Ferromagnetic resonance (FMR) electrical testing apparatus for spintronic devices
11397226 · 2022-07-26
Assignee
Inventors
- Guenole Jan (San Jose, CA, US)
- Son Le (Gilroy, CA, US)
- Luc Thomas (San Jose, CA, US)
- Santiago Serrano Guisan (San Jose, CA, US)
Cpc classification
G01R33/24
PHYSICS
G01N24/00
PHYSICS
International classification
G01R33/24
PHYSICS
Abstract
A scanning ferromagnetic resonance (FMR) measurement system is disclosed with a radio frequency (RF) probe and one or two magnetic poles mounted on a holder plate and enable a perpendicular-to-plane or in-plane magnetic field, respectively, at test locations. While the RF probe tip contacts a magnetic film on a whole wafer under test (WUT), a plurality of microwave frequencies (f.sub.R) is sequentially transmitted through the probe tip. Simultaneously, a magnetic field (H.sub.R) is applied to the contacted region thereby causing a FMR condition in the magnetic film for each pair of (H.sub.R, f.sub.R) values. RF output signals are transmitted through or reflected from the magnetic film to a RF diode and converted to voltage signals which a controller uses to determine effective anisotropy field, linewidth, damping coefficient, and/or inhomogeneous broadening for a sub-mm area. The WUT is moved to preprogrammed locations to enable multiple FMR measurements at each test location.
Claims
1. A scanning ferromagnetic resonance (FMR) measurement system for determining magnetic properties in a magnetic film or in a plurality of device structures that are formed on a wafer under test (WUT), comprising: a RF probe linked to a microwave (RF) generator and having at least a probe tip wherein at least one signal pathway contacts the magnetic film or plurality of device structures during a FMR measurement; a magnetic assembly comprised of at least one magnetic field source that provides a magnetic field proximate to the RF probe tip which together with a simultaneous application of a microwave frequency from the RF generator is configured to induce a first FMR condition in the magnetic film or plurality of device structures; a detection system for monitoring microwave absorbance and a corresponding power loss by the magnetic film or plurality of device structures when the first FMR condition therein is established wherein the WUT is configured to move laterally and vertically relative to the RF probe such that the probe tip contacts the magnetic film or plurality of devices at one or more predetermined locations during a FMR measurement sequence; and a controller to manage the simultaneous application of the microwave frequency and magnetic field, the WUT movement, and to receive a signal from the detection system, wherein the signal is converted to an output comprised of one or more magnetic properties.
2. The scanning FMR measurement system of claim 1 wherein the RF probe and magnetic assembly are attached to a holder plate, and are held stationary while the WUT is moved during the FMR measurement sequence.
3. The scanning FMR measurement system of claim 1 wherein the RF probe and magnetic assembly are attached to a holder plate, and are moved while the WUT is stationary during the FMR measurement sequence.
4. The scanning FMR measurement system of claim 1 that is configured in a transmission mode wherein a RF input signal from the RF generator passes through a first signal pathway in the RF probe tip to the magnetic film or plurality of magnetic devices, and a second signal pathway in the RF probe transmits a RF output signal from the magnetic film or plurality of magnetic devices to a RF diode in the detection system.
5. The scanning FMR measurement system of claim 1 that is configured in a reflectance mode wherein a RF input signal from the RF generator passes through a first signal pathway in the RF probe to the magnetic film or plurality of magnetic devices, and the first signal pathway also transmits a RF output signal from the magnetic film or plurality of magnetic devices to a RF diode in the detection system.
6. The scanning FMR measurement system of claim 1 wherein the detection system comprises a RF diode that converts the RF output signal to a voltage signal, and an analog-to-digital converter between the RF diode and the controller.
7. The scanning FMR measurement system of claim 1 wherein the magnetic assembly has a single magnetic pole that is aligned above the RF probe tip, and applies the magnetic field in a perpendicular-to-plane direction at each of the one or more predetermined locations during the FMR measurement sequence.
8. The scanning FMR measurement system of claim 7 wherein the applied microwave frequency is in a range of 1 to 100 GHz.
9. The scanning FMR measurement system of claim 1 wherein the magnetic assembly has two magnetic poles that are positioned on opposite sides of the RF probe tip, and apply the magnetic field in an in-plane direction at each of the one or more predetermined locations during the FMR measurement sequence.
10. The scanning FMR measurement system of claim 9 wherein the applied microwave frequency is in a range of 0.01 to 100 GHz.
11. The scanning FMR measurement system of claim 5 further comprised of a directional coupler that directs the RF input signal to the RF probe, and is employed to isolate the RF output signal from the RF probe, which is transmitted to the RF diode and then to the controller.
12. The scanning FMR measurement system of claim 1 wherein the RF probe and magnetic assembly are installed in an electrical probe station.
13. The scanning FMR measurement system of claim 1 wherein the controller is programmed to repeat the simultaneous application of a microwave frequency and a magnetic field at each of the one or more predetermined locations thereby inducing at least a second FMR condition, wherein at least one of the microwave frequency and magnetic field is different from the microwave frequency and magnetic field used to induce the first FMR condition.
14. A system comprising: a probe configured to apply one or more microwave frequency values to one or more locations on a magnetic material; a magnetic field source configured to apply one or more magnetic field values to the one or more locations on the magnetic material which together with the application of the one or more microwave frequency values from the probe establishes one or more ferromagnetic resonance conditions at the one or more locations on the magnetic material thereby resulting in a RF output signal for each pair of an applied microwave frequency value and an applied magnetic field value; a RF diode configured to receive RF output signals and convert each RF output signal to a voltage signal; and a controller configured to receive each voltage signal from the RF diode and determine one or more properties of the magnetic material based on each received voltage signal.
15. The system of claim 14, wherein the magnetic field source includes a magnetic pole that is aligned above a tip of the probe and is configured to apply the one or more magnetic fields in a perpendicular-to-plane direction at each of the one or more locations on the magnetic material.
16. The system of claim 14, wherein the magnetic field source includes at least two magnetic poles that are positioned on opposite sides of a tip of the probe and are configured to apply the one or more magnetic fields in an in-plane direction at each of the one or more locations on the magnetic material.
17. The system of claim 14, wherein the one or more microwave frequency values are in a range of about 0.01 to about 100 GHz, and wherein the magnitude of the one or more magnetic field values is up to 3 Tesla.
18. A system comprising: a RF probe configured to apply one or more microwave frequencies to one or more locations on a magnetic material; a magnetic field source configured to provide a magnetic field proximate to the RF probe which together with an application of a microwave frequency from the RF probe is configured to induce a first ferromagnetic resonance condition in the magnetic material; a detection system for monitoring microwave absorbance and a corresponding power loss by the magnetic material when the first FMR condition therein is established and thereby output a voltage signal based on the microwave absorbance and the corresponding power loss by the magnetic material when the first FMR condition therein is established; and a controller configured to manage the application of the microwave frequency and magnetic field and to receive the voltage signal from the detection system, the controller further configured to determine one or more properties of the magnetic material based on the received voltage signal.
19. The system of claim 18, wherein the detection system includes a Schottky diode.
20. The system of claim 18, wherein the magnetic field source has two magnetic poles that are positioned on opposite sides of the RF probe to provide the magnetic field proximate to the RF probe.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
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DETAILED DESCRIPTION
(15) The present disclosure is a scanning FMR system that is designed to measure magnetic properties including H.sub.K and α for magnetic structures that may be substantially smaller than 1 mm in diameter. Multiple test sites across a whole wafer are sequentially measured with either a RF transmission mode or a RF reflectance mode. X-axis and y-axis coordinates on the wafer under test (WUT) are in a plane that is aligned parallel to and above the plane of the wafer chuck. The present disclosure also encompasses a FMR test method for measuring magnetic properties of one or more magnetic films on unpatterned wafers or in device structures. The terms “RF” and “microwave” may be used interchangeably.
(16) In related U.S. patent application Ser. No. 15/463,074, we disclosed a FMR measurement system that relies on a waveguide transmission line (WGTL) that is attached to RF input and RF output connectors and is capable of taking measurements at a plurality of sites on a whole wafer. However, the WGTL is generally custom designed and requires the positioning of the WGTL as close as possible to the WUT to improve the coupling and magnetic field at the device level. Furthermore, the area probed in the measurement is quite large (mm to cm diameter) compared with sub-micron dimensions in the device structures. Now, we have discovered an improved scanning FMR measurement system that may be entirely constructed from commercially available components, and enables magnetic properties to be monitored and measured in smaller structures that may be substantially less than 1 mm in diameter.
(17) Referring to
(18) A magnetic field in magnetic assembly 30 (comprised of at least one magnetic field source) is produced by power input from the power generator 31 when instructed to do so by the controller through link 42a. In preferred embodiments, a magnetic field is applied to a predetermined (x.sub.n, y.sub.n) coordinate on the WUT while a RF signal pathway in the RF probe 40 on mounting bracket 46 contacts a top surface 22t of the magnetic film at the (x.sub.n, y.sub.n) coordinate. As a result of simultaneously applying a microwave frequency (RF input signal) from the RF probe, and a magnetic field of up to 3 Tesla from a pole tip (shown in
(19) The RF detector may be a power diode 44 hereinafter referred to as a RF diode, which detects a RF output signal transmitted from the magnetic film and that exits the RF probe through a second signal pathway and second RF connector (not shown). Each RF output signal corresponds to a RF power loss caused by the FMR condition where a certain amount of microwave power is absorbed and excites the magnetic film to a resonance state. Each FMR measurement may comprise a plurality of RF input signals each corresponding to a different RF frequency. After the FMR measurement is performed at the (x.sub.n, y.sub.n) coordinate, the wafer chuck 20 and WUT 22 are lowered 51d via a signal from the controller 11 through link 42d to reestablish a gap distance below the RF probe. Subsequently, the wafer chuck and WUT are moved to another predetermined (x.sub.n, y.sub.n) coordinate, and then the wafer chuck is raised 51u to enable the RF probe to contact magnetic film top surface 22t for another FMR measurement.
(20) The controller 11 has an electrical connection 42b to a RF generator 48 that provides a plurality of microwave frequencies through link 42c to a first RF connector (not shown) on RF probe 40. In some embodiments, the RF generator produces a first microwave frequency (f1) in the range of 1 to 20 GHz. However, the present disclosure anticipates inserting a frequency multiplier module (not shown) between the RF generator and RF probe that adjusts f1 to a second RF frequency (f2) where f2>f1. For example, when f1=20 GHz, the frequency multiplier module may be an active frequency doubler that adjusts f1 to f2 where f2=40 GHz. According to the first embodiment, RF frequencies below 1 GHz are not practical for the purpose of inducing a FMR condition in the magnetic film.
(21) In a preferred operating mode for a FMR measurement, the applied magnetic field is varied (swept from a minimum to a maximum value) at a constant microwave frequency. The FMR measurement is preferably repeated by sweeping the magnetic field successively through each of a plurality of different microwave frequencies. The RF diode converts the power output from the RF probe to a voltage signal that is transmitted through an output cable 45 to the controller. Thereafter, the controller calculates H.sub.k and α, and in some cases γ and inhomogeneous broadening (L.sub.0), based on each pair of applied magnetic field value and applied microwave frequency used to establish a FMR condition, and on voltage output data from the RF diode for each (x.sub.n, y.sub.n) coordinate used in the FMR measurement sequence.
(22) The present disclosure encompasses designs other than the one illustrated in
(23) Referring to
(24) In
(25) Referring to
(26) Referring to
(27) Referring to
(28) In the exemplary embodiment, controller 11 has a link 42b to a commercial RF generator 48 with capability to generate a range of frequencies mentioned previously. The RF generator is connected by link 42c to a frequency multiplier module 47 such as an active frequency doubler, which in turn is connected through RF input cable 17a to RF input connector 15a on RF probe 40. RF probe end 40e contacts magnetic film 22f during a FMR measurement when a magnetic field from at least one magnetic pole tip (not shown), and a RF frequency from a first signal pathway (40s in
(29) During intervals when no FMR measurements are being performed, the RF probe tip including end 40e is a gap distance>0 from the top surface 22t of the magnetic film 22f on WUT 22. As indicated previously, when the scanning FMR measurement system is programmed to perform a plurality of FMR measurements at a certain (x.sub.n, y.sub.n) coordinate, the wafer chuck is raised so that the RF probe end contacts the magnetic film until the FMR measurements are completed. For the single pole embodiment (
(30) During a FMR measurement when a magnetic field is applied to an area around an (x.sub.n, y.sub.n) coordinate on the magnetic film contacted by the RF probe end 40e, a portion of the microwave power supplied by the RF input signal is absorbed by the magnetic film 22f during a FMR condition so that the RF output signal carried through RF output cable 17b and through a RF power diode has reduced power compared with the RF input signal. The RF power diode may be a Schottky diode, or another commercial RF diode, and converts the RF output signal for each (H.sub.R, f.sub.R) pair to a voltage measurement that is relayed to the controller. In other words, the intensity of the applied magnetic field (H.sub.R) may be varied for a given RF frequency (f.sub.R), or a plurality of RF frequencies may be applied with a constant magnetic field during each FMR measurement at an (x.sub.n, y.sub.n) coordinate. Preferably, the applied magnetic field is swept from a minimum to a maximum value at a constant microwave frequency (F1), and then the FMR measurement is repeated by sweeping the magnetic field successively with each of a plurality of different microwave frequencies (F2, F3, . . . Fn). Once a plurality of FMR measurements is taken at a first (x.sub.n, y.sub.n) coordinate, the wafer chuck and WUT are lowered and “stepped” to a second (x.sub.n, y.sub.n) coordinate for a second set of FMR measurements. Thus, the scanning FMR measurement method described herein comprises taking multiple FMR measurements at a plurality of preprogrammed (x.sub.n, y.sub.n) coordinates, and is managed by the controller 11.
(31) According to a second embodiment shown in
(32) A portion of the microwave power supplied by the RF input signal is absorbed by the magnetic film 22f proximate to a (x.sub.n, y.sub.n) coordinate contacted by the RF probe end. In this case, the RF output signal is carried through the signal pathway 40s used for the input signal and through RF input connector 15a back to directional coupler 60 where the RF signal is routed through RF output cable 17c to Schottky diode 44 or another RF diode, and ADC 49 before reaching controller 11. In alternative embodiments, a power divider or a bias tee may be used instead of the directional coupler as appreciated by those skilled in the art.
(33) As described earlier with respect to the transmission mode, the intensity of the applied magnetic field (H.sub.R) at the (x.sub.n, y.sub.n) coordinate may be swept from a minimum to a maximum value for each in a series of frequencies F1, F2, and so forth up to Fn. Alternatively, the RF frequency may be swept from a minimum to a maximum value for each applied magnetic field in a series of increasing magnitudes from H1, H2, and so forth up to Hn. Once a plurality of FMR measurements is taken at a first (x.sub.n, y.sub.n) coordinate, the wafer chuck and WUT are lowered and “stepped” to a second (x.sub.n, y.sub.n) coordinate for a second series of FMR measurements. Thus, the scanning FMR measurement method of the second embodiment that is based on a RF reflectance mode comprises taking multiple FMR measurements at a plurality of preprogrammed (x.sub.n, y.sub.n) coordinates on a magnetic film 22f. The Schottky diode 44 or another commercial RF diode, converts the RF output signal for each (H.sub.R, f.sub.R) pair to a voltage measurement that is relayed to the controller through ADC 49.
(34) The controller uses the FMR measurement data and one or more of equations (1)-(3) described previously to determine Hk, α, and in some cases γ and inhomogeneous broadening (L.sub.0) at each (x.sub.n, y.sub.n) coordinate on the magnetic film. As indicated earlier, the term “magnetic film” may refer to a stack of layers in an unpatterned film, or in a plurality of devices having sub-millimeter or even sub-micron dimensions along the x-axis and y-axis directions. In all cases, there should be a conductive pathway through the magnetic film to enable a RF frequency (with an applied magnetic field) to induce a FMR condition in the magnetic film.
(35) Referring to
(36) In
(37) Referring to
(38) As a result of the simultaneous application of microwave frequency F1 and the variable magnetic field, the magnetic film achieves a FMR condition and absorbs a portion of the microwave power that depends on the magnetic properties of the magnetic film, the magnitude of F1, and the applied magnetic field (H.sub.R) that induced the ferromagnetic resonance state in the film. Accordingly, in step 112, the RF power diode detects a reduced power value in the RF output signal compared with the value specified by the controller in the RF input signal from step 111.
(39) In step 113, the RF power diode converts the RF output signal to a voltage measurement that is transmitted to the controller (through an ADC in the exemplary embodiments in
(40) Step 114 comprises a repetition of steps 111-113 except the RF input signal has a second frequency F2 that is applied to the magnetic film at the previously selected (x.sub.n, y.sub.n) coordinate after F1 is applied. In some embodiments, steps 111-113 are repeated a plurality of times at each (x.sub.n, y.sub.n) coordinate used for the FMR measurement method. In other words, a third frequency F3 that differs from F1 and F2 may be applied during an interval of time after F2, and so forth up to an “nth” frequency Fn after F3 is applied. Note that the applied magnetic field is preferably swept between a minimum and a maximum value for each frequency F1 up to Fn. Thus, a FMR condition occurs with each applied frequency and with a certain magnetic field value, and each FMR condition has a unique microwave absorbance that is translated into a corresponding voltage signal by the RF power diode. In an alternative embodiment, the applied magnetic field is held constant at a first value H1 while the microwave frequencies are varied (swept) from F1 up to Fn to establish a FMR condition. Thereafter, a second magnetic field H2 that is different from H1 may be applied while the microwave frequencies are varied through a range of values. The scanning FMR measurement method may be repeated by sweeping through a range of RF frequencies with a different magnetic field up to a maximum Hn value.
(41) Referring to step 115, the controller commands the wafer chuck and overlying magnetic film to move to a different (x.sub.n, y.sub.n) coordinate such as from (x.sub.1, y.sub.1) to (x.sub.2, y.sub.2). The movement comprises a first step of disengaging the RF probe tip from the first (x.sub.n, y.sub.n) coordinate with a downward movement of the wafer chuck and WUT (movement 51d in
(42) Thereafter, steps 111-114 are repeated to complete a FMR measurement at the second (x.sub.n, y.sub.n) coordinate. Note that each (x.sub.n, y.sub.n) coordinate may comprise a contact area of less than a square micron up to a plurality of square millimeters depending on the size of the signal probes 40s selected, and each (x.sub.n, y.sub.n) coordinate may be a center point in the area contacted by the RF probe tip.
(43) Depending on the diameter of the WUT that may be 6″, 8″, or 12″, for example, and the number of different (x.sub.n, y.sub.n) coordinates desired for FMR measurements, step 116 indicates that steps 111-115 may be repeated a plurality of times to yield a plurality of FMR measurements involving “n” different (x.sub.n, y.sub.n) coordinates each with a plurality of (H.sub.R, f.sub.R) pairs where f.sub.R is one of F1 up to Fn, and H.sub.R may be varied from a minimum H1 value to a maximum Hn value. At step 117, a decision is made whether or not all of the pre-selected (x.sub.n, y.sub.n) coordinates on the magnetic film have been tested. If “no”, another FMR measurement is taken at a different (x.sub.n, y.sub.n) coordinate. If “yes”, step 118 indicates the scanning FMR measurement method is complete.
(44) As mentioned earlier, the controller is capable of determining magnetic properties in the magnetic film at each measurement location corresponding to a different (x.sub.n, y.sub.n) coordinate. Each FMR measurement yields one or more pairs (frequency, field) also referred to as (H.sub.R, f.sub.R) pairs in equation (1) corresponding to each FMR condition. The controller uses FMR measurement data and one or more of equations (1)-(3) described previously to determine Hk, α, and in some cases γ and inhomogeneous broadening (L.sub.0).
(45) Using the transmission mode embodiment described earlier, we performed FMR measurements on full (unpatterned) film structures.
(46) All components required for assembling a scanning FMR measurement system for either the transmission mode or reflectance mode embodiments described herein are commercially available. The cross-sectional area of the device structures, or the area of unpatterned magnetic films that may be tested with a scanning FMR measurement scheme of the present disclosure are substantially smaller than in the prior art. Moreover, the magnetic assembly described previously enables a more uniform magnetic film to be applied thereby yielding more reliable FMR measurements than conventional methods.
(47) While this disclosure has been particularly shown and described with reference to the preferred embodiment thereof, it will be understood by those skilled in the art that various changes in form and details may be made without departing from the spirit and scope of this disclosure.