METHOD FOR MANUFACTURING A CELLULOSE PRODUCT BY A PRESSURE MOULDING APPARATUS, PRESSURE MOULDING APPARATUS AND CELLULOSE PRODUCT
20220227027 · 2022-07-21
Inventors
Cpc classification
B27N5/00
PERFORMING OPERATIONS; TRANSPORTING
B29C43/3642
PERFORMING OPERATIONS; TRANSPORTING
B29C51/002
PERFORMING OPERATIONS; TRANSPORTING
B29C49/22
PERFORMING OPERATIONS; TRANSPORTING
B29C49/0005
PERFORMING OPERATIONS; TRANSPORTING
Y02W90/10
GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
B31B2120/00
PERFORMING OPERATIONS; TRANSPORTING
B29C51/082
PERFORMING OPERATIONS; TRANSPORTING
B29C43/58
PERFORMING OPERATIONS; TRANSPORTING
B30B5/02
PERFORMING OPERATIONS; TRANSPORTING
B29C43/10
PERFORMING OPERATIONS; TRANSPORTING
B29C51/08
PERFORMING OPERATIONS; TRANSPORTING
B29C51/004
PERFORMING OPERATIONS; TRANSPORTING
B65B43/08
PERFORMING OPERATIONS; TRANSPORTING
B29C43/20
PERFORMING OPERATIONS; TRANSPORTING
B31B50/59
PERFORMING OPERATIONS; TRANSPORTING
B29C43/02
PERFORMING OPERATIONS; TRANSPORTING
B29C43/003
PERFORMING OPERATIONS; TRANSPORTING
B29K2001/00
PERFORMING OPERATIONS; TRANSPORTING
B29K2311/10
PERFORMING OPERATIONS; TRANSPORTING
B29C2043/5808
PERFORMING OPERATIONS; TRANSPORTING
International classification
B29C43/10
PERFORMING OPERATIONS; TRANSPORTING
B29C43/00
PERFORMING OPERATIONS; TRANSPORTING
B29C43/02
PERFORMING OPERATIONS; TRANSPORTING
B29C43/20
PERFORMING OPERATIONS; TRANSPORTING
B29C43/36
PERFORMING OPERATIONS; TRANSPORTING
B29C43/58
PERFORMING OPERATIONS; TRANSPORTING
B29C49/00
PERFORMING OPERATIONS; TRANSPORTING
B29C49/22
PERFORMING OPERATIONS; TRANSPORTING
B29C51/00
PERFORMING OPERATIONS; TRANSPORTING
B29C51/08
PERFORMING OPERATIONS; TRANSPORTING
B31B50/59
PERFORMING OPERATIONS; TRANSPORTING
B65B43/08
PERFORMING OPERATIONS; TRANSPORTING
Abstract
The present invention relates to a method of manufacturing a cellulose product having a flat or non-flat product shape by a pressure moulding apparatus comprising a forming mould. The forming mould has a forming surface defining said product shape, The method comprises the steps of:
arranging a cellulose blank containing less than 45 weight percent water in said forming mould; heating said cellulose blank to a forming temperature in the range of 100° C. to 200° C.; and pressing said cellulose blank by means of said forming mould with a forming pressure acting on the cellulose blank across said forming surface, said forming pressure being in the range of 1 MPa to 100 MPa.
Claims
1. A method for manufacturing a cellulose product having a non-flat product shape by a pressure moulding apparatus comprising a forming mould, the forming mould having at least two openable and closable negative forming surfaces or parts defining said product shape, comprising the steps of: arranging a cellulose blank with loose and separated fibres containing less than 45 weight percent water in said forming mould; heating said cellulose blank to a forming temperature in the range of 100° C. to 200° C.; and pressing said cellulose blank by means of said forming mould with a forming pressure acting on the cellulose blank across said forming surface, said forming pressure being in the range of 1 MPa to 100 MPa, wherein an isostatic pressure is obtained in force defined compressing devices, wherein said compressing devices comprises a flexible barrier or a membrane separating the cellulose blank from a pressure media, wherein: said forming mould comprises the flexible barrier or membrane and said pressure moulding apparatus further comprises a fluid control device for controlling a fluid, the pressure media, to exert the isostatic pressure on said cellulose blank via said fluid impermeable membrane.
2. The method according to claim 1, wherein said cellulose blank contains less than 25 weight percent water, specifically less than 15 weight percent water.
3. The method according to claim 1, wherein said cellulose blank comprises wood pulp, specifically at least 90 weight percent wood pulp.
4. The method according to claim 1, wherein said step of heating at least partly takes place before said step of pressing.
5. The method according claim 1, wherein the forming mould comprises a forming mould part and pressure mould part and at least one of said forming mould part and pressure mould part is heated before said step of pressing.
6. A pressure moulding apparatus for manufacturing a cellulose product having a non-flat product shape starting from a cellulose blank with loose and separated fibres comprising: a forming mould at least two openable and closable negative forming surfaces or parts defining said product shape, wherein an isostatic pressure is obtained in force defined compressing devices, wherein said compressing devices comprises a flexible barrier or a membrane surrounding and separating the cellulose blank from a pressure media, wherein: said forming mould comprises the flexible barrier or membrane; and said pressure moulding apparatus further comprises a fluid control device configured to control a fluid, the pressure media, to exert the isostatic pressure on said cellulose blank via said fluid impermeable membrane, wherein, the flexible membrane is arranged between said fluid control device and said cellulose blank.
7. A cellulose product having a non-flat shape comprising compressed loose and separated fibres, wherein the cellulose product is a hollow bottle.
8. A cellulose product according to claim 7, wherein the cellulose product is mainly uniform in thickness.
Description
BRIEF DESCRIPTION OF DRAWINGS
[0054] These and other aspects of the present invention will now be described in more detail, with reference to the appended drawings showing example embodiments of the invention, wherein:
[0055]
[0056]
[0057]
[0058]
[0059]
[0060]
[0061]
[0062]
[0063]
DESCRIPTION OF EXAMPLE EMBODIMENTS
[0064] Various aspects of the disclosure will hereinafter be described in conjunction with the appended drawings to illustrate and not to limit the disclosure, wherein like designations denote like elements, and variations of the described aspects are not restricted to the specifically shown embodiments, but are applicable on other variations of the disclosure.
[0065] In the present detailed description, a method for manufacturing a cellulose product, a pressure moulding apparatus, and a cellulose product will be described.
[0066] Various embodiments of sheet materials or blanks according to the disclosure are mainly discussed with reference to a cellulose blank placed in position for forming in a forming mould, in a flat shape. It should be noted that this by no means limits the scope of the present invention, which equally well includes, for example, a blank pre-shaped into a three-dimensional object. For instance, the blank may be presented to the forming mould in a shape similar to the desired final shape of the object. Another embodiment could comprise a cellulose blank, which is supplied to the mould in a web on a roll.
[0067] A flat shape may refer to a generally two-dimensional (2D) shape, such as for example the shape of a blank or a sheet material, and essentially non-flat shapes may refer to any suitable three-dimensional (3D) shape. An object according to the disclosure may be made in a two-dimensional shape, a three-dimensional shape, or formed into a three-dimensional shape from a two-dimensional blank or sheet material.
[0068] Moreover, by schematically showing a coherent sheet of cellulose fibres, this will by no means limit the scope of present invention, which equally well includes, for example, blanks with loose and separated fibres applied to the forming mould.
[0069] In the present detailed description, various embodiments of the three-dimensional object to be formed and the mould to form the objects according to the present invention are mainly discussed with reference to a hollow bowl, a hollow cup or a hollow bottle, with mainly uniform thickness. It should be noted that this by no means limits the scope of the present invention, which equally well includes, for example, complex shapes with different thickness, non-hollow portions or massive objects. For instance, the object can advantageously comprise stiffeners, creases, holes, 3D shaped text, hinges, locks, threads, snaps, feet, handles or surface patterns.
[0070]
[0071]
[0072]
[0073] As is customary, the thickness of the final component 101b is uniform and consequently the thickness of the cavity t.sub.1=r.sub.b−r.sub.a between the two moulds 102a and 102b is uniform. Since conventional tools for compressing is made of stiff metal, or similar non-flexible material, and since dry cellulose fibres not behave as a pressure equalising fluid, the pressure P in said cavity will depend on the amount of present blank 101 and the local pressure generating principle.
[0074] The local pressure generating principle at pressure P.sub.2 and P.sub.5 is defined by the force F. The local pressure generating principle at P.sub.4 is defined by the geometry of the cavity and the amount of present blank 101. The local pressure P.sub.3 is determined by a combination of force and shape defined pressure generating principle.
[0075] A shape defined pressure, like P.sub.4, is highly dependent of the actual present amount of blank 101. Small and normally stochastic variations in the local material supply will drastically affect the obtained local pressure. Force defined pressure has linear gain and is a far more robust process for industrial usage.
[0076]
[0077] A force defined compressing device according to an example embodiment of the present disclosure will now be described with reference to
[0078] The forming mould 3 of this embodiment of the present disclosure uses one stiff forming mould part 2a placed under a multi-use membrane 4. The membrane 4 constitutes a seal for a pressure media or fluid 5, such as for example hydraulic oil, contained in a pressure chamber, not shown in the figure. The membrane 4, also called diaphragm, can preferably be made of rubber, silicon, elastomer or polyurethane.
[0079] Similar press devices are found in completely different industries like for example when forming metal sheets for aircrafts or processing of metallic powder into homogeneous materials. For instance, isostatic presses for conventional purposes normally uses very high pressure, such as within the range 1000-2000 bar.
[0080] The cellulose blank 1a, mainly comprising cellulose fibres with some additives and agents, has as shown in
[0081] In order to form the cellulose product, or a part of a cellulose product, from the cellulose blank 1a, the cellulose blank 1a, has to be heated to a forming temperature T.sub.1, which may be in the range 100° C. to 200° C. The forming mould part 2a may be heated to a desired temperature T.sub.2 so that heat is transferred to the cellulose blank 1a in order to achieve the forming temperature T.sub.1 of the cellulose blank 1a. The forming mould 3 may for example be pre-heated to a temperature of 150-170° C. by pumping heated oil into internal channels 7 of the forming mould part 2a. An alternative way to pre-heat the forming mould 3 is to use integrated electrical resistors, not shown in the figure. The cellulose blank 1a can also be pre-heated, for example by using infrared rays prior to tool entrance. Heating the pressure media 5 to a pressure media temperature T.sub.5 may also be a suitable alternative.
[0082] In
[0083] The compressing device may comprise a fluid control device (not shown in the figures) and may be an actuator compressing the fluid 5 or a fluid flow control device for controllable allowing pressurized fluid 5 to enter the pressure chamber having the flexible membrane 4 as a portion of a wall thereof. The apparatus may comprise the fluid 5, or the fluid 5 may be air taken from the surrounding atmosphere.
[0084] The present inventors has found that a pressure P.sub.1 of 4 MPa (40 bar) at a temperature of 160° C. when forming the cellulose product gives a fibril aggregation in the cellulose fibres that compares with many thermoplastics after 10 seconds of holding time.
[0085] In order to reduce the cycle time for industrial production of cellulose products from compressed material 1b, the cooling of said compressed material 1b may for example be done by pumping cooled oil into internal channels 7 arranged in the forming mould part 2a or into the pressure chamber wherein the forming mould part 2a temperature T.sub.2 and pressure media 5 temperature T.sub.5 quickly can be lowered after the fibril aggregation has completed in the cellulose fibres.
[0086] The process and the device will return to its open state shown in
[0087] The final thickness t.sub.1 of the cellulose product may vary slightly depending on the actual local amount of cellulose fibres.
[0088] In an alternative embodiment, a stiff forming mould part may be used instead of the flexible or pliable membrane 4, which may be suitable if different pressure levels are desired when forming the cellulose product. The use of a flexible membrane 4 may provide an isostatic compressing method resulting in a homogeneous cellulose product with high strength and short production cycle time.
[0089] One difference between the inventive compressing method and device in
[0090] Above, one example embodiment of the isostatic compressing method and device was described with reference to
[0091] Referring to
[0092] Said thin film barrier 6 may be made of a thermoplastic material like PET or PLA, having a thickness within the range 1-700 μm.
[0093]
[0094]
[0095] By holding the equal pressure P.sub.1 at the temperature T.sub.1 for a certain period of time X, the fibril aggregation in the cellulose fibres will create a bio-composite component of the compressed material 1b with mechanical properties close to thermoplastics. If as an example, the pressure P.sub.1 being 4 MPa (40 bar), the forming temperature T.sub.1 being 140° C., the temperature T.sub.2 of the forming mould part 2b being 160° C., and the time period X being 10 seconds, the bio-composite component of the compressed material 1b with mechanical properties close to thermoplastics can be achieved.
[0096] By removing the pressure media 5 and lower the pressure to atmosphere pressure P.sub.0 after the time period X the cellulose product formed by the compressed material 1b can be ejected and if needed cut to its final shape.
[0097] One advantage with the method discussed in
[0098] Turning to
[0099] In
[0100] By closing the pre-heated forming mould 3 with a closing force F.sub.c which is higher than an opening force created by the pressure P.sub.1 applied by the pressure media to the inside of the forming mould 3 by the pressure media nozzle 8 shown in
[0101]
[0102] The filling process is taking place between the steps shown in
[0103]
[0104] According to present disclosure the pressure media 9 is constituted by the beverage that is intended to be filled into the cellulose product, such as e.g. milk, juice, water and carbonated beverages.
[0105] The film barrier 6 can preferable be made of a thin thermoplastic material like PET or PLA, having a thickness in the range of 1-700 μm, wherein the film barrier 6, conventionally applied in paper packages for beverages, also seal the cellulose fibres 1b from contact with the beverage 9 during storage and usage of the cellulose product.
[0106] The cycle time for the process step shown in
[0107]
[0108] The final forming stage where fibril aggregation in the cellulose fibres of the cellulose blank 1a takes place is shown in
[0109] The embodiment of the compressing device according to
[0110] The above described examples of the compressing method, with reference to
[0111] Referring to
[0112]
[0113]
[0114] As shown in
[0115] The cavity thickness, s, between the two mould parts 2a, 2b is therefore compensated so the most narrow cavity thickness s.sub.min is situated adjacent to where the cellulose blank is thinnest t.sub.min and the most wide cavity thickness s.sub.max is situated adjacent to where the un-compressed cellulose blank 1a is thickest t.sub.max, by means of the negative pressure mould 2b, pressing the cellulose blank 1a against the forming positive mould 2a with a substantially equal forming pressure P.sub.1 acting on the cellulose blank 1a across the forming surface.
[0116] Moreover, the relation between thickness of the cellulose blank, t, and the cavity thickness, s, and the final cavity shape, is also related to the geometrical pressure generation of the cavity. The force F determines the pressure P.sub.1 on top of the positive forming mould part 2a while the convexity, thickness and angel of the cavity adjacent to the most narrow cavity thickness s.sub.min determines the final pressure P.sub.1.
[0117] The inventors of present invention have found that the final shape of the cavity is a complex algorithm t(P) in order to obtain substantially isostatic pressure P.sub.1 where both mathematical, preferably FEM-analysis, and empirical tests, preferably trial-and-error, is required to obtain equal pressure all over the component.
[0118] According to another embodiment of the present disclosure, without flexible membrane, the geometrically pressure compensated cavity in
[0119]
[0120] The preference for the method of creating isostatic pressure without flexible membrane, presented in relation to
[0121] The advantage for using the method described in relation to
[0122] As an alternative, the forming mould 3 may also be arranged with a membrane constructed as a massive flexible membrane structure. In
[0123] In an alternative embodiment, the massive flexible membrane 4 may have a varied thickness, where the massive flexible membrane is for example shaped or casted into a structure with a varied thickness. The thinner and thicker areas of the massive flexible membrane with varied thickness may compensate for areas in the forming mould parts which need smaller or bigger deformation of the membrane in order to equalize or even out the pressure subjected to the cellulose blank 1a. By using a massive flexible membrane structure the forming mould can be made cheaper and simpler in construction.
[0124] The massive flexible membrane 4 is constructed so that when the pressure, F, is applied from the forming mould parts, the massive flexible membrane 4 deforms in order to provide the isostatic pressure. The massive flexible membrane 4 may be made of a suitable elastomeric material, such as for example rubber, silicone, polyurethane or other elastomer. Due to the flexible properties of the massive flexible membrane 4, the massive flexible membrane 4 applies an isostatic pressure to the cellulose blank 1a.
[0125] In
[0126] In
[0127] In
[0128] In the claims, the word “comprising” does not exclude other elements or steps, and the indefinite article “a” or “an” does not exclude a plurality. The mere fact that certain measures are recited in mutually different dependent claims does not indicate that a combination of these measured cannot be used to advantage
[0129] It will be appreciated that the above description is merely exemplary in nature and is not intended to limit the present disclosure, its application or uses. While specific examples have been described in the specification and illustrated in the drawings, it will be understood by those of ordinary skill in the art that various changes may be made and equivalents may be substituted for elements thereof without departing from the scope of the present disclosure as defined in the claims. Furthermore, modifications may be made to adapt a particular situation or material to the teachings of the present disclosure without departing from the essential scope thereof.
[0130] Therefore, it is intended that the present disclosure not be limited to the particular examples illustrated by the drawings and described in the specification as the best mode presently contemplated for carrying out the teachings of the present disclosure, but that the scope of the present disclosure will include any embodiments falling within the foregoing description and the appended claims.
[0131] Reference signs mentioned in the claims should not be seen as limiting the extent of the matter protected by the claims, and their sole function is to make claims easier to understand.