SPECIAL CONTROLLED-RELEASE BACTERIAL FERTILIZER FOR PEANUTS AND PREPARATION METHOD THEREOF
20220127204 · 2022-04-28
Assignee
Inventors
- Jialei ZHANG (Jinan, Shandong, CN)
- Xinguo LI (Jinan, Shandong, CN)
- Shubo WAN (Jinan, Shandong, CN)
- Feng GUO (Jinan, Shandong, CN)
- Jianguo WANG (Jinan, Shandong, CN)
- Zheng ZHANG (Jinan, Shandong, CN)
- Gao CHEN (Jinan, Shandong, CN)
- Chaohui TANG (Jinan, Shandong, CN)
- Sha YANG (Jinan, Shandong, CN)
- Zhenying PENG (Jinan, Shandong, CN)
- Jingjing MENG (Jinan, Shandong, CN)
Cpc classification
C05G5/30
CHEMISTRY; METALLURGY
C05G5/30
CHEMISTRY; METALLURGY
C05G3/60
CHEMISTRY; METALLURGY
C05F1/005
CHEMISTRY; METALLURGY
C05G3/40
CHEMISTRY; METALLURGY
C05F11/08
CHEMISTRY; METALLURGY
C05F11/08
CHEMISTRY; METALLURGY
C05F11/02
CHEMISTRY; METALLURGY
C05F11/02
CHEMISTRY; METALLURGY
International classification
C05G3/60
CHEMISTRY; METALLURGY
C05G3/40
CHEMISTRY; METALLURGY
Abstract
The invention relates to the technical field of agricultural planting, in particular to a controlled-release bacterial fertilizer for peanuts and a preparation method of the special controlled-release bacterial fertilizer. The special controlled-release bacterial fertilizer is composed of an inner layer and an outer layer; after the outer layer is released completely, the inner-layer network structure gradually absorbs water and preserves moisture, and has good slow release and controlled release properties, thereby achieving the gradual release of the inner layer, high fertilizer utilization rate, exerting the efficacy of the microbial agent and facilitating the large-area promotion.
Claims
1. A controlled-release bacterial fertilizer for peanuts, characterized in that wherein the bacterial fertilizer is composed of an inner layer and an outer layer; the outer layer: 20-40 parts of fulvic acid, 10-30 parts of chitin, 5-20 parts of alginic acid, 10-12 parts of rice husk carbon, 8-10 parts of cellulose, 0.5-0.8 part of glucolactone, 10-15 parts of sodium carboxymethyl starch, 10-20 parts of modified starch, 3-5 parts of calcium chloride, 100-200 million/g of bacillus subtilis, 50-100 million/g of bacillus gelatinosus, 100-200 million/g of bacillus thuringiensis, 50-100 million/g of bacillus laterosporus, 50-100 million/g of bacillus mucilaginosus, 50-100 million/g of streptomyces, and 50-100 million/g of Aspergillus niger; the inner layer: 10-30 parts of urea formaldehyde powder, 15-20 parts of polyethylene glycol, 30-40 parts of natto powder, 10-30 parts of fulvic acid, 10-30 parts of chitin, 5-20 parts of alginic acid, 100-200 million/g of bacillus subtilis, 80-120 million/g of bacillus gelatinosus, 100-200 million/g of bacillus thuringiensis, 50-100 million/g of bacillus laterosporus, 50-100 million/g of paecilomyces lilacinus, 100-200 million/g of Trichoderma aureoviride, 50-100 million/g of streptomyces, and 100-200 million/g of Aspergillus niger.
2. The controlled-release bacterial fertilizer for peanuts according to claim 1, wherein the relative molecular weight of the cellulose is 80000-100000.
3. A method for preparing the controlled-release bacterial fertilizer for peanuts according to claim 1, wherein the method comprises the following steps: (1) uniformly mixing urea formaldehyde powder, polyethylene glycol and ⅓ weight of natto powder in the inner layer, evenly stirring, and then adding 1-fold weight of water, heating to 95° C., stirring for 1 h, then adding the remaining natto powder, evenly mixing, then carrying out ultrasonic treatment for 20 min, cooling to 38° C., adding fulvic acid, chitin, alginate and active bacteria, then pelletizing and drying to obtain an inner core layer; and (2) adding water whose weight is 2 times those of carboxymethyl starch sodium and modified starch into the carboxymethyl starch sodium and modified starch in the outer layer, then heating to 70-80° C., adding calcium chloride, evenly stirring, then adding rice husk carbon and cellulose, evenly stirring, cooling to room temperature, adding the active bacteria, spraying the previously obtained mixture on the inner core layer at room temperature and then drying the prepared particles at low temperature.
Description
DESCRIPTION OF THE EMBODIMENTS
[0020] The technical solution of the disclosure will be further explained and illustrated through embodiments.
Example 1
[0021] A special controlled-release bacterial fertilizer for peanuts:
[0022] The outer layer: 30 kg of fulvic acid, 22 kg of chitin, 12 kg of alginic acid, 12 kg of rice husk carbon, 8 kg of cellulose (relative molecular weight is 80000-100000), 0.5 kg of glucolactone, 15 kg of sodium carboxymethyl starch, 15 kg of modified starch, 5 kg of calcium chloride, 200 million/g of bacillus subtilis, 100 million/g of bacillus gelatinosus, 150 million/g of Bacillus thuringiensis, 80 million/g of Bacillus laterosporus, 80 million/g of Bacillus mucilaginosus, 50 million/g of streptomyces and 80 million/g of Aspergillus niger.
[0023] The inner layer: 24 kg of urea formaldehyde powder, 15 kg of polyethylene glycol, 40 kg of natto powder, 20 kg of fulvic acid, 20 kg of chitin, 20 kg of alginic acid, 200 million/g of bacillus subtilis, 100 million/g of Bacillus gelatinosus, 150 million/g of Bacillus thuringiensis, 80 million/g of Bacillus laterosporus, 80 million/g of Bacillus mucilaginosus, 80 million/g of paecilomyces lilacinus, 200 million/g of Trichoderma harzianum, 100 million/g of Trichoderma aureoviride, 50 million/g of streptomycete and 80 million/g of Aspergillus niger.
[0024] The preparation method is as follows:
[0025] (1) The urea formaldehyde powder, polyethylene glycol and 1/3 weight of natto powder in the inner layer were evenly mixed, and then 1-fold weight of water was added, the above materials were heated to 95° C. and stirred for 1 h. Then, the remaining natto powder was added. The mixture was evenly stirred and subjected to ultrasonic treatment for 20 min, cooled to 38° C., fulvic acid, chitin, alginic acid and active bacteria were added, and then the above mixture was pelletized and dried to obtain a core inner layer;
[0026] (2) Water whose weight was twice those of sodium carboxymethyl starch and modified starch was added in sodium carboxymethyl starch and modified starch in the outer layer, the above materials were heated to 70-80° C., and calcium chloride was added. After the above materials were evenly stirred, rice husk carbon and cellulose were added. The above materials were evenly stirred and cooled to room temperature, the active bacteria were added, the above mixture was sprayed to the inner core layer under room temperature, and then the prepared particles were dried at low temperature.
Example 2
[0027] A special controlled-release bacterial fertilizer for peanuts:
[0028] The outer layer: 20 kg of fulvic acid, 30 kg of chitin, 12 kg of alginic acid, 12 kg of rice husk carbon, 10 kg of cellulose (relative molecular weight is 80000-100000), 0.8 kg of glucolactone, 10 kg of sodium carboxymethyl starch, 20 kg of modified starch, 3 kg of calcium chloride, 100 million/g of bacillus subtilis, 100 million/g of Bacillus gelatinosus, 100 million/g of Bacillus thuringiensis, 100 million/g of Bacillus laterosporus, 100 million/g of Bacillus mucilaginosus, 50 million/g of Streptomyces and 100 million/g of Aspergillus niger.
[0029] The inner layer: 10 kg of urea formaldehyde powder, 18 kg of polyethylene glycol, 30 kg of natto powder, 30 kg of fulvic acid, 10 kg of chitin, 18 kg of alginic acid, 100 million/g of bacillus subtilis, 100 million/g of Bacillus gelatinosus, 100 million/g of Bacillus thuringiensis, 100 million/g of Bacillus laterosporus, 100 million/g of Bacillus mucilaginosus, 50 million/g of paecilomyces lilacinus, 150 million/g of Trichoderma harzianum, 200 million/g of Trichoderma aureoviride, 50 million/g of streptomycete and 100 million/g of Aspergillus niger.
[0030] The preparation method is the same as that in example 1.
Example 3
[0031] A special controlled-release bacterial fertilizer for peanuts:
[0032] The outer layer: 40 kg of fulvic acid, 10 kg of chitin, 20 kg of alginic acid, 10 kg of rice husk carbon, 8 kg of cellulose (relative molecular weight is 80000-100000), 1 kg of glucolactone, 10 kg of sodium carboxymethyl starch, 20 kg of modified starch, 4 kg of calcium chloride, 200 million/g of bacillus subtilis, 100 million/g of Bacillus gelatinosus, 200 million/g of Bacillus thuringiensis, 100 million/g of Bacillus laterosporus, 50 million/g of Bacillus mucilaginosus, 100 million/g of Streptomyces and 100 million/g of Aspergillus niger.
[0033] The inner layer: 30 kg of urea formaldehyde powder, 20 kg of polyethylene glycol, 35 kg of natto powder, 30 kg of fulvic acid, 30 kg of chitin, 10 kg of alginic acid, 200 million/g of bacillus subtilis, 100 million/g of Bacillus gelatinosus, 200 million/g of Bacillus thuringiensis, 100 million/g of Bacillus laterosporus, 50 million/g of Bacillus mucilaginosus, 100 million/g of Paecilomyces lilacinus, 100 million/g of Trichoderma harzianum, 200 million/g of Trichoderma aureoviride, 100 million/g of streptomycete and 100 million/g of Aspergillus niger.
[0034] The preparation method is the same as that in example 1.
Example 4
[0035] The formula of a special controlled-release bacterial fertilizer for peanuts is the same as that in example 1.
[0036] The preparation method is as follows:
[0037] (1) The urea formaldehyde powder, polyethylene glycol and natto powder in the inner layer were evenly mixed, and then 1-fold weight of water was added, and the above materials were heated to 95° C. and stirred for 1 h. The mixture was evenly mixed and subjected to ultrasonic treatment for 20 min and cooled to 38° C., fulvic acid, chitin, alginic acid and active bacteria were added, and then the above mixture was pelletized and dried to obtain a core inner layer;
[0038] (2) Water whose weight was twice those of sodium carboxymethyl starch and modified starch was added in sodium carboxymethyl starch and modified starch in the outer layer, the above materials were heated to 70-80° C., and calcium chloride was added. After the above materials were evenly stirred, rice husk carbon and cellulose were added. The above materials were evenly stirred and cooled to room temperature, the active bacteria were added, the above mixture was sprayed to the inner core layer under room temperature, and then the prepared particles were dried at low temperature.
Comparative Example 1
[0039] A special controlled-release bacterial fertilizer for peanuts:
[0040] The outer layer: 30 kg of fulvic acid, 22 kg of chitin, 12 kg of alginic acid, 20 kg of rice hull carbon, 0.5 kg of glucolactone, 15 kg of sodium carboxymethyl starch, 15 kg of modified starch, 5 kg of calcium chloride, 200 million/g of bacillus subtilis, 100 million/g of Bacillus gelatinosus, 150 million/g of Bacillus thuringiensis, 80 million/g of Bacillus laterosporus, 50 million/g of Bacillus mucilaginosus, 50 million/g of Streptomyces and 80 million/g of Aspergillus niger.
[0041] The inner layer: 24 kg of urea formaldehyde powder, 15 kg of polyethylene glycol, 1 kg of polyglutamic acid, 20 kg of fulvic acid, 20 kg of chitin, 10 kg of alginic acid, 200 million/g of bacillus subtilis, 100 million/g of Bacillus gelatinosus, 150 million/g of Bacillus thuringiensis, 80 million/g of Bacillus laterosporus, 80 million/g of Bacillus mucilaginosus, 80 million/g of Paecilomyces lilacinus, 200 million/g of Trichoderma harzianum, 100 million/g of Trichoderma aureoviride, 50 million/g of streptomycete and 80 million/g of Aspergillus niger.
Comparative Example 2
[0042] A special controlled-release bacterial fertilizer for peanuts:
[0043] The outer layer: 30 kg of fulvic acid, 22 kg of chitin, 12 kg of alginic acid, 20 kg of cellulose (relative molecular weight is 80000-100000), 0.5 kg of glucolactone, 15 kg of sodium carboxymethyl starch, 15 kg of modified starch, 5 kg of calcium chloride, 200 million/g of bacillus subtilis, 100 million/g of Bacillus gelatinosus, 150 million/g of Bacillus thuringiensis, 80 million/g of Bacillus laterosporus, 50 million/g of Bacillus mucilaginosus, 50 million/g of Streptomyces and 80 million/g of Aspergillus niger.
[0044] The inner layer: 24 kg of urea formaldehyde powder, 15 kg of polyethylene glycol, 1 kg of polyglutamic acid, 20 kg of fulvic acid, 20 kg of chitin, 10 kg of alginic acid, 200 million/g of bacillus subtilis, 100 million/g of Bacillus gelatinosus, 150 million/g of Bacillus thuringiensis, 80 million/g of Bacillus laterosporus, 80 million/g of Bacillus mucilaginosus, 80 million/g of Paecilomyces lilacinus, 200 million/g of Trichoderma harzianum, 100 million/g of Trichoderma aureoviride, 50 million/g of streptomycete and 80 million/g of Aspergillus niger.
[0045] The preparation method is the same as that in example 1.
Comparative Example 3
[0046] A special controlled-release bacterial fertilizer for peanuts:
[0047] The outer layer: 30 kg of fulvic acid, 22 kg of chitin, 12 kg of alginic acid, 12 kg of rice husk carbon, 8 kg of cellulose (relative molecular weight is 80000-100000), 15 kg of sodium carboxymethyl starch, 15 kg of modified starch, 5 kg of calcium chloride, 200 million/g of bacillus subtilis, 100 million/g of Bacillus gelatinosus, 150 million/g of Bacillus thuringiensis, 80 million/g of Bacillus laterosporus, 80 million/g of Bacillus mucilaginosus, 50 million/g of Streptomyces and 80 million/g of Aspergillus niger.
[0048] The inner layer: 24 kg of urea formaldehyde powder, 20 kg of fulvic acid, 20kg of chitin, 20 kg of alginic acid, 200 million/g of bacillus subtilis, 100 million/g of Bacillus gelatinosus, 150 million/g of Bacillus thuringiensis, 80 million/g of Bacillus laterosporus, 80 million/g of Bacillus mucilaginosus, 80 million/g of Paecilomyces lilacinus, 200 million/g of Trichoderma harzianum, 100 million/g of Trichoderma aureoviride, 50 million/g of streptomycete and 80 million/g of Aspergillus niger.
[0049] The preparation method is as follows:
[0050] (1) 1-fold weight of water was added in urea formaldehyde powder in the inner layer, heated to 95° C. and stirred for 1 h, the above mixture was subjected to ultrasonic treatment for 20 min and cooled to 38° C., fulvic acid, chitin, alginic acid and active bacteria were added, and then the above mixture was pelletized and dried to obtain an core inner layer;
[0051] (2) Water whose weight was twice those of water whose weight was twice those of former two was added in sodium carboxymethyl starch and modified starch in the outer layer and then heated to 70-80° C., and calcium chloride was added. After the above materials were evenly stirred, rice husk carbon and cellulose were added. The above materials were evenly stirred and cooled to room temperature, the active bacteria were added, the above mixture was sprayed to the inner core layer under room temperature, and then the prepared particles were dried at low temperature.
Effect Example
[0052] (I) A release rule of effective nitrogen element in field nutrition of bacterial fertilizers provided by examples and comparative examples of the disclosure is detected according to a method provided by patent CN104541726. Specific detection results are shown in Table 1.
TABLE-US-00001 TABLE 1 Seedling Floricome Pod bearing Maturity stage (%) stage (%) stage (%) stage(%) Example 1 1.35 20.79 73.15 83.27 Example 4 1.21 17.60 64.37 78.12 Comparative 3.68 43.14 69.28 73.55 example 1 Comparative 2.15 31.28 70.33 75.29 example 2 Comparative 5.01 57.25 67.92 72.25 example 3
[0053] II) The same batch of Huayu No.22 peanut seeds was taken as experimental materials, the bacterial fertilizers prepared in examples and comparative examples were applied to an experimental field. Three groups of parallel experiments were conducted for each example and comparative example. 25 kg of bacterial fertilizer was applied in each mu. The blank experimental group was set for sowing, and the overall field was a field after continuous peanut cultivation for 2 years. It was sown on May 1 and harvested on September 20. Each group was kept consistent during the sowing soil, field control, fertilizer and water. Firstly, the incidence of diseases and insect pests in the whole growth cycle was counted. The specific results are shown in Table 2
TABLE-US-00002 TABLE 2 Disease rate (%) Inset pest rate (%) Example 1 3.1 5.4 Example 2 3.3 6.0 Example 3 2.9 5.3 Example 4 4.8 6.5 Comparative 6.7 8.2 example 1 Comparative 5.2 8.7 example 2 Comparative 7.7 9.2 example 3
[0054] (III) During test, sowing was carried out for the second year. Before and after planting, soil pH, soil urease activity and soil aeration were detected. The specific results are shown in Table 3 (test results after planting).
TABLE-US-00003 TABLE 3 Soil urease Soil pH activity Aeration degree (%) Example 1 6.98 0.96 36.32 Example 2 6.83 0.89 35.81 Example 3 6.85 0.92 35.77 Example 4 6.82 0.83 35.12 Comparative 6.71 0.68 34.05 example 1 Comparative 6.69 0.72 34.29 example 2 Comparative 6.63 0.65 33.91 example 3 Control 5.61 0.51 28.09
[0055] The soil planting experimental field was the same area. Soil samples were randomly selected for pH measurement and the average value was taken. Therefore, the pH before planting was considered to be the same, among which, the soil pH before sowing was 5.71; the soil urease activity was 0.55 mg/kg/h; and the soil aeration degree was 30.30%.
[0056] (IV) The yield per plant and yield per unit area were counted.
TABLE-US-00004 TABLE 4 Com- Com- Com- parative parative parative Exam- Exam- Exam- Exam- exam- exam exam Blank ple 1 ple 2 ple 3 ple 4 ple 1 ple 2 ple 3 control Yield per 55.1 54.9 54.3 52.8 47.6 49.2 46.2 40.6 plant (g) Yield per 7.12 6.87 6.69 6.11 5.73 5.96 5.62 5.10 unit area (kg/6.67 m.sup.2)