METHODS OF HIGH THROUGHPUT HYDROCOLLOID BEAD PRODUCTION AND APPARATUSES THEREOF
20230249146 · 2023-08-10
Inventors
Cpc classification
B01J19/285
PERFORMING OPERATIONS; TRANSPORTING
B01J2/08
PERFORMING OPERATIONS; TRANSPORTING
International classification
B01J2/08
PERFORMING OPERATIONS; TRANSPORTING
B01J13/00
PERFORMING OPERATIONS; TRANSPORTING
B01J19/00
PERFORMING OPERATIONS; TRANSPORTING
Abstract
A method of creating hydrocolloid beads includes forcing a hydrocolloid gel suspension through a plurality of nozzles, wherefrom the hydrocolloid gel forms into a plurality of gel drops and fall into a reactant bath. The drops are exposed to the reactant bath for a predetermined period of time, wherein the drops form firm or semi-firm beads as they remain in the reactant bath. The firm or semi-firm beads are removed from the reactant bath, rinsed, and dried.
Claims
1. A method of creating hydrocolloid beads, the method comprising: forcing a hydrocolloid gel suspension through a plurality of nozzles, wherefrom the hydrocolloid gel forms into a plurality of gel drops and fall into a reactant bath; exposing the drops to the reactant bath for a predetermined period of time, wherein the drops form firm or semi-firm beads as they remain in the reactant bath; removing the beads from the reactant bath; rinsing the beads; and drying the beads.
2. The method of claim 1, wherein the hydrocolloid gel suspension has a viscosity within a range of 2,000 and 20,000 centipoise at room temperature.
3. The method of claim 1, wherein the reactant bath contains calcium ions (Ca2+), potassium ions (K+), and/or magnesium ions (Mg2+).
4. The method of claim 1, wherein the reactant bath has a temperature within a range of 60 and 180° F.
5. The method of claim 1, wherein removing the beads from the reactant bath comprises separating the beads from deionized reactant.
6. The method of claim 5, wherein the beads are separated from the deionized reactant with a vibrating screen.-.
7. The method of claim 5, further comprising introducing the deionized reactant to the reactant bath.
8. The method of claim 7, further comprising adding ions to the deionized reactant and/or the reactant bath.
9. The method of claim 1, wherein the predetermined period of time is between 1 minute and 10 minutes.
10. The method of claim 1, wherein the bath is maintained at a temperature within the range of 60 to 165° F.
11. The method of claim 1, wherein the beads have a pH within a range of 3.0 to 6.0.
12. The method of claim 1, wherein the beads are pasteurized at a temperature of at least 250° F.
13. The method of claim 1, wherein the beads have a size of between 1 mm and 5 mm.
14. The method of claim 1, wherein the beads have a viscosity of between 2,000 and 10,000 centipoise.
15. The method of claim 1, wherein the beads contain 0-10% protein and between 70% and 98% water.
16. A device for creating hydrocolloid beads, the device comprising: a delivery system configured to dispense gel drops into a reactant bath platform, wherein the reactant bath platform comprises a tray that contains a reactant solution, the tray arranged so as to allow the gel drops to be exposed to the reactant solution for a predetermined time to allow the gel drops to form semi-firm or firm beads, wherein the reactant bath platform further includes an exit port through which the semi-firm or firm beads may exit the tray; a rinse platform configured to capture the semi-firm or firm beads as they exit the reactant bath platform; a sprayer positioned to spray the semi-firm or firm beads on the rinse platform with a rinse; a dryer positioned to blow warm, dry air on the rinsed beads; at least one gate, wherein the at least one gate is configured to form a barrier across a portion of a width of the tray; and a gap formed in a portion of the gate.
17. The device of claim 16, wherein the rinse consists of water.
18. The device of claim 16, wherein the rinse comprises water and at least one of: oil; salts, lecithin, and preservatives.
19. The device of claim 16, further comprising a pump positioned to pump the semi-firm or firm beads from the exit port to the rinse platform.
20. A device for creating hydrocolloid beads, the device comprising: a delivery system configured to dispense gel drops into a reactant bath platform, wherein the reactant bath platform comprises a tray that contains a reactant solution, the tray arranged so as to allow the gel drops to be exposed to the reactant solution for a predetermined time to allow the gel drops to form semi-firm or firm beads, wherein the reactant bath platform further includes an exit port through which the semi-firm or firm beads may exit the tray; and a rinse platform configured to capture the semi-firm or firm beads as they exit the reactant bath platform; a sprayer to spray the semi-firm or firm beads on the rinse platform with a rinse; a dryer positioned to blow warm, dry air on the rinsed beads; wherein a base of the tray further comprises at least one of: an inclined surface and a conveyor system.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
[0011] The present disclosure makes reference to the accompanying drawings. In the drawings, like reference numbers indicate identical or functionally similar elements. The drawings are not necessarily drawn to scale.
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DETAILED DESCRIPTION
[0021] The presently disclosed devices and methods will now be described more fully in detail with reference to the accompanying drawings, in which some embodiments of the present disclosure are shown. This disclosure should not, however, be construed as limited to the embodiments set forth herein; rather, they are provided so that this disclosure will be complete and will fully convey the scope of the inventive subject matter to those skilled in the art.
[0022] High-throughput methods of creating hydrocolloid beads and devices for practicing the disclosed method will now be described. In use, the methods are capable of generating millions of firm or semi-firm hydrocolloid beads per minute. In some embodiments, the presently disclosed methods are capable of producing at least forty (40) pounds of beads every two (2) minutes.
[0023] In some embodiments, the presently disclosed methods use a dispensing apparatus to dispense drops of a hydrocolloid gel suspension into a reactant bath. In some embodiments, the hydrocolloid gel suspension is forced through a plurality of nozzles using a pressured line. As the gel suspension exits the nozzles, it forms drops by natural force (e.g., gravity) and/or mechanical force (e.g., shearing the gel suspension via nozzle vibration, a spinning disk, or a spinning wire). The drops them enter the reactant bath. Once the drops are in the bath, they are guided down an inclined tray, chute, or conveyor in the reactant bath for a predetermined amount of time, during which the drops of gel form into firm or semi-firm beads. The time the gel droplets are left in the bath may vary from a little as a few seconds to as long as five minutes, with the beads continuing to harden over as they dwell in the bath. When the beads reach the end of the conveyor they exit the bath and enter a drainage basin. Once the beads have exited the bath they are rinsed at least one time with water or with a water salt solution (optionally containing one or more preservatives) and then packed for storage and/or transportation. In some instances, depending on the intended use of the end user, the beads are packed into a brine solution or dried.
[0024] The hydrocolloid gel suspension may have a viscosity that ranges from 0-5,000 centipoise, in some embodiments. The hydrocolloid gel suspension may be heated or, alternatively, may be used as a cold gel suspension. The gel suspension may include a single hydrocolloid or a combination of hydrocolloids, such as sodium alginate, pectin, gellan gum, k-carrageenan, xanthan gum, and/or locus bean gum.
[0025] In embodiments in which a reactant bath is used to form the hydrocolloid beads and/or the hydrocolloid gel suspension, The process may be performed at ambient or heated temperatures. The heating process may, in some cases, partially or fully pasteurize the resulting hydrocolloid beads. Without wishing to be bound by theory, heating the hydrocolloid material(s) may result in at least partial pasteurization. In these and other embodiments, the hydrocolloid beads may be packed in a brine solution or optionally be pasteurized after formation, if desired. Numerous configurations and variations of hydrocolloid bead formation and either concurrent or subsequent stabilization are possible and contemplated herein.
[0026] The composition of the hydrocolloid gel suspension may vary based on the intended use of the end user. In some embodiments, the hydrocolloid gel suspension may be a relatively simple solution containing at least 90% by volume of water and up to 10% by volume hydrocolloid. In these and other embodiments, the gel suspension may also contain a humectant such as sorbitol, corn syrup, erythritol, glycerin, and/or other humectants. If present, humectants may occupy up to 30% of the total volume of the suspension. In certain situations, the gel suspension may contain up to 20% carbohydrates and/or 50% protein. In select embodiments, the gel suspension may include some combination of water, protein and carbohydrates in a ratio of, for example, 70%/20%/10% by volume, respectively. If present, the carbohydrates may be derived from corn syrup, sugar, high fructose corn syrup, sorbitol, erythritol, honey, molasses, and/or another carbohydrate source that is soluble in water. The protein source may be individual amino acids or complete protein sources such as fish protein, or other soluble proteins such as pea, soy, wheat, casein, and/or whey.
[0027] The reactant bath may consist of distilled water in some embodiments. However, in other embodiments, the reactant bath may include ions, such as K+, Ca2+, and/or Mg2+. In select embodiments, the reactant bath uses calcium chloride or calcium acetate as an ion source. The reactant bath may also contain a preservative, such as potassium sorbate, in some embodiments.
[0028] After the beads exit the bath, any remaining reactant may be removed from the beads by either shaking the beads and/or rinsing the beads. After reactant removal, the beads may be packaged with a brine solution, sprayed or otherwise exposed to a solution that may contain lecithin, preservatives, salts, and/or oils to coat the beads. The coated beads may be dried, in some embodiments, to achieve a desire moisture content ranging from 0% to 95%. There are a number of suitable methods for drying the coated beads, such as, for example, using a conventional conveyor dryer having a length of 5 feet to 20 feet. Conventional dryers have known ways to modify the extent of the drying to reach a desired moisture content.
[0029] The fully formed and ready to use beads can be between 0.100 mm and 5 mm in size and may contain up to 98% water. In some embodiments, the beads may have a moisture content of 70-95%. As noted, the beads may also contain up to 20% carbohydrates and 50% protein or some combination of water, protein and carbohydrates. In select embodiments, the beads contain 70% water, 20% protein, and 10% carbohydrates by volume.
[0030]
[0031] The delivery system 10, shown in
[0032] A pumping system 16 may include a conventional pump, which may be any suitable pump such as a peristaltic pump, positive displacement pump, or a pressurized pumping system.
[0033] The pumping system 16 forces the deliverable solution through a first delivery tube 42 to one or more valves 44. The valves 44 may be any suitable valve, for example, a solenoid valve. One or more secondary delivery tubes 46 connects the valve 44 to the manifolds 12. A pressure gauge 47 may be included to measure pressure as the deliverable solution is delivered to the manifold. The pumping system may also include a safety pressure release valve that releases pressure in the event the pressure in the first delivery tube 42 exceeds a preset level.
[0034] The bath platform 60, best shown in
[0035] Following entry into the bath platform 60, in the illustrated embodiment, the soft beads begin to flow down the tray 62 at a rate dictated by the incline of the tray 62 and the flow of the reactant bath. The gates 66 form a barrier across a majority of the width of the tray 62, with a slight separation or gap G from a sidewall on one end of the tray or a cutout formed in the gate 66. The side of the opening alternates from one gate 66 to the next such that the beads traverse back and forth across the width of the tray as they descend. One having ordinary skill in the art will recognize different tray 62 constructs for passing the beads around or through the gates 66 to force the beads to move from one side of the tray 62 to the other, slowing the descent, and all such constructs are within the scope of the present application. After passing the final gate 66 the reactant bath and the beads fall through the exit port 68 where the beads are captured in a drainage and rinse basin 80 and the reactant solution falls into the recirculation system 72. In another embodiment, the gates 66 may be removed and the length of the tray 62 extended to as to extend the amount of time it takes for the beads to reach the end of the tray 62.
[0036] The recirculation system illustrated in
[0037] The exit port 68 deposits the beads onto the rinse platform 80. As illustrated in
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[0039]
[0040] The hydrocolloid gel suspension may contain any desired nutrients and/or additives. For example, in some embodiments, the hydrocolloid gel suspension may contain one or more plant-based and/or animal-based proteins. In select embodiments, the hydrocolloid gel suspension may contain one or more isolate proteins (e.g., wheat protein, soybean protein, pea protein, and/or other plant-based protein). The hydrocolloid gel suspension may have a viscosity within the range of 2,000 and 20,000 centipoise (e.g., 4,000 – 15,000 centipoise, or 5,000 – 10,000 centipoise) at room temperature.
[0041] Method 200 also includes exposing the drops to the reactant bath for a predetermined period of time, wherein the drops form firm or semi-firm beads as they remain in the reactant bath (Block 204). In some embodiments, the predetermined period of time the drops are exposed to the reactant bath is between one (1) minute and ten (10) minutes. In select embodiments, the drops may be exposed to the reactant bath for between two (2) and (8) minutes, or, in some cases, approximately five (5) minutes. The reactant bath may contain calcium ions (Ca2+), potassium ions (K+), and/or magnesium ions (Mg2+). The reactant bath may be kept at room temperature or above room temperature, as desired. If the reactant bath is kept at or rear room temperature, probiotics may be included in the hydrocolloid gel suspension and in the resulting beads. In some cases, the reactant bath has a temperature within a range of 60 and 180° F. In select embodiments, the reactant bath may have a temperature within a range of 60 to 90° F.
[0042] Method 200 further includes removing the beads from the reactant bath (Block 206). In some cases, removing the beads from the reactant bath is accomplished by separating the beads from deionized reactant, for example, using a vibrating and rotating drum. If desired, gravity and a mesh screen may be used to collect and dry the beads.
[0043] Method 200 also optionally includes, in some embodiments, reintroducing deionized reactant back into the reactant bath (Block 208). If deionized reactant is reintroduced, additional ions can be added to the reactant and/or the reactant bath to ensure a sufficient quantity of ions is available to aid in gel formation. Method 200 may be carried out, in some embodiments, at a temperature within the range of 60 to 165° F. In select embodiments, method 200 may be carried out at a temperature within the range of 60 to 90° F.
[0044] The beads formed by method 200 may have numerous desirable qualities. For example, the beads may have a substantially uniform cross-section with no discernable outer skin. The beads may also have a squishy (sponge-like) texture and be resistant to syneresis. The beads may have any desired size, such as between 1 mm and 5 mm, in some embodiments. The beads may have a viscosity of between 2,000 and 10,000 centipoise, such as between 4,000 and 8,000 centipoise, or approximately 5,000 centipoise, in some embodiments. The beads may have a pH of between 3.0 and 6.0, such as between 3.5 and 5.5, in some cases.
[0045] The beads may contain any desired amounts and ratios of nutrients. For example, in some embodiments, the beads may contain at least 1% protein and between 70% and 95% water. In some embodiments, the beads may contain between 2% and 10% protein and 80% to 95% water. The beads may contain a colorant, if desired.
[0046] It is understood that the embodiments described herein are merely illustrative of the present disclosure. Variations in the process and/or the construction of the device may be contemplated by one skilled in the art without limiting the intended scope of the inventive subject matter herein disclosed and as defined by the following claims.