DIRECT REDUCTION SHAFT FURNACE WITH PROBE FOR MEASURING INTERIOR GAS ANALYSIS

Abstract

A direct reduction shaft furnace having at least one probe disposed vertically within the reduction zone thereof. The probe preferably extends from the top to the bottom of the reduction zone. The probe allows for gas sampling along the length thereof and transmittal of the gas to at least one type of gas analysis device. The probe may also allow for the measurement of the temperature and pressure of the gas sample as it is taken.

Claims

1-15. (canceled)

16. An apparatus for the direct reduction of metal ore, the apparatus comprising: a vertical shaft furnace, the shaft furnace having a metal ore reducing zone; at least one probe for sampling gas from within the reduction zone of said vertical shaft furnace; the at least one probe being disposed vertically within the reduction zone and extending through the entire reduction zone; the probe comprising a plurality of sampling pipes, each sampling pipe having an upper portion and an end portion, the sampling pipes being disposed within at least one support pipe.

17. The apparatus as recited in claim 16 wherein the support pipe encases and supports a portion of the upper portion of all of the sampling pipes.

18. The apparatus as recited in claim 17 wherein the end portion of each of the sampling pipes is configured to allow for intake of a gas sample therethrough.

19. The apparatus as recited in claim 18 wherein the end portion of each of the sampling pipes further includes a thermocouple to measure a temperature of the gas sample.

20. The apparatus of claim 19 wherein the sampling pipes are each of different length and extend down through the reduction zone different distances so as to allow for intake of samples from different depths in said reduction zone.

21. The apparatus as recited in claim 17 wherein each of said sampling pipes: are the same length as a rest of the sampling pipes; has a gas intake port disposed through the wall thereof at a different position along a length thereof than the rest of the sampling pipes, the gas intake port configured to allow for intake of a gas sample therethrough; has the end portion thereof closed off to prevent gas from entering therethrough.

22. The apparatus as recited in claim 21 wherein each of the sampling pipes further includes a thermocouple disposed adjacent the gas intake port to measure a temperature of the gas sample.

23. The apparatus as recited in claim 22 wherein: a first of the sampling pipes is concentrically nested within the support pipe, the first sampling pipe being longer than and having an end portion protruding from the support pipe; each subsequent one of the sampling pipes being concentrically nested within a previous of the sampling pipes and being longer than the previous sampling pipe so as to have an end portion protruding from the previous sampling pipe.

24. The apparatus as recited in claim 23 wherein the end portion of each of said sampling tubes is configured to allow for intake of a gas sample therethrough.

25. The apparatus as recited in claim 24 wherein the end portion of each of the sampling pipes includes a thermocouple disposed therein to measure a temperature of the gas sample.

26. The apparatus as recited in claim 15 further comprising a gas analysis system.

27. The apparatus as recited in claim 26 wherein the gas analysis system includes a gas cooling system to cool the gas sample before compositional analysis.

28. The apparatus as recited in claim 27 wherein the gas analysis system further includes a gas compositional analyzer.

29. The apparatus as recited in claim 28 wherein said gas compositional analyzer includes a mass spectrometer.

30. The apparatus as recited in claim 28 wherein the gas analysis system further includes a gas pressure measurement system.

Description

BRIEF DESCRIPTION OF THE DRAWINGS

[0015] FIG. 1 is a schematic depiction of a vertical shaft type furnace into which the present gas analysis probe may be installed;

[0016] FIG. 2A is a cross section across the diameter of a first embodiment of the probe 6 used in the present invention;

[0017] FIG. 2B is a side view of the first embodiment of the probe 6;

[0018] FIG. 2C is a 3D perspective view of the first embodiment of the probe 6;

[0019] FIG. 3 is a side view of A second embodiment of the probe 6;

[0020] FIG. 4 depicts a side view of another embodiment of a probe 6 for use in the present invention;

[0021] FIG. 5 is a 3D perspective view of a telescoping embodiment of a probe 6 for use in the present invention;

[0022] FIG. 6 shows a schematic depiction of a probe 6 which is disposed vertically within the reduction zone and connected to a temperature measurement system, and a gas analysis system.

DETAILED DESCRIPTION OF THE INVENTION

[0023] The present invention relates to a DR shaft furnace having at least one probe disposed vertically within the reduction zone thereof. The probe preferably extends from the top to the bottom of the reduction zone. The probe allows for gas sampling along the length thereof and transmittal of the gas to at least one type of gas analysis device and to a pressure measurement instrument. The probe may also allow for the measurement of the temperature of the gas sample as it is taken. Thus, the inventive combination of the DR furnace and the probe allows for the taking of gas samples and temperatures at different levels inside of the furnace. The probe can be installed vertically at one or more locations along the diameter of DR shaft furnace.

[0024] Different depictions of a first embodiment of the probe 6 used in the present invention is shown in FIGS. 2A-2C. This embodiment has separate gas sampling pipes 8 that have different lengths and a supporting pipe 7. In this embodiment, all of the gas sampling pipes 8 are longer than the support pipe 7. Gas samples are drawn into the sampling pipe through the open end thereof. A thermocouple (shown schematically in FIG. 6) may be stationed at the open end of each sampling pipe 8. This allows for a temperature profile measurement of the reduction zone of the DR furnace and indicates the temperature of the gas as taken for analysis. In this embodiment, all of the sampling pipes 8 are all of different lengths in order to take gas samples all along the reduction zone. FIG. 2A is a cross section across the diameter of the first embodiment of the probe 6. FIG. 2B is a side view of the first embodiment of the probe 6. Finally, FIG. 2C is a 3D perspective view of the first embodiment of the probe 6.

[0025] In another embodiment there may be multiple support tubes 7. FIG. 3 is a side view of this second embodiment of the probe 6. Two or more support pipes 7 may hold the sampling pipes 8. There may be gaps between support tubes 7′ and 7″ and a sampling tube 8 may terminate in this gap to take samples at this level in the reduction zone. Again, thermocouples (shown schematically in FIG. 6) may be stationed at the open end of each sampling pipe 8.

[0026] FIG. 4 depicts yet another embodiment of a probe 6 for use in the present invention. In this embodiment, there is a single support pipe 7 and all of the sampling pipes 8 are about the same length. Each sampling pipe 8 has a sampling port 9 at a different location thereon so as to allow for gas samples to be taken along the entire reduction zone. As discussed above, thermocouples (shown schematically in FIG. 6) may be installed in each sampling pipe 8 adjacent to the sampling port 9.

[0027] FIG. 5 depicts a telescoping embodiment of a probe 6 for use in the present invention. In this embodiment, the sampling pipes 8 are concentrically nested in a telescoping fashion within the support pipe 7. Thus, a first sampling pipe 8 is concentrically nested within the support pipe 7. The first sampling pipe 8 being longer than and protruding from the support pipe 7. Next another sampling pipe 8 is concentrically nested within the first sampling pipe. This concentric nesting is continued with additional sampling pipes 8 to provide as many gas sampling pipes 8 as is necessary or desired to sample the entire reduction zone. Each additional sampling pipe 8 being longer than and protruding from the previous sampling port in which it is nested. As the other embodiments, thermocouples (shown schematically in FIG. 6) may be installed at the terminal (gas sampling) end of each sampling pipe 8.

[0028] The support pipes 7 and sampling ports 8 are formed of material selected to be suitable at the high temperature condition and corrosive atmosphere of the DR furnace.

[0029] In general, the probe 6 is designed to take gas samples at different levels inside of the DR furnace reduction zone, as well as (optionally) measuring the temperature. Gas samples will be used for gas analysis, and pressure measurement. The probe 6 may be installed vertically in up to 5 different locations along the diameter of DR shaft furnace reduction zone.

[0030] FIG. 6 shows a schematic depiction of a shaft furnace probe 6 with a schematic depiction of a temperature measurement system, and a gas analysis system attached thereto. The gas analysis system includes gas transmission lines 14, a gas cooling apparatus 10 which cools the gas samples. The gas samples are then directed to both a gas compositional analyzing system 11, and a gas pressure measuring system 12. The temperature measuring system 13 includes thermocouples/transmission lines 15.

[0031] The sample analysis system 11 may include a mass spectrometer or laser/infrared analyzer.

[0032] The probe 6 may be fixed to the furnace roof. The fixation may be accomplished by, for example, employing a welded flange at the top of the probe 6. The pipes (support 7 and sampling 8) may be welded together along their length to give higher mechanical strength and resistance to bending and fracture.