Process for fabricating a photonic chip via transfer of a die to a receiving substrate
11320592 · 2022-05-03
Assignee
Inventors
Cpc classification
H01S5/1032
ELECTRICITY
International classification
Abstract
The invention relates to a process for fabricating a photonic chip including steps of transferring a die to an actual transfer region of the receiving substrate comprising a central region entirely covered by the die and a peripheral region having a free surface, a first waveguide lying solely in the central region, and a second waveguide lying in the peripheral region; depositing an etch mask on a segment of the die and around the actual transfer region; and dry etching a free segment of the die, the free surface of the peripheral region then being partially etched.
Claims
1. A process for fabricating a photonic chip comprising at least one optoelectronic component placed on a receiving substrate and optically coupled to a first integrated waveguide and a second integrated waveguide, the first integrated waveguide being located in the receiving substrate at a depth smaller or equal to a threshold value, the second integrated waveguide being located in the receiving substrate at a depth larger than the threshold value, the process comprising the following steps: defining an actual transfer region on an upper face of the receiving substrate in which a die of the optoelectronic component is to be entirely located, the transfer region comprising: a central region having predefined dimensions Lc, lc in a plane of the receiving substrate, said central region being configured to be entirely covered by the die following a step of transferring the die to the receiving substrate, and a peripheral region surrounding the central region and configured to be partially covered by the die following the transferring step due to a positioning uncertainty, the actual transfer region having predefined dimensions preset on the basis of the dimensions Lc, lc and of the positioning uncertainty; producing the die, with initial dimensions that are preset on the basis of the dimensions Lc, lc and of the positioning uncertainty; producing the receiving substrate comprising: the first integrated waveguide, which lies solely in the central region; and the second integrated waveguide, which is superposed on and optically coupled to the first integrated waveguide; transferring the die to the actual transfer region of the receiving substrate, the central region then being entirely covered by the die and the peripheral region including a first free surface not covered by the die; depositing an etch mask, on the one hand on a segment of the die, and on the other hand around the actual transfer region, the peripheral region including a second free surface not covered by the etch mask; and producing the optoelectronic component from the die, by dry etching of a free segment of the die that is not coated by the etch mask, the second free surface of the peripheral region being etched to a depth smaller than or equal to the threshold value.
2. The fabricating process according to claim 1, wherein the first integrated waveguide has a first spacing, with respect to the upper face, smaller than the threshold value.
3. The fabricating process according to claim 1, wherein the receiving substrate comprises a third integrated waveguide, which is superposed on and optically coupled to the second integrated waveguide, and which lies outside of the actual transfer region and has a third spacing, with respect to the upper face, smaller than the preset threshold value PA.
4. The fabricating process according to claim 1, wherein, following the step of producing the die, the die has initial dimensions at least equal to Lc+2d.sub.ip, lc+2d.sub.ip, respectively.
5. The fabricating process according to claim 1, wherein the actual transfer region has dimensions at least equal to Lc+4d.sub.ip, lc+4 d.sub.ip, respectively.
6. The fabricating process according to claim 1, comprising, before the step of producing the optoelectronic component, a step of removing a growth substrate of the die by wet etching, the wet etching resulting in lateral over-etching of the die in a plane parallel to the receiving substrate over a nonzero distance, the die then having initial dimensions that are furthermore preset on the basis of the nonzero distance.
7. The fabricating process according to claim 1, comprising a step of producing a plurality of optoelectronic components from the same die, each optoelectronic component being coupled to a corresponding first integrated waveguide.
8. The fabricating process according to claim 1, wherein the optoelectronic component is a laser diode, a photodiode or an electro-optical modulator.
9. The fabricating process according to claim 1, wherein the die is made based on a III-V semiconductor compound.
10. The fabricating process according to claim 1, the optoelectronic component being a DFB laser diode, a Bragg mirror being placed in the first integrated waveguide.
11. The fabricating process according to claim 1, the optoelectronic component being a DBR laser diode, two Bragg mirrors bounding an optical cavity of the laser diode and being placed in second integrated waveguides that are each superposed on and optically coupled to one end of said first integrated waveguide.
12. The fabricating process according to claim 1, comprising fabricating a plurality of photonic chips from the same receiving substrate.
13. The fabricating process according to claim 1, wherein producing the optoelectronic component comprises etching the receiving substrate excluding any region of the receiving substrate directly overlying any portion of the first integrated waveguide.
14. The fabricating process according to claim 1, comprising forming the second integrated waveguide with a second spacing with respect to the upper face larger than the first spacing.
15. The fabricating process according to claim 14, comprising forming a third integrated waveguide having a third spacing with respect to the upper face is larger than the first spacing.
16. The fabricating process according to claim 15, wherein the third integrated waveguide has at least a portion located in the central region.
17. The fabricating process according to claim 15, wherein the third integrated waveguide has at least a portion located within the central region to overlap with the first integrated waveguide.
18. The fabricating process according to claim 1, wherein the second integrated waveguide has at least a portion located within the central region.
19. The fabricating process according to claim 1, wherein the second integrated waveguide has at least a portion located within the central region to overlap with the first integrated waveguide.
20. The fabricating process according to claim 1, wherein the first and second integrated waveguides are not etched during the dry etching.
21. The fabricating process according to claim 1, comprising: removing a substrate of the die including over-etching a lateral portion of the die, the second free surface including a portion of the upper face of the receiving substrate exposed during the over-etching.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
(1) Other aspects, aims, advantages and features of the invention will become more clearly apparent on reading the following detailed description of preferred embodiments thereof, which description is given by way of nonlimiting example, with reference to the appended drawings, in which:
(2)
(3)
(4)
(5)
(6)
DETAILED DESCRIPTION OF PARTICULAR EMBODIMENTS
(7) In the figures and in the rest of the description, elements that are identical or similar have been referenced with the same references. In addition, the various elements are not shown to scale for the sake of clarity of the figures. Moreover, the various embodiments and variants are not exclusive of one another and may be combined together. Unless otherwise indicated, the term “substantially”, “about” and “of” the order of mean to within 10%, and preferably to within 5%. Moreover, the terms “comprised between . . . and . . . ” and equivalents are to be understood inclusive of limits, unless otherwise indicated.
(8) The invention relates to a process for fabricating one or more photonic chips from a given die transferred to a functionalized receiving substrate.
(9) A photonic chip is an optoelectronic device comprising at least one optoelectronic component resting on a receiving substrate and optically coupled to an integrated waveguide located in the receiving substrate. This waveguide forms one portion of an integrated photonic circuit.
(10) The die comprises a semiconductor segment intended to allow the one or more optoelectronic components to be produced, this semiconductor segment being obtained by epitaxy from a growth substrate. The die may have initial dimensions (Lv.sup.(i), lv.sup.(i)) in a plane parallel to the receiving substrate of the order of 1 to several square millimetres, and a thickness of the order of a few tens to a few hundred microns. Here, the length of the die will be denoted L and its width 1. The die may have a polygonal initial shape, a square or rectangular shape for example, or a circular or oval shape.
(11) The optoelectronic component may notably be a laser diode or a photodiode. It is made based on a semiconductor, i.e. it mainly comprises the semiconductor in question. In may thus comprise a stack of thin layers made of various semiconductor compounds containing the semiconductor. Preferably, the optoelectronic component is of III-V type, and may be made based on InP or GaAs. The die is then referred to as a III-V die. The optoelectronic component may comprise a heterostructure formed from an n-doped layer, from a p-doped prayer, and from an intermediate active layer containing quantum wells.
(12) The receiving substrate is said to be functionalized in the sense that it comprises at least one waveguide integrated into the substrate, i.e. produced on or under the upper face of the receiving substrate. It may also comprise other passive optical components (multiplexers or demultiplexers, fibre-optic couplers, etc.) and/or active optical components (modulators, etc.), optically coupled to one another so as to form the integrated photonic circuit. The receiving substrate may be an SOI substrate, i.e. it may comprise a thin layer of silicon and a carrier substrate made of silicon, between which is inserted an oxide layer referred to as the BOX (for buried oxide). The thin silicon layer may be covered with a thin layer allowing the die to be bonded to the upper face of the receiving substrate, for example an oxide layer in the case of bonding by molecular adhesion.
(13) Generally, the photonic chip may be a transmitter Tx in which may be found laser diodes each coupled to one integrated waveguide, and, for example, modulators, at least one multiplexer, and a coupler to an optical fibre. The photonic chip may also be a receiver Rx comprising a coupler, a demultiplexer, and photodiodes. It may also be a transceiver comprising both laser diodes and photodiodes. In the rest of the description, purely by way of illustration, the photonic chip is a transmitter comprising at least one laser diode made of a III-V compound, said laser diode being optically coupled to a first waveguide of an integrated photonic circuit, this waveguide being integrated into a receiving substrate made based on silicon, for example of SOI type.
(14) Moreover, the fabricating process employs at least one step of structuring the die by dry etching, so as to produce the one or more optoelectronic components. The dry etching consists in ion bombardment of the free surface of the die, i.e. the surface not protected by an etch mask (also known as a hard mask). It is essentially a physical etch that therefore has a highly anisotropic character. It may thus, for example, be a question of reactive ion etching (RIE) or of inductively coupled plasma RIE (ICP-RIE).
(15)
(16) An orthogonal three-dimensional direct coordinate system XYZ, in which the XZ-plane is a plane parallel to the plane of the receiving substrate 20, the Z-axis is oriented along the longitudinal axis of the integrated waveguide 23, the X-axis is oriented along the width of the waveguide 23, and the Y-axis is oriented from the receiving substrate 20 toward the die 10, is defined here and will be referred to in the rest of the description.
(17) With reference to
(18) The die 10 has initial dimensions (Lv.sup.(i), lv.sup.(i) in the XZ-plane, i.e. an initial length Lv.sup.(i) along the Z-axis and an initial width lv.sup.(i) along the X-axis. These initial dimensions (Lv.sup.(i), lv.sup.(i) here depend on a lateral over-etch d.sub.sgl of the die 10, which occurs during the removal of the growth substrate 11 by wet etching, and on desired final dimensions (Lv.sup.(f), lv.sup.(f) of the die 10. The final dimensions (Lv.sup.(f), lv.sup.(f) correspond to the dimensions of the die 10 before the step of dry etching carried out to form the optoelectronic component. By way of example, the desired final dimensions (Lv.sup.(f), lv.sup.(f)) are 1×1 mm.sup.2 and the lateral over-etch d.sub.sgl is here of the order of 100 μm. Thus, the initial dimensions (Lv.sup.(i), lv.sup.(i)) are here at least equal to 1.2×1.2 mm.sup.2. Final dimensions (Lv.sup.(f), lv.sup.(f) of 1×1 mm.sup.2 notably allow a plurality of ridge laser diodes to be produced from the same die 10, as notably indicated in document WO2018/087485A1, each laser diode for example having a wavelength of about 800 μm, a width of about 50 μm, with an inter-diode spacing of about 200 μm.
(19) With reference to
(20) Moreover, a target transfer region Zr.sub.c is defined on the upper face 20a of the receiving substrate 20, in which region the die 10 is intended to be located after the transferring step. This target transfer region Zr.sub.c here has dimensions identical to the initial dimensions (Lv.sup.(i), lv.sup.(i)) of the die 10. The integrated waveguide 23 extends continuously through and out of the target transfer region Zr.sub.c.
(21) With reference to
(22) With reference to
(23) With reference to
(24) With reference to
(25) The inventors have observed that the positioning uncertainty d.sub.ip of the die 10 may lead to a local structural degradation of the integrated waveguide 23 in the target transfer region Zr.sub.c. Specifically, in this example, the free surface 25 of the receiving substrate 20 may be etched to a depth P.sub.sgv the value of which notably depends on the operating conditions of the etch and on the nature of the etched materials. It may be seen that the value P.sub.sgv of this vertical over-etch may be larger than the spacing e.sub.gap between the waveguide 23 and the upper face 20a of the receiving substrate 20. The depth P.sub.sgv of the vertical over-etch may reach a value of about 75 nm, and thus lead to at least partial etching of the integrated waveguide 23 when the spacing e.sub.gap is smaller than this value P.sub.sgv. Said integrated waveguide thus undergoes a local structural degradation that may lead to a decrease in the performance of the photonic chip 1. Moreover, this local deterioration of the integrated waveguide 23 may be accentuated when the fabricating process comprises at least one additional step of dry etching, for example during the structuring of the n-doped InP semiconductor layer 14. A new vertical over-etch of the receiving substrate 20, for example of a value of about 75 nm, may then occur, aggravating the local degradation of the structure of the integrated waveguide 23.
(26) Moreover, as illustrated in
(27) A process for fabricating a photonic chip 1 according to one embodiment will now be described with reference to
(28) With reference to
(29) It is desired for the die 10, after the step of removing the growth substrate 11 by wet etching, to have final dimensions at least equal to (Lc, lc). The target transfer region Zr.sub.c therefore corresponds to the central region Zc increased by a distance d.sub.sgl related to the lateral over-etch that occurs during the wet etching of the growth substrate 11. This target transfer region Zr.sub.c is therefore centred on the central region Zc and has dimensions (Lr.sub.c, lc) at least equal to (Lc+2d.sub.sgl, lc+2d.sub.sgl).
(30) To take into account the positioning uncertainty of the die 10 about the target transfer region Zr.sub.c, which is of a value d.sub.ip here equal to 300 μm, the die 10 has initial dimensions (Lv.sup.(i), lv.sup.(i)) at least equal to (Lr.sub.c+2d.sub.ip, lr.sub.c+2d.sub.ip), and therefore at least equal to (Lc+2d.sub.sgl+2d.sub.ip, lc+2d.sub.sgl+2d.sub.ip), i.e. here at least equal to 1.8×1.8 mm.sup.2. It is therefore possible to define an actual transfer region Zr.sub.e (also called effective transfer region Zr.sub.e) as being the region in which the die 10 will be entirely located after the transferring step, given the positioning uncertainty d.sub.ip about the target transfer region Zr.sub.c. This actual transfer region Zr.sub.e is therefore centred on the central region Zc and has dimensions (Lr.sub.e, lr.sub.e) at least equal to (Lc+2d.sub.sgl+4d.sub.ip, lc+2d.sub.sgl+4d.sub.ip), i.e. here at least equal to 2.4×2.4 mm.sup.2.
(31) In other words, the actual transfer region Zr.sub.e is the region of the receiving substrate 20, encircling the central region Zc, to which the die 10 will actually be transferred given the predefined positioning uncertainty d.sub.ip and here the predefined lateral over-etch d.sub.sgl related to the wet etch of the growth substrate 11. The die 10 will therefore be entirely located in this actual transfer region Zr.sub.e, in the sense that it will not be partially located outside of this region Zr.sub.e.
(32) In addition, the transfer of a die 10 of initial dimensions (Lv.sup.(i), lv.sup.(i)) defined beforehand to the actual transfer region Zr.sub.e allows it to be ensured that the central region Zc will indeed be entirely covered by the die 10 after the transferring step, and here also after the step of wet etching the growth substrate 11. In other words, the central region Zc will not comprise a free surface not covered by the die 10. The central region Zc is delineated by a peripheral border that is at a distance of a value d.sub.sgl+2d.sub.ip from the peripheral border of the actual transfer region Zr.sub.e.
(33) The peripheral region Zp is the area of the actual transfer region Zr.sub.e that encircles the central region Zc. It is therefore intended to be only partially covered by the die 10 after the transferring step. Thus, it is intended to have a so-called free surface 25, i.e. a surface that is not covered by the die 10, which will be subjected to a vertical over-etch of a preset threshold depth P.sub.th, in the step or steps of dry etching employed by the fabricating process.
(34)
(35)
(36)
(37) With reference to
(38) With reference to
(39) The first waveguide 23, which is intended to be optically coupled to the optoelectronic component, lies, in the XZ-plane, solely in the central region Zc. In other words, it does not extend into the peripheral region Zp. Because of its arrangement in the XZ-plane, and despite a potentially small spacing e.sub.gap.sup.(1) with respect to the upper face 20a of the receiving substrate 20, which spacing is defined so as to optimize the optical coupling to the laser diode, it will not experience a local structural degradation by the vertical over-etching of the receiving substrate 20, no matter what the actual transfer position of the die 10 in the region Zr.sub.e as a result of the predefined positioning uncertainty d.sub.ip, and no matter what the potential lateral over-etch of predefined value d.sub.sgl during the wet etching of the growth substrate 11. Specifically, it is not located in the peripheral region Zp and is therefore safe from the vertical over-etch related to the dry etching.
(40) The second waveguide 24 is superposed, along the Y-axis, on the first waveguide 23, and is optically coupled thereto. It lies, in the XZ-plane, at least in the peripheral region Zp. It here also extends, on the one hand, out of the transfer region Zr, and on the other hand, also into the central region Zc over a distance allowing the optical coupling to the first waveguide 23 to be optimized. Because of its spacing e.sub.gap.sup.(2), which is larger than the threshold value P.sub.th, and despite lying in the peripheral region Zp, it is safe from the vertical over-etch of the receiving substrate 20. P.sub.th is defined as being the maximum value of the cumulative vertical over-etch undergone in the peripheral region Zp as a result of the one or more various steps of dry etching employed in the fabricating process.
(41) With reference to
(42) With reference to
(43) With reference to
(44) With reference to
(45) In so far as the peripheral region Zp has a free surface 25, the dry etching results in vertical over-etching of the free surface 25 of the receiving substrate 20 over a distance P.sub.sgv.sup.(a). In this example, the fabricating process comprises two steps of dry etching, which each lead to a vertical over-etch of values P.sub.sgv.sup.(a) and P.sub.sgv.sup.(b). Thus, the threshold value P.sub.th is here substantially equal to the sum of P.sub.sgv.sup.(a) and of P.sub.sgv.sup.(b). The threshold value P.sub.th may be substantially equal to 150 nm, when P.sub.sgv.sup.(a) and P.sub.sgv.sup.(b) are each of the order of 75 nm.
(46) However, in so far as the first waveguide 23 is located solely in the central region Zc, it is not damaged by the vertical over-etch P.sub.svg.sup.(a) because it is protected by the presence of the die 10. Furthermore, in so far as the second waveguide 24 is located in the peripheral region Zp but with a spacing e.sub.gap.sup.(2) larger than P.sub.th, it is also not damaged by the vertical over-etch P.sub.sgv.sup.(a), which is in sufficient to reach it.
(47) With reference to
(48) With reference to
(49) With reference to
(50) The dry etching causes further vertical over-etching of the free surface 25 of the receiving substrate 20, of a value P.sub.sgv.sup.(b), this over-etch adding to the preceding vertical over-etch a value P.sub.sgv.sup.(a). The vertical over-etch of the free surface 25 of the peripheral region Zp of the receiving substrate 20 then reaches the threshold value P.sub.th.
(51) However, in so far as the first waveguide 23 is solely located in the central region Zc, it is not damaged by this new vertical over-etch of value P.sub.sgv.sup.(b). Furthermore, in so far as the second waveguide 24 is located in the peripheral region Zp with a spacing e.sub.gap.sup.(2) larger than P.sub.th, it is also not damaged by this vertical over-etch of value P.sub.sgv.sup.(b).
(52) Thus, the fabricating process makes it possible to prevent the one or more various dry etches employed, which induce a vertical over-etch of the free surface 25 of the receiving substrate 20, from degrading the integrated waveguide, and in particular the first and second integrated waveguides. The performance of the photonic chip 1 is therefore maintained.
(53) Particular embodiments have just been described. Various variants and modifications will appear obvious to those skilled in the art.
(54) Thus, a given die 10 may allow a plurality of laser diodes to be produced. By way of example, each laser diode may be a ridge diode, or even a vertical-cavity surface-emitting laser (VCSEL).
(55) The fabricating process may allow a plurality of photonic chips to be produced on the same receiving substrate 20. It then comprises a step of dicing the receiving substrate 22 to singulate the photonic chips.
(56) In the example of
(57) In the case where the optoelectronic component is a laser diode, it may be hybrid and then comprise reflectors bounding the optical cavity of the laser source located in the receiving substrate 20. Thus, in the case of a distributed-Bragg-reflector (DBR) laser, the optical cavity is bounded by two Bragg gratings located in the first waveguide 23, or as a variant in the second (or third) waveguide. More precisely, two second waveguides are optically coupled to the first waveguide 23, and each comprise one Bragg mirror. In the case of a distributed-feedback (DFB) laser, a given Bragg grating extends, in the first waveguide 23, over the entire length of the optical cavity.