be kept obtained because the signal input to the processing section 60 is as given by Eq. (11) at all times.
(52) Eq. (11) representing the signal applied to the processing section 60 when the noise canceling function is active is obtained by replacing I1 of Eq. (2) representing the signal applied to the processing section 60 when the noise canceling function is inactive by I1.sub.DC. Consequently, it is not necessary to perform cumbersome adjustments whenever the noise canceling function is activated or deactivated.
(53) In the present embodiment, the electron beam source 11 corresponds to the “electron beam source” of the present invention. The noise canceling aperture 12 and amplifier 42 together correspond to the “electron beam detecting portion” of the present invention. The effective value calculating circuit 44 corresponds to the “DC component extracting portion” of the present invention. The detector 15, preamplifier circuit 20, and amplifier circuit 30 together correspond to the “image detecting portion” of the present invention. The divider circuit 54 corresponds to the “division portion” of the present invention. The multiplier circuit 58 corresponds to the “multiplication portion” of the present invention.
(54) As described so far, according to the electron microscope of the first embodiment, the effective value of the noise signal is calculated by the effective value calculating circuit 44. The output signal from the divider circuit 54 is multiplied by the output signal from the effective value calculating circuit 44 by means of the multiplier circuit 58. Consequently, the gain of the noise canceling circuit 50 can be determined irrespective of the image signal. Thus, if various settings in the illumination system, imaging system, and detection system are modified for imaging, the gain can be maintained constant. The gain will vary only when the beam current located above the noise canceling aperture 12 is varied. Because the effective value of the noise signal is being computed, an image signal of unity magnification that has been noise-canceled can be obtained after a given time (from several seconds to tens of seconds) that is set in the circuitry if no manipulations are performed. This dispenses with adjustment of the gain. If a CFEG (cold-field emission gun) is used as the electron beam source 11, an image free from emission noises can be observed by performing manipulations similar to manipulations of a Schottky emission gun.
(55) According to the electron microscope of the present embodiment, a division is performed using analog signals and so it is easy to make a connection with an external device. More latitude is allowed in determining a range of input voltages than when a division is performed using digital computations. The technique of the present embodiment can cancel emission noises detected with numerous electron microscope-related detectors available on the market and, therefore, much greater versatility is offered.
(56) As described so far, according to the present embodiment, an electron microscope can be offered which can eliminate difficulties with adjustments heretofore encountered when conventional analog division techniques are used without being affected by decreases in emission current and which achieves a noise canceling function having greater versatility than digital division techniques.
(57) As shown in
2. Second Embodiment
(58)
(59) In the present embodiment, the output signal from the amplifier 42 and the output signal from the amplifier 32 are applied to the processing section 60 and converted into digital form by A/D converters 62 and 64, respectively. The processing section 60 calculates the effective value of the output value from the A/D converter 62 over a preset time by digital computation. The offset added to the image signal by the preamplifier circuit 20 is amplified by the amplifiers 24 and 32. The processing section 60 subtracts the resulting value (Gp×Ga×B) from the output value from the A/D converter 64 by digital computation, and divides this difference by the output value from the A/D converter 62 similarly to Eq. (5). Also, the processing section 60 performs a multiplication of the result of the division (quotient) and the result of the calculation of the effective value (Gn×I2).sub.RMS similarly to Eq. (6) by digital computation. Furthermore, the processing section 60 adds the subtracted value (Gp×Ga×B) to the product by digital computation. Then, the processing section 60 averages or otherwise arithmetically processes the resulting slim and sends the result to the PC 2 shown in
(60) In the present embodiment, the electron beam source 11 corresponds to the “electron beam source” of the present invention. The noise canceling aperture 12 and the amplifier 42 together correspond to the “electron beam detecting portion” of the present invention. The detector 15, the preamplifier 20, and the amplifier circuit 30 together correspond to the “image detecting portion” of the present invention. The processing section 60 corresponds to all of the “DC component extracting portion”, the “division portion”, and the “multiplication portion” of the present invention.
(61) The electron microscope of the second embodiment described so far can yield the same advantageous effects as the first embodiment.
3. Third Embodiment
(62)
(63)
(64) The integrating circuit 71 receives the output signal (see
(65) The capacitor 72 is used to cut off DC components. The capacitor 72 removes DC components from the output signal (see
(66) The inverting amplifier circuit 73 inverts the signal (see
(67) The adder circuit 74 sums up the output signal (see
(68) The non-inverting amplifier circuit 75 buffers and outputs the output signal (see
(69) In the low-pass filter 70 of the example of
(70) In the present embodiment, the electron beam source 11 corresponds to the “electron beam source” of the present invention. The noise canceling aperture 12 and the amplifier 42 together correspond to the “electron beam detecting portion” of the present invention. The filter circuit 70 corresponds to the “DC component extracting portion” of the present invention. The detector 15, preamplifier circuit 20, and amplifier circuit 30 together correspond to the “image detecting portion” of the present invention. The divider circuit 54 corresponds to the “division portion” of the present invention. The multiplier circuit 58 corresponds to the “multiplication portion” of the present invention.
(71) According to the electron microscope of the third embodiment described so far, the output signal from the low-pass filter 70 can be kept at a constant voltage in the same way as for the effective value calculating circuit 44 of the first embodiment. Consequently, the electron microscope of the third embodiment can yield the same advantageous effects as the first embodiment.
4. Fourth Embodiment
(72)
(73)
(74) In the present embodiment, an image signal S×I1 (see
V.sub.1=Gp×S×I1 (12)
(75) The output signal V.sub.1 from the preamplifier circuit is amplified by a factor of Ga by the amplifier 32. Therefore, using Eq. (12), the output signal V.sub.2 (see
V.sub.2=Ga×Gp×S×I1 (13)
(76) When the noise canceling function is inactive, the output signal V.sub.2 from the amplifier circuit 30 is applied to the adder 56 via the switch circuit 59 and added to the output signal from the amplifier 57. The amplifier 57 gives a gain, Gp×Ga, equal to the product of the gain Gp of the amplifier 24 and the gain Ga of the amplifier 32 to the brightness B. Therefore, the output signal V.sub.7 from the adder 56 is given by
V.sub.7=Ga×Gp×(S×I1+B) (14)
(77) The analog output signal V.sub.7 from the adder 56 is applied to the processing section 60 and converted into digital form by the A/D converter 62 and then averaged or otherwise arithmetically processed and sent to the PC 2 shown in
(78) On the other hand, where the noise canceling function is active, the output signal V.sub.2 from the amplifier circuit 30 is noise-canceled and then applied to the adder 56 via the switch circuit 59.
(79) In particular, the output signal V.sub.2 from the amplifier circuit 30 is applied to the input (X) on the numerator side of the divider circuit 54. The output signal from the amplifier 42 contained in the noise detection circuit 40 is applied to the input (Y) of the denominator side of the divider circuit 54. As described already in connection with the first embodiment, the amplifier 42 converts the emission current I2 (see
(80) Accordingly, using Eqs. (13) and (4), the output signal V.sub.5 (see
(81)
(82) As already described with reference to the first embodiment, the multiplier circuit 58 performs multiplication of the output signal V.sub.5 (see
(83) The output signal V.sub.6 from the multiplier circuit 58 is applied to the adder 56 via the switch circuit 59 and added to the output signal (Gp×Ga×B) from the amplifier 57 by the adder 56. Therefore, the output signal V.sub.7 (see
(84) The analog output signal V.sub.7 from the adder 56 is applied to the processing section 60 and converted into digital form by the A/D converter 62, then averaged or otherwise arithmetically processed, and sent to the PC 2 shown in
(85) In the present embodiment, the electron beam source 11 corresponds to the “electron beam source” of the present invention. The noise canceling aperture 12 and the amplifier 42 together correspond to the “electron beam detecting portion” of the present invention. The effective value calculating circuit 44 corresponds to the “DC component extracting portion” of the present invention. The detector 15, the preamplifier circuit 20, and the amplifier circuit 30 together correspond to the “image detecting portion” of the present invention. The divider circuit 54 corresponds to the “division portion” of the present invention. The multiplier circuit 58 corresponds to the “multiplication portion” of the present invention.
(86) According to the electron microscope of the fourth embodiment described so far, the same signal as in the first embodiment is applied to the processing section 60 whether the noise canceling function is inactive or active. Consequently, the electron microscope of the fourth embodiment yields the same advantageous effects as the first embodiment, although the configuration is simpler than the first embodiment.
(87) The present invention is not restricted to the present embodiment. Rather, various changes and modifications are possible without departing from the gist and scope of the present invention.
(88) It is to be understood that the above-described embodiments are merely exemplary and that the present invention are not restricted thereto. For example, the various modifications may be combined appropriately.
(89) The present invention embraces configurations substantially identical (e.g., in function, method, and results or in purpose and advantageous effects) with the configurations described in the embodiments of the invention. Furthermore, the invention embraces configurations described in the embodiments and including portions which have non-essential portions replaced. In addition, the invention embraces configurations which produce the same advantageous effects as those produced by the configurations described in the embodiments or which can achieve the same objects as the configurations described in the embodiments. Further, the invention embraces configurations which are similar to the configurations described in the embodiments except that well-known techniques have been added.
(90) Having thus described my invention with the detail and particularity required by the Patent Laws, what is desired protected by Letters Patent is set forth in the following claims.