PROCESS FOR THE RECOVERY OF AT LEAST ONE FRACTIONAL SUBSTANCE FROM VAPOURS DURING ALCOHOL REDUCTION OF A BEVERAGE, AND FRACTIONAL SUBSTANCE RECOVERY DEVICE

Abstract

Process for recovering at least one fractional substance from vapours during the alcohol reduction of a beverage, and fractional substance recovery device for carrying out the process, in which an alcoholic beverage to be reduced in alcohol content is supplied to a degasser of a fractional substance recovery device, in which vapours are removed from the degasser and the alcoholic beverage passed through the degasser is supplied to a device for alcohol reduction, in which the vapours are fed to a plurality of fractional condensation stages which follow one another in series and in which at least one fractional substance is separated from the vapours under pressure and/or temperature, and in which the fractional substances separated in the respective fractional condensation stage are collected in a collecting container or are fed to an inoculation station, through which the separated fractional substances are fed in metered quantities to an alcohol-reduced drink.

Claims

1. Process for recovering at least one fractional substances from vapours during the alcohol reduction of a beverage, in which an alcoholic beverage is supplied to a degasser of a fractional substance recovery apparatus, in which vapours are removed from the degasser and the alcoholic beverage passed through the degasser is fed to a device for reducing alcohol, in which the vapours are fed to a plurality of fractional condensation stages which follow one another in series and in which at least one fractional substance is separated from the vapours under pressure and/or temperature, and in which the fractional substances separated in the respective fractional condensation stage are collected in a collecting container or fed to a inoculation station, through which one or several separated fractional substances are fed in dosed form to a reduced-alcohol beverage.

2. Process according to claim 1, wherein in the fractional condensation stage the supplied vapours are pressurized via a pump, preferably vacuum pump, and subsequently cooled with at least one cooler, in particular heat exchanger, and subsequently at least one fractional substance is separated via a separator .

3. Process according to claim 1, wherein the vapours are pressurized with increasing pressure in the fractional condensation stages following one another in series .

4. Process according to claim 1, wherein in a first fractional condensation stage the vapours are compressed from 100 mbar to 1.5 to 2 bar.

5. Process according to claim 1, wherein in a second fractional condensation stage, which is connected downstream of the first condensation stage, the remaining vapours are compressed from 1.5 to 2 bar to an increased pressure of 3 to 5 bar.

6. Process according to claim 1, wherein in a third fractional condensation stage the remaining vapours of 3 to 5 bar are compressed to an increased pressure.

7. Process according to claim 1, wherein before the alcohol reduction of the alcoholic beverage, the vapours of the alcoholic beverage are removed.

8. Process according to claim 1, wherein the fractional substances separated by the fractional condensation stages are fed through the inoculation station to an alcohol-reduced beverage which is finished by the alcohol reduction apparatus and has been discharged from the alcohol reduction process.

9. Process according to claim 1, wherein in the inoculation station the amount of the separated fractional substances from the fractional substance recovery device, which are supplied to the finished alcohol-reduced beverage, are selected and adjusted.

10. A fractional substance recovery device for recovering at least one fractional substance from vapours during alcohol reduction of a beverage, with a degasser, with a plurality of fractional condensation stages arranged in series one after the other, which are connected downstream of the degasser, wherein at least one line extending through the fractional condensation stages is provided, and each condensation stage comprises at least one fractional substance which is discharged through the at least one separator .

11. Fractional substance recovery device according to claim 10, wherein the at least one fractional condensation stage comprises at least one pump, and downstream thereof at least one cooler, and downstream thereof at least one separator (-75).

12. Fractional substance recovery device according to claim 10, wherein at least two coolers are provided in a fractional condensation stage and downstream of each cooler at least one separator for the at least one fractional substance is provided.

13. Process according to claim 3, wherein vapours are pressurized with increasing pressure in the fractional condensation stages following one another in series and are cooled to a constant temperature range of the fractional condensation stages before leaving the respective condensation stage.

14. Process according to claim 4, wherein in the first fractional condensation stage the vapours are cooled to a temperature of 40° C. to 50° C.

15. Process according to claim 5, wherein in the second fractional condensation stage, which is connected downstream of the first condensation stage, the remaining vapours are cooled to a temperature of 5° C. to 10° C.

16. Process according to claim 6, wherein in the third fractional condensation stage the remaining vapours are cooled to a temperature of 5° C. to 10° C.

17. Fractional substance recovery device according to claim 10, wherein the at least one fractional condensation stage comprises at least one vacuum pump and downstream thereof at least one heat exchanger.

Description

[0018] The invention as well as other advantageous designs and further developments of the same are described and explained in more detail below on the basis of the examples shown in the drawings. The features to be taken from the description and the drawings can be applied individually on their own or in combination with each other. It is shown:

[0019] FIG. 1 a schematic view of a device for the production of reduced-alcohol beverages, and

[0020] FIG. 2 is a schematic view of a fractional substances recovery device.

[0021] A device 10 for the production of reduced-alcohol beverages comprises a heat exchanger 12, to which steam at a temperature of, for example, 110° C. is fed via a line 11 to a first circuit. In the second circuit of the heat exchanger a line 13 is provided leading to a separator 14. From the bottom of the separator 14 a line 16 emerges, which carries the non-alcoholic beverage. The non-alcoholic beverage is preferably wine or beer. In the outlet line there is a heat exchanger 17, which cools down the temperature of the finished product and serves the heat economy. In addition, line 16 contains a cooler 18, which cools the finished product down to, for example, 5° C. Finally, there is an inoculation station 19, which is fed with fractional substances that are separated from vapours of the alcoholic beverage by a fraction recovery device 60 (FIG. 2). This is explained below. Downstream of the inoculation station 19 is a storage container 21 for receiving the finished product, i.e. the reduced-alcohol or dealcoholised beverage, which is enriched with fractional substances via the inoculation station 19.

[0022] Starting from the head of the separator 14, a line 22 runs which carries warm, nonseparated vapours and leads to the lower part of a tower 23, which forms a rectifier. From the bottom 24 of the tower 23 there is a line 26 leading to the second circuit of the heat exchanger 12. This circuit is thus closed.

[0023] The beverage to be dealcoholised or reduced in its alcohol content, such as wine, beer or sparkling wine, is stored in a storage tank 27. From the storage tank 27, a line 61 leads to the fractional material recovery device 60. This line 61 leads in particular to a degasser 62 of the fractional material recovery device 60. From the degasser 62, a line 28 leads to a heat exchanger 17 in the second circuit of the device. Via line 28 the alcoholic beverage, which is reduced by vapours by the degasser 62, is preferably fed to a heat exchanger not shown in detail, whereby the beverage is cooled down before the beverage is fed in the centre of the tower 23. In tower 23, which is preferably made of stainless steel, a higher first packing 29 and a second packing 31 are provided. The two packings are spaced apart. Packing 29 has a distance from the inlet of line 22 and thus also a considerable distance from the bottom 24.

[0024] Line 28 enters between the two packings 29, 31. Packing 31 has a distance from the head 32 of the tower. A line 33 of considerable diameter leaves the upper part of the head 32, which carries vapours containing alcohol, fragrances and aromas. The temperature in head 32 is, for example, 30° C. This corresponds to about 44 mbar. The temperature in tower 23 above floor 24, for example, is 39° C., so that a pressure of 70 mbar is present. In the steady state of the rectifier, line 33 carries 80% of the alcohol, whereby “alcohol” is always understood to mean “ethyl alcohol”. Line 33 leads to a condenser 34, which is fed via line 36 with cooling water obtained by ambient cooling and evaporation cooling. Heated water is discharged through one line 37.

[0025] In the condenser 34, the vapours fed to the head are not yet condensed, which is why the condenser 34 is fed via a line 38 to a cooler 39. Its cooling system is supplied with ice water via a pipe 41. A vacuum line 42 leads into the head of the cooler 39, which is connected to a vacuum pump 43 and which also generates the vacuum present in tower 23. From the bottom of the cooler 39, a line 44 exits, which carries liquefied alcohol, fragrances, aromas, higher alcohols in liquid form, with a concentration not exceeding 82%. The percentage may be between 20 and 80 % depending on the dealcoholisation effort. The liquid is fed by a pump 46 to head 32 at a level not exceeding the outlet of line 33 and above the second package 31.

[0026] Parallel to line 44, a line 47 leaves the bottom of the cooler. This line carries the alcohol that is not needed for feedback and is finally discharged, which is pumped to an alcohol tank by a pump 48.

[0027] A controller 51 determines the quantity ratio in lines 44 and 47. When the device 10 is started up, line 47 remains closed at first due to its action, and this until the alcohol content in lines 44, 33, 38 has reached the desired level, e.g. 80 %. The regulator 51 prevents a further increase of the alcohol content by releasing line 48, to the extent that it is guaranteed that it maintains the desired level on the feedback path of the alcohol percentage.

[0028] FIG. 2 shows a schematic enlargement of the fractional substance recovery device 60. The line 61 leads the alcoholic beverage from the storage tank 27 to the degasser 62. From an underside of the degasser 62 the degassed alcoholic beverage is fed via a pump 63 through the line 28 to the heat exchanger 17. Vapours of the alcoholic beverage are removed from the degasser 62. These vapours are available in gas or vapour form. For example, they can have a temperature of 40 to 50 C°. The vapours comprise water, aromas, fragrances, CO2 and alcohol.

[0029] The vapours are fed via line 64 to one or more fractional condensation stages 66, 67, 68 connected in series. In this embodiment, the fractional substances recovery device 60 comprises, for example, the three functional condensation stages 66, 67, 68 shown. There may be fewer or more such fractional condensation stages.

[0030] The fractional condensation stages 66, 67, 68 are preferably of the same design. For this reason, the structure of the fractional condensation stage 66 is described, which also applies to the others. Therefore, the same reference numbers were used for the same components.

[0031] On the inlet side a pump 71, especially a vacuum pump, is provided by which the supplied vapours are compressed. Subsequently, the compressed vapours are cooled by one or more successive coolers 72, 73, especially heat exchangers. The compressed and cooled vapours are then fed to a separator 75, which has a line 76, via which the fractional substance separated in the respective fractional condensation stage is discharged. The separated fractional substances can be fed into one or each of the separate collection containers 84, 85 or collection containers for any further use or the inoculation station 19. The remaining vapours are fed via line 77 to a subsequent fractional condensation stage.

[0032] If only one fractional condensation stage is provided, the separator 75 can be omitted so that line 77 leads directly to the inoculation station 19.

[0033] With the fractional substance recovery device 60 shown, water and alcohol can be separated in the first fractional condensation stage 66 due to compression of the vapours to, for example, 1 to 2 bar and subsequent cooling to, for example, 40° C. to 50° C., and discharged into a waste or collection container via line 76.

[0034] In a subsequent second fractional condensation stage 67, the remaining vapours, which have been reduced in terms of water and alcohol, are further compressed, for example to 3 to 5 bar, and then cooled with one or more coolers 72, 73. At least one fragrance or aroma can be removed from the separator 75 via a line 78, which can be fractionated at these set conditions within the condensation stage. This fragrance or aroma can be fed to the injection station 19 or also collected in a collecting tank 86. Via the separator 75 downstream of the second cooler 73, a further fraction can be fed to the inoculation station 19 or a collecting tank 87. Via line 77, the remaining vapours are fed, for example, to a third fractional condensation unit 68. By means of the pump 71 a compression to e.g. 10 to 12 bar can be achieved. In the separator 75 separated fractional substances, e.g. from the first and second cooler 72, 73 can be fed via line 79, 83 to the inoculation station 19 or a collecting container 88. 89. For example, CO2 or slightly enriched CO2 may remain in the third fractional condensation stage, which can be fed via line 77 to the inoculation station 19.

[0035] By means of the described fractional substance recovery device 60, a specific separation of individual fractional substance from the vapours can be controlled depending on the number of fractional condensation stages. These can be optionally returned to the reduced-alcohol or dealcoholised beverage or disposed of. In particular, a recirculation of CO2 and/or aroma substance is provided for. This allows an enrichment of taste and/or a minimisation of CO2 pollution.