ASSEMBLY AND METHOD FOR PRODUCING METAL POWDER
20210394267 · 2021-12-23
Inventors
Cpc classification
B22F2009/0888
PERFORMING OPERATIONS; TRANSPORTING
B22F2009/0896
PERFORMING OPERATIONS; TRANSPORTING
B22F2009/0892
PERFORMING OPERATIONS; TRANSPORTING
B07B2201/04
PERFORMING OPERATIONS; TRANSPORTING
International classification
Abstract
An assembly and method for producing powder are provided. The assembly includes a melting chamber, an atomizing vessel, and a powder processing device. The melting chamber includes a crucible, a tundish, and a filtering device. The crucible is arranged for melting a material. The crucible and tundish are configured for providing a flow path for the melted material from the crucible into the tundish. The filtering device is arranged in the flow path. The tundish is connected to an atomizing nozzle. The atomizing nozzle is configured to direct molten material from the tundish towards and into the atomizing vessel. The atomizing vessel comprises an outlet which is configured to extract solidified, atomized particles of the formerly molten material from the atomizing vessel. The powder processing device includes one or more separation units which are arranged for outputting one or more powders from the atomized particles.
Claims
1-39. (canceled)
40. An assembly for producing powder, wherein said assembly comprises: a melting chamber comprising a transfer device, a melting device and a tundish, wherein the melting device comprises a crucible for melting metal material and holding said melted metal material, wherein the transfer device is configured to position metal material into the crucible at elevated temperature, wherein the crucible is configured for providing a flow path for allowing a flow of said melted metal material from the crucible into the tundish, wherein the tundish is connected to an atomizing nozzle, wherein the melting chamber further comprises a filtering device with a filtering element which is arranged between the crucible and the tundish, wherein the filtering element is arranged in said flow path, an atomizing vessel comprising an inlet end, wherein the atomizing nozzle is configured to direct molten metal material from the tundish towards and into the inlet end of the atomizing vessel, wherein the atomizing vessel comprises an outlet opening which is configured to extract solidified, atomized particles of the formerly molten metal material from the atomizing vessel, and a powder processing device connected to the outlet opening of the atomizing vessel, wherein said powder processing device comprising multiple separation units, wherein each separation unit of said multiple separation units is configured for extracting a different fraction out of the solidified atomized particles from the atomizing vessel, wherein the different fractions comprise different weight fractions and/or different size fractions, and for providing multiple different fractions as separate products of the assembly for producing powder.
41. The assembly according to claim 40, wherein the crucible is configured for holding melted metal material with a volume in a range of approximately 10-0.1 liters.
42. The assembly according to claim 40, wherein the transfer device is configured to position a materials container into the crucible, wherein the crucible is heated at or near a melting temperature of the metal material.
43. The assembly according to claim 42, wherein the materials container comprises to be melted material, wherein the materials container is made from the same, to be melted material, or wherein the materials container is made from a combustible material.
44. The assembly according to claim 42, wherein the melting chamber comprises a storage device which is arranged for accommodating multiple materials containers inside the melting chamber, wherein the storage device is configured for subsequently presenting one materials container of said multiple materials containers to the transfer device, and/or wherein the transfer device is arranged for taking one materials container of said multiple materials containers out of the storage device.
45. The assembly according to claim 44, wherein the storage device comprises a storage turret with multiple materials container storage positions.
46. The assembly according to claim 40, wherein the assembly comprises a fluid conduit, wherein the fluid conduit debouches near and/or in the tundish for providing a substantially inert gas into the tundish
47. The assembly according to claim 40, wherein the powder processing device comprises: one or more sifting units, wherein each sifting unit of said one or more sifting units is arranged for extracting a predetermined size fraction of atomized particles; one or more cyclone separation units, wherein each cyclone separation unit of said one or more cyclone separation units is arranged for extracting a predetermined weight fraction of atomized particles; or one or more air classifiers, wherein each air classifier of said one or more air classifiers is arranged for extracting a predetermined fraction of atomized particles based on a combination of size, shape and density.
48. The assembly according to claim 40, wherein the powder processing device comprises a combining unit which is configured to combine amounts of powder from several of different fractions in order to provide a powder mixture with a preselected size and/or weight distribution.
49. The assembly according to claim 40, wherein the assembly comprises two or more powder processing devices, each powder processing device is configured for processing atomized particles of one predetermined metal or metal alloy, and wherein each of the two or more powder processing device are configured for processing atomized particles of a different metal or metal alloy.
50. The assembly according to claim 40, wherein the filtering element is configured to filter out: contaminations and/or particles with a diameter substantially equal to or larger than a diameter of the atomizing nozzle; and/or oxides, wherein said oxides comprises a different viscosity as the melted metal material.
51. The assembly according to claim 40, wherein the filtering device is coupled to the crucible, wherein the filtering element is arranged adjacent to an outflow channel of said crucible; wherein the filtering device is coupled to the tundish, wherein the filtering element is arranged in front of an input opening of said tundish; or wherein the filtering device is arranged spaced apart from the crucible and the tundish, wherein the filtering element is arranged in the flow path of the liquid material from the crucible and into the tundish.
52. The assembly according to claim 40, wherein the filtering device comprises an overflow arrangement, wherein the overflow arrangement is configured for directing at least a part of the liquid material which does not flow through the filtering element, to flow into a waste container.
53. The assembly according to claim 40, wherein the filtering device comprises a filter turret comprising multiple filtering elements, wherein the filter turret is rotatable for moving one of the multiple filtering elements into and out of the flow path of the liquid material.
54. A method for producing powder using an assembly according to claim 40, wherein the method comprises the steps of: positioning an amount of material in a hot crucible, melting the amount of material in the crucible, transferring the liquid material from the crucible to a tundish, wherein the liquid material from the crucible traverses a filtering element before the liquid material flows into the tundish, directing molten material from the tundish, via an atomizing nozzle towards and into an inlet end of an atomizing vessel in order to produce atomized particles which solidify in the atomizing vessel, extracting the solidified, atomized particles of the formerly molten material via an outlet opening of the atomizing vessel and directing said solidified atomized particles to a powder processing device, using multiple separation units of the powder processing device such that each separation unit of said multiple separation units extracts a different fraction out of the solidified atomized particles from the atomizing vessel, wherein the different fractions comprise different weight fractions and/or different size fractions and providing multiple different fractions as separate products of the assembly for producing powder.
55. The method according to claim 54, wherein the steps of the method are subsequently carried out and/or are carried out recurrently, without substantially cooling down the crucible.
56. A materials container for use in an assembly for producing powder, wherein the materials container is configured to comprise to be melted material, wherein the materials container is made from a combustible material, or wherein the materials container is made from the same, to be melted, material.
57. An assembly for producing powder, wherein said assembly comprises a melting chamber comprising a melting device, wherein the melting device comprises a receptacle and a heating device, wherein the receptacle is configured for receiving a materials container according to claim 56, wherein the melting device is configured for heating the materials container in the receptacle.
58. The assembly according to claim 57, wherein the melting device comprises a crucible, wherein the melting chamber further comprises a tundish, wherein the crucible is configured for providing a flow path for allowing a flow of melted material from the crucible into the tundish, wherein the tundish comprises an outlet, wherein the assembly further comprises: an atomizing nozzle in fluid connection with the outlet of said tundish, an atomizing vessel comprising an inlet end, wherein the atomizing nozzle is configured to direct molten material towards and into the inlet end of the atomizing vessel, wherein the atomizing vessel comprises an outlet opening which is configured to extract solidified, atomized particles of the formerly molten material from the atomizing vessel, and a powder processing device comprising one or more separation units which are arranged for outputting one or more powders from said atomized particles.
59. The assembly according to claim 58, wherein the melting chamber further comprises a filtering device which is arranged between the crucible and the tundish, wherein the filtering device is arranged in said flow path.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
[0065] The invention will be elucidated on the basis of exemplary embodiments shown in the attached drawings, in which:
[0066]
[0067]
[0068]
[0069]
[0070]
[0071]
[0072]
[0073]
[0074]
[0075]
DETAILED DESCRIPTION OF THE INVENTION
[0076]
[0077] The melting chamber 2 comprises, inter alia, a crucible 5, a tundish 6 and a filtering device 7. The crucible 5 is arranged for melting a material. In particular the crucible 5 is arranged for melting metal material for producing metal powder. The crucible 5 comprises a container 8 which is made from a ceramic material and is provided with a coil 9 for inductively heating and melting metal material inside said crucible 5. At least in use the coil 9 is connected to a power source for directing a suitable current through the coil 9 for inductively heating the metal inside the container 8. As schematically shown in the example of
[0078] The crucible 5 and tundish 6 are configured for providing a flow path for said melted material from the crucible 5 into the tundish 6. For example the crucible 5 is configured for tipping in the direction T1 of the tundish 6 and for pouring melted material from the crucible 5 into the tundish 6.
[0079] As schematically indicated in
[0080] It is noted, that in case melted material cannot pass the filtering device 7, the melting chamber 2 is provided with a flow path which directs the overflowing melted material from the filtering device 7 towards a disposal system 11. For example, the filtering device 7 may be arranged in a filter holder 7′ which substantially extends above the edge of the tundish 6 towards the disposal system 11. Accordingly, any overflowing melted material can flown over the filter holder 7′ into the disposal system 11.
[0081] It is further noted, that the crucible 5 is configured for tipping in the direction T2 towards the disposal system 11 in order to empty the crucible 5 by pouring the melted material from the crucible 5 directly into the disposal system 11. In case the melted material comprises to much irregularities or when an operator OP is of the opinion that the melted material is not suitable for producing powder, the melted material in the crucible 5 can be disposed of by pouring the melted material into the disposal system 11. The melting chamber 2 is preferably provided with observation means which allow the operator OP to view and check the melted material in the crucible 5. This observation means may comprise a camera mounted in the melting chamber 2 or, in a simple embodiment, may comprise a window 10 in a side wall of the melting chamber 2.
[0082] The tundish 6 comprises a container 12 with an opening 13 in the bottom wall, which opening 13 connects to an atomizing nozzle 14. The tundish 6 also comprises a coil 15 for resistively heating the tundish 6 and/or for inductively heating a metal inside the container 12. Also this coil 15 comprises a hollow tube which allows to provide a cooling fluid to flow through the hollow tube for cooling the coil 15 during use, in particular in case the coil 15 is used for inductively heating a metal inside the container 12. The opening 13 and the atomizing nozzle 14 usually have a small diameter and may be at least partially blocked when the melted material in the tundish 6 would comprise particles. By using the filtering device 7 for filtering the melted material before it is poured into the tundish 6, blocking of the opening 13 and/or the atomizing nozzle 14 by particles in the melted material can at least substantially be prevented.
[0083] As schematically shown in
[0084] Furthermore, the melting chamber 2 comprises a materials container 18 comprising to be melted material. The materials container 18 is connected to a manipulator device 19 which allows positioning the materials container 18 into the crucible 5, and release the materials container 18. In the schematic simplified presentation in
[0085] Alternatively, the manipulator 19 may comprises a robot arm (not shown) which allows for a more complex movement and handling of the materials containers 18, for example for moving a materials container 18 from a supply of materials containers 18 inside the melting chamber 2 into the crucible 5. After the crucible 5 has melted at least the material inside the materials container 18, and the melted material is poured out of the crucible 5, the manipulator 19 then can take a further materials container 18 from the supply of materials containers 18 and position this further materials container 18 into the crucible 5. Accordingly, as long as there are material containers in the supply of materials containers, the melting and atomizing process can continue without a need for opening the melting chamber 2.
[0086] As schematically shown in
[0087] The atomizing vessel 3 further comprises an outlet 22 which is configured to extract solidified, atomized particles of the formerly molten material from the atomizing vessel 3. In the example shown in
[0088] The fluid with solidified, atomized particles is subsequently directed to the powder processing device 4 which comprises one or more separation units which are arranged for outputting one or more powders from said atomized particles. In the example shown in
[0089] The fluid outputted at the top output 26 of the cyclone separator device 24 is directed through a filter device 27 and is expelled out of a fluid output 28 of the assembly 1. It is noted that in a further development, the fluid outputted at the fluid output 28 may be recycled and/or re-used for the above described atomizing process.
[0090] The atomized particles collected and outputted at the bottom part 25 of the cyclone separator device 24, are directed to a sifting assembly 29. In the example shown in
[0091] It is noted that in case one or more of the collected fractions of powder material is not desired or not needed for short term use, these fractions of powder material may be recycled by putting these fractions of powder material inside a materials container 18 for future use in the assembly 1 for the production of powder material.
[0092] It is noted that in the example as depicted in
[0093]
[0094] The melting chamber 41 again comprises, inter alia, a crucible 43, a tundish 44 and a filtering device 45. The crucible 43 is arranged for melting a material and is in general configured in substantially the same way as the crucible 5 of
[0095] As schematically shown in
[0096] Just as the first example in
[0097] It is noted that the crucible 43 is provided with heating elements 48 for heating and melting the to be melted material inside the crucible 43, and that the tundish 44 is provided with heating elements 49 for at least substantially preventing that the melted material inside the tundish 44 cools off.
[0098] As schematically shown in
[0099] It is noted that the atomizing nozzle 44′ and the outlet opening of the tundish 44 are connected to provide a flow passage for the melted material. The atomizing nozzle 44′ or the construction around the atomizing nozzle 44′ comprises a supporting and/or sealing member for the tundish 44, in particular for arranging the outlet opening of said tundish 44 adjacent or adjoining an inlet opening of said atomizing nozzle 44′. The atomizing nozzle 44′ and the tundish 44 in this embodiment are separate components. Preferably, the atomizing nozzle 44′ is configured so that the tundish 44 abuts the atomizing nozzle 44′ and its position with respect to the atomizing nozzle is maintained at least substantially by gravity. Accordingly the tundish 44 can easily be separated from the atomizing nozzle 44′ by lifting the tundish 44 from its support, which makes it easy to exchange the atomizing nozzle 44′ and/or the tundish 44 for a new one.
[0100] As schematically shown in
[0101] In a third example, an embodiment of the assembly for producing powder comprises a filtering device 51 which is coupled to the tundish 50. As shown in the schematic cross-section of
[0102] At each position of a filter element 52, the filter turret 53 comprises a receiving opening 54 for melted material. In use, one of the filter elements 52 is arranged facing a crucible and the melted material is poured out of the crucible into the receiving opening 54 of said one of the filter elements 52. The melted material that traverses said one of the filter elements 52 is then collected in the tundish 50. Accordingly, the one of the filter elements 52 is arranged in between the crucible and the tundish 50, in particular the one of the filtering elements 52 is arranged in the flow path of the liquid material from the crucible and into the tundish 50.
[0103] It is noted that the crucible may be arranged with respect to the tundish 50 in the same configuration as shown for example in
[0104] As schematically shown in
[0105] Furthermore, as schematically indicated in
[0106] As schematically shown in
[0107] It is noted that the tundish 50 is provided with heating elements 61 for heating the melted material inside the tundish 50 and/or for preventing that the melted material cools off too much before it flows through the opening 59.
[0108]
[0109] The melting chamber 71 again comprises, inter alia, a crucible 73, a tundish 74 and a filtering device 75.
[0110] The crucible 73 is arranged for melting a material and is in general configured in substantially the same way as the crucible 5 of
[0111] The tundish 74 is arranged directly underneath the crucible 73. In particular, the upper side of the tundish 74 is arranged directly underneath the filtering device 75 for receiving the melted material from the crucible 73 which has passed the filtering device 75. The tundish 74 is in general configured in substantially the same way as the tundish of the previous examples shown in
[0112] The example of
[0113] Just as the first example in
[0114] It is further noted that the storage container 81 for use in the assembly according to this fourth example, is provided with a central tubular opening 82 for accommodating the hollow tube 77 of the crucible 73. As schematically indicated in
[0115] All other aspects and parts of the assembly 70 for producing powder of this fourth example may be equal or corresponding to the aspects and parts of the assembly 1 for producing powder according to the first example.
[0116]
[0117] As schematically shown in
[0118] The transfer device 95 is configured for taking one of said containers 94, 94′ out of the storage device 96, and for positioning the container 94 in the receptacle 93 of the melting device 92.
[0119] In the example shown in
[0120] The crucible 92 is configured for tilting in a direction T1 towards the tundish 98 to provide a flow path for pouring melted material from the crucible 92 into the tundish 98. In addition, the crucible 92 is configured for tilting in a direction T2 towards a disposal system 101. Also a plug member 102 is provided, which plug member 102 is vertically movable for arranging a tip end 103 in the opening 99 of the tundish 98.
[0121] The assembly 90 according to this fifth example also comprises an atomizing vessel 104 and a powder processing device comprising one or more separation units, which may be equal or corresponding to the aspects and parts of the assembly 1 for producing powder according to the first example.
[0122] In particular, the melting chamber 91 may comprises a filtering device which is arranged between the crucible 92 and the tundish 98, wherein the filtering device is arranged in the flow path for pouring melted material from the crucible 92 into the tundish 98, according to any one of the previous examples.
[0123] It is noted that in the fifth example, the melting device 92 is a crucible, and the melted material inside the crucible can be visually examined, for example by an operator OP, via the window 105 in a wall of the melting chamber 91, before it is poured into the tundish 98. However, in an alternative exemplary embodiment, transfer device 95 may be configured to position the materials container 94 directly into the tundish 98. This latter example, the tundish 98 constitutes the melting device for heating and melting the material container with its material content.
[0124] The use of the materials containers 18, 81, 94, 94′ provides a major step forward in the production of powder material. The materials containers 18, 81, 94, 94′ provide a constant external shape to the material to be melted, which allows the same and easy handling for each materials container. The materials containers can be filled with to be melted material of substantially any shape, as long as it fits inside the materials container. Accordingly, it is not necessary to break or split the to be melted material into small fractions or bulk material.
[0125] In addition, due to the constant external shape, which is preferably accommodated to the internal shape of the crucible, the materials containers can be positioned in a hot crucible. This allows to use the assembly for powder production according to the present invention in repeating atomization runs in which repeatedly the following steps are performed: [0126] a. a new materials container is arranged in the hot crucible, [0127] b. after the materials container and the to be melted material therein has been melted, pouring the liquid material into the tundish, preferably via a filtering device, [0128] c. after the liquid material has been poured into the tundish, the hot crucible is filled with a new materials container (go back to step a).
[0129] For example, the to be melted material is placed in several materials containers 94, 94′. Each materials container has a volume of 1 liter and could hold about 4 to 5 kg metal material. If we have 10 materials containers 94, 94′ in a setup as for example shown in
[0130]
[0131] It is noted that an inductive heating device 114 provides heat directly to electrically conductive material, such as metal, inside the receptacle 111. Since the receptacle 111 is preferably made from a ceramic material, which preferably is not electrically conductive, the inductive heating device 114 cannot heat up the receptacle 111 when no electrically conductive material is inside. In order to heat up the receptacle 111 before liquid metal is poured into the receptacle 111, preferably via a filtering device, as described above, the receptacle is preferably provided with a secondary heating device 114′, which is preferably arranged in the side walls and/or in isolation material surrounding the side walls as schematically shown in
[0132] In an embodiment, the secondary heating device 114′ comprises an electrically conductive material, which is heated by means of the inductive heating device 114. In addition or alternatively, in an embodiment, the secondary heating device 114′ comprises a resistive heating.
[0133] As shown in
[0134] The atomizing nozzle 115 comprises a flow channel 120 which is in fluid communication with the outlet opening 113 of the receptacle 111 in order to allow melted material to flow from the receptacle 111 through the atomizing nozzle 115 to an atomizing outlet 121. The atomizing nozzle 115 is further provided with gas outlets 116 for directing gas jets onto the flow of melted material out of the atomizing outlet 121. The gas outlets 116 are arranged adjacent and at least partially surrounding the atomizing outlet 121 of the atomizing nozzle 115.
[0135] In the example showed in figured 6, the gas outlets 116 are in fluid connection with a gas reservoir 117. In use, the gas reservoir 117 is connected to a supply 119 for pressurized gas via a supply channel 118.
[0136] Furthermore, the atomizing nozzle 115 of this example is provided with an nozzle heating device 122. The nozzle heating device 122 comprises an inductive and/or resistive heating device for heating at least the flow channel 120 and/or the material inside the flow channel 120, preferably melted metal in at least the lower part of the flow channel 120. The nozzle heating device 121 comprises a coil which spirals around the flow channel 120, and which in use is connected to a power source for directing a suitable current through the coil for inductively and/or resistively heating the flow channel 120. In case the nozzle heating device 122 is configured as an inductive heating, the coil preferably comprises a hollow tube which allows to provide a cooling fluid to flow through the tube for cooling the nozzle heating device 122 during use.
[0137] Due to the nozzle heating device 122, it can substantially be prevented that the melted material in the flow channel 120 clogs up the flow channel 120 and/or the atomizing outlet 121. Without such a nozzle heating device 122, the temperature of the melted material in the flow channel 120 when traveling from the receptacle 111 to the atomizing outlet 121 may decreases. When the temperature of the melted material in the flow channel decreases, the viscosity of the melted material will increase, the flow of the melted material through the flow channel 120 will decrease further, and the temperature of the melted material will decrease even further, up to the moment that the material in the flow channel 120 is no longer flowing and the flow channel and the atomizing nozzle are blocked, which is also known as nozzle freeze.
[0138] During the atomization of a material, the liquid material flows out of the atomizing outlet 121. Various beams of pressurized gas from the gas outlets 116 blow against the liquid material below the atomizing nozzle 115, and the liquid material is atomized or nebulized to form small droplets of liquid material. The small droplets are substantially airborne, cool down and solidify to form powder.
[0139] The assembly of the present invention utilizes the fact that the liquid droplets and the resulting powder are/is airborne in the pressurized gas for transporting the powder further through the assembly for processing the powder and/or separating the powder from the gas flow. Various examples of powder processing arrangements are shown in
[0140]
[0141] As soon as the temperature of the droplets is below the melting temperature of the material, the gas with suspended solidified droplets which form the powder are guided through a heat exchange unit 132 for cooling down the powder to make it easier to process the powder downstream. In addition, active cooling the powder by the heat exchange unit 132 substantially prevents that the parts of the assembly downstream of the heat exchange unit 132 heat up to much.
[0142] Downstream the heat exchange unit 132, the airborne powder is introduced into a cyclone or air classifier 133 serving to separate powder particles from the gas, wherein the separated powder gravitates towards the downward outlet of the cyclone or air classifier 133 towards a sifting unit 134. Lightweight and small powder particles do not gravitate towards the downward outlet, but are carried away by the gas via the upper outlet towards a filtering unit 137.
[0143] In the sifting unit 134, course powder particles, which have a size bigger than the mesh size of the sieve in the sifting unit 134, are directed to a course powder particle container 136. The medium size powder particles, which have a size smaller than the mesh size of the sieve in the sifting unit 134, are directed to a medium powder particle container 135.
[0144] In the filtering unit 137, the lightweight and small particles are removed from the gas flow and are directed to a fine powder particle container 138. The filtered gas is subsequently expelled via a gas exhaust 139.
[0145]
[0146] The smaller solidified droplets, which are suspended in the turbulent gas, are removed out of the atomizing vessel 141 together with the gas at an upper outlet of the atomizing vessel and are directed to a cyclone or air classified 142. The mixture of gas with airborne solidified droplets is introduced into the cyclone or air classifier 142 serving to separate the solidified droplets from the gas, wherein the solidified droplets gravitate towards the downward outlet of the cyclone or air classifier 142 towards the intermediate buffer 143. The gas is removed out of the cyclone or air classified 142 via an upper outlet and is expelled via a gas exhaust.
[0147] In the intermediate buffer 143 the powder particles are preferably sifted in order to remove the most course particles, using a sieve with a mesh size preferably larger than 20 micro-meters, for example using a sieve with a mesh size of 200 micro-meters.
[0148] The assembly further comprises an valve 144 at the output of the intermediate buffer 143 in order to control the output of powder material from the intermediate buffer 143 to the separation units, which in this example have a dedicated gas-circuit. This dedicated gas-circuit comprises a pump 145 for generating a gas flow, which is mixed with the powder particles from the intermediate buffer 143. The gas flow transports the powder particles through a heat exchange unit 146 for cooling down the powder, and then towards a first cyclone or air classifier 147 serving to separate powder particles from the gas.
[0149] In the first cyclone or air classifier 147, a first fraction of the powder gravitates towards the downward outlet of the cyclone or air classifier 147, and is directed via an outlet valve 148 towards a sifting unit 149.
[0150] In the sifting unit 149, course powder particles, which have a size bigger than the mesh size of the sieve in the sifting unit 149, are directed to a course powder particle container 151. The medium size powder particles, which have a size smaller than the mesh size of the sieve in the sifting unit 149, are directed to a medium powder particle container 150.
[0151] Lightweight and small powder particles, which do not gravitate towards the downward outlet of the first cyclone or air classifier 147, are carried away by the gas via the upper outlet towards a second cyclone or air classifier 152. In the second cyclone or air classifier 152, a second fraction of the powder gravitates towards the downward outlet of the cyclone or air classifier 152, and is directed via an outlet valve 153 to a fine powder particle container 154.
[0152] Very lightweight and small powder particles, which do not gravitate towards the downward outlet of the second cyclone or air classifier 152, are carried away by the gas via the upper outlet towards filtering unit 155. In the filtering unit 155 substantially all remaining particles are removed from the gas flow, and the gas is directed to the inlet of the pump 145 and/or mixed with the gas from the source 140 for pressurized gas which in use supplies pressurized gas to the atomizing nozzle. Accordingly, at least a part of the gas in the dedicated gas-circuit of the separation units can be re-used.
[0153]
[0154] The smaller solidified droplets, which are suspended in the turbulent gas, are removed out of the atomizing vessel 161 together with the gas at an upper outlet of the atomizing vessel and are directed to a cyclone or air classified 162. The mixture of gas with airborne solidified droplets is introduced into the cyclone or air classifier 162 serving to separate the solidified droplets from the gas, wherein the solidified droplets gravitate towards the downward outlet of the cyclone or air classifier 162 towards the intermediate buffer 163. The gas is removed out of the cyclone or air classified 162 via an upper outlet and is expelled via a gas exhaust.
[0155] In the intermediate buffer 163 the powder particles are preferably sifted in order to remove the most course particles, using a sieve with a mesh size preferably larger than 20 micro-meters, for example using a sieve with a mesh size of 200 micro-meters.
[0156] The assembly further comprises an valve 164 at the output of the intermediate buffer 163 in order to control the output of powder material from the intermediate buffer 163 to the separation units, which in this example have a dedicated first gas-circuit. This dedicated first gas-circuit comprises a first pump 165 for generating a gas flow which is mixed with the powder particles from the intermediate buffer 163. The gas flow transports the powder particles through a heat exchange unit 166 for cooling down the powder, and then towards a first cyclone or air classifier 167 serving to separate powder particles from the gas.
[0157] In the first cyclone or air classifier 167, a first fraction of the powder gravitates towards the downward outlet of the cyclone or air classifier 167, and is directed via an outlet valve 168 towards a second gas-circuit.
[0158] Lightweight and small powder particles, which do not gravitate towards the downward outlet of the first cyclone or air classifier 167, are carried away by the gas via the upper outlet towards a second cyclone or air classifier 178. In the second cyclone or air classifier 178, a second fraction of the powder gravitates towards the downward outlet of the cyclone or air classifier 178, and is directed via an outlet valve 179 to a fine powder particle container 180.
[0159] Very lightweight and small powder particles, which do not gravitate towards the downward outlet of the second cyclone or air classifier 178, are carried away by the gas via the upper outlet towards filtering unit 181. In the filtering unit 181 substantially all remaining particles are removed from the gas flow, and the gas is directed back to the inlet of the pump 165 and/or mixed with the gas from the source 160 for pressurized gas which in use supplies pressurized gas to the atomizing nozzle.
[0160] The first fraction of powder particles from the first cyclone or air classifier 167 is directed to a second gas-circuit which comprises a second pump 169 for generating a gas flow which is mixed with the first fraction of powder particles from first cyclone or air classifier 167. The gas flow transports the powder particles towards a third cyclone or air classifier 170 serving to separate powder particles from the gas.
[0161] In the third cyclone or air classifier 170, a third fraction of the powder gravitates towards the downward outlet of the cyclone or air classifier 170, and is directed via an outlet valve 171 towards a course powder particle container 172.
[0162] Lightweight and small powder particles, which do not gravitate towards the downward outlet of the third cyclone or air classifier 170, are carried away by the gas via the upper outlet towards a fourth cyclone or air classifier 173. In the fourth cyclone or air classifier 173, a second fraction of the powder gravitates towards the downward outlet of the cyclone or air classifier 173, and is directed via an outlet valve 174 to an intermediate powder particle container 175.
[0163] Very lightweight and small powder particles, which do not gravitate towards the downward outlet of the fourth cyclone or air classifier 173, are carried away by the gas via the upper outlet towards filtering unit 176. In the filtering unit 176 substantially all remaining particles are removed from the gas flow, and the gas is directed back to the inlet of the second pump 169 and/or mixed with the gas from the source 160 for pressurized gas which in use supplies pressurized gas to the atomizing nozzle.
[0164] It is noted that the process of producing powder using an assembly according to the present invention, delivers powders with a certain particle size distribution PD, as schematically shown in
[0165] In a further exemplary embodiment as schematically shown in
[0166] In addition
[0167] From the various examples of powder processing arrangements, as for example shown in
[0168] It is noted that in case the combining unit 203 is used for the different materials, also the combining unit 203 must be cleaned when changing from the first material to the second material. Alternatively, each powder processing device 202, 202′ may comprise its own combining unit 203. In particular, the combining unit 203 may be integrated or form an integral part of the powder processing device 202, 202′.
[0169]
[0170] The melting chamber 302 comprises, inter alia, a crucible 305, a tundish 306 and a filtering device 307. The crucible 305 is arranged for melting metal material for producing metal powder. The crucible 305 comprises a container 308 which is made from a ceramic material and is provided with a coil 309 for inductively heating and melting metal material inside said crucible 305. At least in use the coil 309 is connected to a power source for directing a suitable current through the coil 309 for inductively heating the metal inside the container 308. The crucible 305 and tundish 306 are configured for providing a flow path for said melted material from the crucible 305 into the tundish 306. In particular, the crucible 305 is configured for tipping in the direction T1 of the tundish 306 and for pouring melted material from the crucible 305 into the tundish 306.
[0171] As schematically indicated in
[0172] The tundish 306 comprises a container 312 with an opening in the bottom wall, which opening connects to an atomizing nozzle 314. The tundish 306 also comprises a resistively heating device 215 for heating the tundish 306 and a material inside the container 312.
[0173] As schematically shown in
[0174] Furthermore, the melting chamber 302 comprises a materials containers 318, 318′ comprising to be melted material. The materials containers 318, 318′ are connected to a manipulator device 319 which allows positioning the materials container 318 into the crucible 305, and release the materials container 318. In addition, the manipulator 319 is configured for accommodating multiple materials containers 318′ inside the melting chamber 302, and for subsequently positioning one of said multiple materials containers 318′ into the crucible 305. After the crucible 305 has melted at least the material inside the materials container 318, and the melted material is poured out of the crucible 305 into the tundish 306, the manipulator 319 then can position a further materials container 318′ into the crucible 305. Accordingly, the melting and atomizing process can continue as long as there are materials containers 318, 318′ to be successively placed in the crucible 305. The melting chamber 302 is furthermore provided with a supply arrangement 317 for supplying further materials contains 318″ into the melting chamber 302.
[0175] The melting chamber 302 is preferably provided with observation means which allow the operator OP to view and check the process in the melting chamber 302. This observation means comprises a window 310 in a side wall of the melting chamber 302.
[0176] As schematically shown in
[0177] The atomizing vessel 321 further comprises an outlet 322 which is configured to extract solidified, atomized particles of the formerly molten material from the atomizing vessel 321. The fluid used in the atomizing process also leaves the atomizing vessel 321 via the outlet 322 and takes the solidified, atomized particles along with it towards a cyclone or air classifier 324, which separates the solidified, atomized particles from the fluid. The solidified, atomized particles gravitate towards the downward outlet of the cyclone or air classifier 324 towards a cooling member 325, and via a valve 326 and a course sieve 327, into an intermediate buffer 330. The gas is removed out of the cyclone or air classified 324 via an upper outlet and is expelled via a gas exhaust 328. The cooling member 325 is preferably a heat exchanger which is configured for cooling down the solidified, atomized particles. In the course sieve 327 the powder particles are preferably sifted in order to remove the most course particles, using a sieve with a mesh size of 200 micro-meters. The most course particles are collected and provided to a first residue container 327′.
[0178] The resulting powder in the intermediate buffer 330 is transported by a screw conveyor 331 and delivered to a gas supply line 332 towards the powder processing device 304. The gas with solidified, atomized particles is directed from the supply line 332 to a series arrangement of several filter devices 333, 335, 337, 339, preferably gas-driven sieving devices, each filtering out a predetermined size fraction from the powder, and delivering each size fraction in a corresponding container 334, 336, 338, 340.
[0179] Very lightweight and small powder particles, which pass all the filtering devices 333, 335, 337, 339, are carried away by the gas towards final filtering unit 341, for example comprising HEPA filters. In the final filtering unit 341 substantially all remaining particles are removed from the gas flow, and the gas is directed via an outlet 343 to a pump (not shown), which pump is configured for pressurizing gas and supplying the pressurized gas to the inlet 344 of the supply line 332. The remaining particles can at least partially be collected in a second residue container 342. It is noted that the gas used in the powder processing device 304 can be air, but preferably the gas is a substantially inert gas. Preferably the inert gas is selected or configured in order to at least substantially prevent contamination of the powder material and/or to at least substantially prevent chemical reactions of the powder material such as oxidation.
[0180] It is noted that the material from the first and/or second residue containers 327′, 342 can be collected and recycled by putting these inside a materials container 318″ for future use in the assembly 301 for the production of powder material.
[0181] It is to be understood that the above description is included to illustrate the operation of the preferred embodiments and is not meant to limit the scope of the invention. From the above discussion, many variations will be apparent to one skilled in the art that would yet be encompassed by the scope of the present invention.
[0182] In summary, the present invention relates to an assembly and method for producing powder. The assembly comprises:
a melting chamber comprising a crucible, a tundish and a filtering device, wherein the crucible is arranged for melting a material, wherein the crucible and tundish are configured for providing a flow path for said melted material from the crucible into the tundish, wherein the filtering device is arranged in said flow path, wherein the tundish is connected to an atomizing nozzle,
an atomizing vessel, wherein the atomizing nozzle is configured to direct molten material from the tundish towards and into the atomizing vessel, wherein the atomizing vessel comprises an outlet which is configured to extract solidified, atomized particles of the formerly molten material from the atomizing vessel, and
a powder processing device comprising one or more separation units which are arranged for outputting one or more powders from said atomized particles.