APPARATUS COMPRISING AT LEAST ONE THZ DEVICE AND METHOD OF OPERATING SUCH APPARATUS
20220120667 · 2022-04-21
Inventors
Cpc classification
G01N21/01
PHYSICS
G01N21/15
PHYSICS
International classification
Abstract
An apparatus includes at least one Terahertz (THz) device that transmits or receives THz radiation or transmits and receives THz radiation. The apparatus also provides a flow of protective gas in at least one portion of the beam path of the THz radiation.
Claims
1-23. (canceled)
24. An apparatus comprising: at least one Terahertz (THz) device configured to transmit and/or receive THz radiation, said apparatus being configured to provide a flow of protective gas in at least one portion of a beam path of said THz radiation, wherein said flow comprises a free jet.
25. The apparatus according to claim 24, wherein said protective gas comprises at least one of: a) dry air; b) dry gas; c) dry gas mixture; or d) at least one gas which does not comprise an absorption line in a frequency range of said THz radiation.
26. The apparatus according to claim 24, wherein said protective gas comprises a dew-point temperature of −20 degrees Celsius or less.
27. The apparatus according to claim 24, wherein said protective gas effects an attenuation of said THz radiation along said beam path of 0.1 dB or less.
28. The apparatus according to claim 24, further comprising at least one of: a) at least one protective gas supply device configured to provide said flow of protective gas; orb) at least one pressure controller for influencing a pressure of said flow of protective gas.
29. The apparatus according to claim 24, wherein said apparatus further comprises at least one nozzle configured to direct at least a portion of said flow of protective gas to said at least one portion of said beam path of said THz radiation.
30. The apparatus according to claim 29, wherein said at least one nozzle is arranged a) parallel with respect to said beam path of said THz radiation or a reference axis of said at least one THz device and/or coaxially with respect to said beam path of said THz radiation or a reference axis of said at least one THz device; or b) at an acute angle with respect to said beam path of said THz radiation or a reference axis of said at least one THz device.
31. The apparatus according to claim 24, further comprising an inlet port for receiving protective gas from an external supply.
32. The apparatus according to claim 24, further comprising a supply for said protective gas.
33. The apparatus according to claim 32, wherein said supply comprises at least one of: a) a protective gas tank for at least temporarily storing said protective gas; or b) a protective gas generator configured to generate said protective gas.
34. The apparatus according to claim 24, wherein said apparatus is configured to provide one or more gas jets of said protective gas.
35. The apparatus according to claim 34, wherein at least one of said gas jets comprises and/or is a free jet.
36. The apparatus according to claim 24, wherein said flow of protective gas comprises a flow in a direction a) parallel to said beam path of said THz radiation or b) at least substantially parallel to said beam path of said THz radiation.
37. The apparatus according to claim 24, wherein a nominal working distance between said at least one THz device and a measuring object interacting with said THz radiation transmitted from and/or received by said at least one THz device is equal to or greater than 4 centimeter (cm).
38. The apparatus according to claim 29, wherein said apparatus comprises: a first nozzle configured to provide a first jet of said protective gas; and a second nozzle wherein the second nozzle is a ring nozzle arranged coaxially around said first nozzle.
39. The apparatus according to claim 38, wherein said second nozzle is configured to provide a second jet, wherein the second jet at least partly coaxially surrounds said first jet.
40. The apparatus according to claim 24, wherein said apparatus comprises: a housing, wherein said at least one THz device is arranged in an interior of said housing.
41. The apparatus according to claim 40, comprising: a supply for said protective gas, wherein at least one component of said protective gas supply is arranged within and/or constituted by said interior of said housing.
42. The apparatus according to claim 31, wherein said apparatus comprises a housing, wherein said inlet port is arranged at and/or integrated into said housing.
43. The apparatus according to claim 42, further comprising: at least one nozzle configured to direct at least a portion of said flow of protective gas to said at least one portion of said beam path of said THz radiation, wherein the at least one nozzle is arranged at and/or integrated into said housing, and wherein a fluid communication between said inlet port and said at least one nozzle is enabled via an interior of the housing.
44. The apparatus according to claim 40, wherein said housing comprises an opening for passing through said THz radiation, and wherein at least one nozzle configured to direct at least a portion of said flow to said at least one portion of said beam path of said THz radiation a) is arranged in or around said opening, and/or b) forms said opening.
45. The apparatus according to claim 44, wherein said apparatus comprises at least one lid configured for opening and/or closing said opening.
46. The apparatus according to claim 45, wherein the at least one lid is configured for sealingly closing said opening.
47. The apparatus according to claim 45, wherein said lid is attached to at least one of: the housing or the nozzle.
48. The apparatus according to claim 44, wherein a window is provided in said opening, wherein said window is configured to sealingly close said opening, and wherein said window is transparent to said THz radiation.
49. The apparatus according to claim 24, further comprising a positioning system.
50. The apparatus of claim 24, further comprising: a positioning system configured to position said apparatus at least a measuring distance from a measuring object, wherein said measuring distance is at least 2 centimeters, wherein a spatial region between said apparatus and said measuring object is exposed to the surroundings, and wherein no solid body is arranged between said apparatus and said measuring object.
51. A method of operating an apparatus comprising at least one THz device, wherein said at least one THz device is configured to transmit and/or receive THz radiation, wherein said apparatus provides a flow of protective gas in at least one portion of a beam path of said THz radiation, wherein said flow comprises a free jet.
52. The method according to claim 51, wherein said apparatus further comprises at least one nozzle, wherein said at least one nozzle directs at least a portion of said flow to said at least one portion of said beam path of said THz radiation.
53. A method for performing measurements, comprising: transmitting THz radiation along a beam path using at least one THz device; providing a flow of protective gas to at least one portion of the beam path of the THz radiation using a protective gas flow device, wherein the flow of protective gas comprises a free jet of protective gas; and positioning, using a positioning system, an apparatus that includes the THz device to a measuring distance (md) from a measuring object, wherein the measuring distance (md) is at least equal to or greater than 4 centimeters, and wherein no solid body is arranged between the apparatus and the measuring object.
54. The method of claim 53, wherein the measuring distance (md) is at least equal to or greater than 10 centimeters.
55. The method of claim 53, further comprising: determining by at least a control device one or more measurements of the measuring object, wherein at least the control device determines the one or more measurements from at least a portion of the THZ radiation that is reflected from or transmitted through the at least one measuring object.
56. The method of claim 55, wherein determining by at least the control device the one or more measurements comprises: determining a layer thicknesses of one or more layers arranged on a surface of the measuring object, wherein the one or more layers include: a) at least one paint layer; or b) at least one coating layer; or c) at least one paint layer and at least one coating layer.
57. The method of claim 55, wherein the at least one paint layer comprises at least one wet paint layer; or wherein the at least one coating layer comprises at least one wet coating layer.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
[0053] Further features, aspects and advantages of the embodiments are given in the following detailed description with reference to the drawings in which:
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DETAILED DESCRIPTION
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[0066] According to further embodiments, said at least one THz device comprises at least one of: a) a THz transmitter 110 configured to transmit THz radiation TR1, b) a THz receiver 110a configured to receive THz radiation TR2, c) a THz transceiver (not shown) configured to transmit and to receive THz radiation TR. According to further embodiments, more than one THz transmitter 110 and/or more than one THz receiver 110a and/or more than one THz transceiver (not shown) may also be provided. Presently, the exemplary configuration of
[0067] According to further embodiments, said THz radiation TR comprises at least one frequency component in the range of 0.3 THz and 100 THz, preferably in the range of 0.5 THz and 10 THz, more preferably in the range of 3.0 THz to 10 THz. According to further embodiments, said THz radiation TR may comprise one or more THz pulses.
[0068] According to further embodiments, said protective gas PG comprises, or preferably is, at least one of: a) dry air, b) dry gas, c) dry gas mixture.
[0069] According to further embodiments, said protective gas PG comprises at least one gas which does not comprise an absorption line in a frequency range of said THz radiation TR.
[0070] According to further embodiments, said protective gas PG effects an attenuation of said THz radiation TR along said beam path BP of 0.1 dB or less, preferably for any frequency of said THz radiation TR.
[0071] According to further embodiments, said protective gas PG, e.g. dry air, comprises a dew-point temperature of −20 degrees Celsius (° C.) or less, preferably of −30° C. or less, further preferably of −40° C. or less.
[0072] According to further embodiments, said apparatus 100 further comprises at least one protective gas supply device 120 configured to provide said flow F of protective gas PG.
[0073] According to further embodiments, said apparatus 100 further comprises at least one pressure controller 128 for influencing, particularly controlling, a pressure of said flow F of protective gas PG. According to further embodiments, said influencing, particularly controlling, said pressure of said flow F of protective gas PG may comprise an open-loop or a closed-loop control. According to further embodiments, reference measurements using said THz radiation TR, TR2, may be made, and at least one parameter P1 characterizing fluid flow properties of a region of said beam path BP of said THz radiation TR may be determined, e.g. by a control device 300 which is explained in detail further below. As an example, under control c1 of the control device 300, the THz transmitter 110 may transmit first THz radiation TR1 to said measuring object 10, and the THz receiver 110a may receive the reflected portion TR2, based on which said control device 300 may determine said at least one parameter P1, cf. the data link c2. Based on said at least one parameter P1, said control device 300 may control an operation of the protective gas supply device 120, cf. the data link c3, e.g. to influence (increase or decrease or maintain) a pressure of said flow F of protective gas PG, whereby a closed-loop control as mentioned above is enabled. This way, the pressure of said flow F of protective gas PG may be optimized regarding a precision of said THz measurements, e.g. attaining a laminar or even homogenous flow F of said protective gas in at least a portion of said beam path BP of said THz radiation TR. Preferably, the pressure of said flow of protective gas may be controlled such as to ensure a spatially and temporally constant flow velocity of said flow of protective gas in the region of the beam path BP. According to further embodiments, an open-loop control of said pressure of said flow F of protective gas PG is also possible.
[0074] According to further embodiments, said (optional) pressure controller 128 may also form part of the protective gas supply device 120 and/or may be connected in series thereto, e.g. to an output (as exemplarily depicted by
[0075] According to further embodiments, said apparatus 100 may comprise at least one flow regulator for influencing, particularly controlling, a volume flow of said (flow F of) protective gas PG. In this regard, according to further embodiments, the details explained above with respect to the pressure controller 128 may be applied correspondingly to the flow regulator.
[0076] According to further embodiments, said apparatus 100 further comprises at least one nozzle 122, wherein preferably said at least one nozzle 122 is configured and/or arranged so as to direct said flow F of protective gas PG, or at least a portion of said flow F, to said at least one portion P′ of said beam path BP of said THz radiation TR, wherein preferably said at least one nozzle 122 is a free jet nozzle 122. This enables to provide the region comprising said beam path BP of said THz radiation TR with a precisely controllable flow F of protective gas PG. According to further embodiments, said flow F may comprise or be a laminar flow, preferably a homogenous flow. According to further embodiments, said at least one nozzle 122 may form part of said at least one protective gas supply device 120, preferably an integral part.
[0077] According to further embodiments, said apparatus 100 further comprises an inlet port 124 for receiving protective gas PG1 from an external supply 200. According to further embodiments, said inlet port 124 may e.g. form part of said at least one protective gas supply device 120.
[0078] According to further embodiments, said apparatus 100 further comprises a, preferably local, supply 126 for said protective gas PG, wherein said, preferably local, supply 126 is preferably attached to and/or integrated into at least one other component of said apparatus 100. According to further embodiments, said, preferably local, supply 126 may form part of said at least one protective gas supply device 120.
[0079] According to further embodiments, said external supply 200 and/or said, preferably local, supply 126 comprises at least one of: a) a protective gas tank T1, T2 for at least temporarily storing said protective gas, b) a protective gas generator G1, G2 configured to generate said protective gas, wherein preferably said protective gas generator G1, G2 is configured to receive atmospheric air AA and to convert said atmospheric air AA into said protective gas PG1, preferably into dry air.
[0080] According to further embodiments, said apparatus 100 is configured to provide one or more gas jets F1, F2, F3 of said protective gas PG, wherein preferably said one or more gas jets contribute to or constitute said flow F. According to further embodiments, said at least one nozzle 122 may be provided, wherein said at least one nozzle 122 may be configured to provide said one or more gas jets of said protective gas PG.
[0081] According to further embodiments, said flow F and/or at least one of said gas jets comprises and/or is a free jet. This enables particularly large nominal working distances for said apparatus (e.g., between the apparatus and/or its THz device(s) 110, 110a and the measuring object 10), because the THz radiation TR may efficiently be “shielded” from atmospheric air AA (and/or other surrounding fluids that may affect a propagation of THz radiation) by said free jet(s) of protective gas PG. Particularly, this way, no housing or any other (solid) body or device for guiding said flow F and/or gas jets (apart from e.g. the optional nozzle 122) are required to be placed between the apparatus 100 and the measuring object 10 that interacts with said THz radiation TR. According to further embodiments, a potential core length of said free jet is equal to or larger than about 2 cm in some embodiments or 4 cm in other embodiments.
[0082] According to further embodiments, the apparatus 100 may comprise a control device 300, as mentioned above. Said control device 300 may e.g. at least temporarily control an operation of said apparatus 100 and/or of at least one component of said apparatus 100.
[0083] According to further embodiments, said control device 300 comprises at least one calculating unit 302 and at least one memory unit 304 associated with (i.e., usably by) said at least one calculating unit 302 for at least temporarily storing a computer program PRG and/or data (not shown), wherein said computer program PRG is e.g. configured to at least temporarily control an operation of said apparatus 100, e.g. the execution of a method according to the embodiments, for example for controlling the operation of said THz device 110, 110a and/or the protective gas supply device 120 and/or one of its components.
[0084] According to further embodiments, said at least one calculating unit 302 may comprise at least one of the following elements: a microprocessor, a microcontroller, a digital signal processor (DSP), a programmable logic element (e.g., FPGA, field programmable gate array), an ASIC (application specific integrated circuit), hardware circuitry. According to further embodiments, any combination of two or more of these elements is also possible.
[0085] According to further embodiments, the memory unit 304 comprises at least one of the following elements: a volatile memory, particularly a random-access memory (RAM), a non-volatile memory, particularly a Flash-EEPROM. Preferably, said computer program PRG is at least temporarily stored in said non-volatile memory.
[0086] According to further embodiments, an optional computer-readable storage medium SM comprising instructions, e.g. in the form of a further computer program PRG′, may be provided, wherein said further computer program PRG′, when executed by a computer, i.e. by the calculating unit 302, may cause the computer 302 to carry out the method according to the embodiments or at least one step thereof. As an example, said storage medium SM may comprise or represent a digital storage medium such as a semiconductor memory device (e.g., solid state drive, SSD) and/or a magnetic storage medium such as a disk or hard disk drive (HDD) and/or an optical storage medium such as a compact disc (CD) or DVD (digital versatile disc) or the like.
[0087] According to further embodiments, the control device 300 may comprise one or more interfaces (not shown) for a, preferably bidirectional, data exchange with other components 110, 110a, 120, e.g. to control an operation of the THz device(s) 110, 110a and/or the protective gas supply device 120, e.g. a pressure controller 128 associated with and/or integrated into said protective gas supply device 120.
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[0089] According to further embodiments, cf. the apparatus 100c of
[0090] According to further embodiments, also cf.
[0091] According to further embodiments, said at least one nozzle 122 (e.g., a reference axis of said at least one nozzle) is arranged at an acute angle with respect to said beam path BP of said THz radiation TR or a reference axis of said at least one THz device, wherein preferably said acute angle ranges between 0 degrees and 30 degrees, preferably between 0 and 20 degrees. According to further embodiments, the nozzle 122 and/or said flow F provided thereby may also comprise another angle with said THz beam path BP, may e.g. be substantially perpendicular to said beam path, as exemplarily depicted by
[0092] According to further embodiments, said flow F (
[0093] According to further embodiments, cf.
[0094] Moreover, when using the principle according to embodiments, and in contrast to conventional approaches, the measuring object 10 (
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[0097] According to further embodiments, said apparatus 100f, cf.
[0098] Similar to
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[0100] According to further embodiments, cf.
[0101] According to further embodiments, said second jet F42 (i.e., the sheath flow), may comprise ambient air AA and/or said protective gas PG. As the fluid of the (radially outer) second jet F42 usually does not (or at least not substantially) interact with the, preferably radially inner, THz beam path, the second jet F42 may comprise ambient air AA. However, for further increasing precision and a nominal working distance dw (
[0102] According to further embodiments, both nozzles 1221, 1222 may be provided in form of an integrated nozzle device 1220, which may be supplied with protective gas PG by a corresponding common protective gas supply device 120a. According to further embodiments, at least one of the components 1221, 1222, 120a may also be arranged within or at a housing 130 (
[0103] While exemplarily depicted together with two THz devices 110, 110a in
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[0106] According to further embodiments, it is also possible to provide the first (inner) nozzle 1221—instead of a single, preferably circular, opening, with a plurality of either equally spaced and/or regularly arranged and/or stochastically distributed individual nozzle openings to provide said flow F, similar to the nozzle openings 1222_a.
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[0108] According to further embodiments, each nozzle 1221, 1222 may comprise an individual inlet port (not shown) for receiving protective gas PG and/or ambient air or the like, wherein especially a radial velocity distribution of said flow(s) generated by said nozzles 1221, 1222 may flexibly be controlled.
[0109] According to further embodiments, cf. the apparatus 100j of
[0110] According to further embodiments (
[0111] According to further embodiments, cf. the apparatus 100k of
[0112] According to further embodiments, said at least one nozzle 122 may be provided around said opening 132 having said window 136, e.g. being attached to an outer surface 130a of the housing 130, and said at least one nozzle 122 may comprise an inlet port 124′ for receiving the protective gas PG, e.g. from an external supply 200. Particularly, in these embodiments, the inlet port 124′ is outside the housing 130 of the apparatus 100k (in which e.g. said at least one THz device 110, 110a may be arranged), so that the interior I of the housing 130 is not provided with “fresh” protective gas when said at least one nozzle 122 is supplied with said protective gas PG to provide said flow F of protective gas PG to the beam path of the THz radiation TR. According to further embodiments, the housing 130 may be hermetically sealed, and the interior I may be filled with protective gas prior to sealing, e.g. during manufacturing of said housing 130.
[0113] According to further embodiments, cf. the apparatus 100l of
[0114] According to further embodiments, said apparatus 100l comprises at least one lid 134 for, particularly selectively, opening and/or closing, preferably sealingly, particularly hermetically (gastight) sealingly, closing, said opening 132, wherein preferably said lid 134 is, particularly rotatably, attached to at least one of: the housing 130, the nozzle 122. Presently, in
[0115] According to further embodiments, the opening and/or closing of said lid 134 or the opening 132, respectively, may e.g. be performed depending on an operational state of said apparatus 100l. E.g., for an activated state, e.g. usable for performing measurements using said THz radiation TR, said lid 134 may—at least temporarily—be opened, and for a deactivated state, said lid 134 may be closed.
[0116] According to further embodiments, an actuator 135 (e.g., electromagnetic actuator) may be provided to drive movement of said lid 134, i.e. for opening said lid 134 and/or closing said lid 134. In the closed state, the lid 134 prevents e.g. particles to enter the interior I of the housing 130, while in the opened state, the lid 134 enables transmission and/or reception of THz radiation TR, as well as e.g. (optionally) a flow F of protective gas through said opening 132. If, according to further embodiments, a flow F of protective gas PG is provided through said opening 132 in the opened state of the lid 134, particles are prevented from entering the interior I of the housing 130 by means of said protective gas flow F.
[0117] According to further embodiments, said actuator 135 may comprise a spring or spring mechanism (not shown), preferably arranged and/or configured to exert a spring force (“closing force”) on said lid 134 such that it is retained in its closed state, i.e. sealing the opening 132, by said closing force. Preferably, said spring or spring mechanism may be configured such that in the absence of said flow F of protective gas, said lid 134 remains in its closed state, sealing the opening 132, due to said closing force, wherein in the presence of said flow F of protective gas, an “opening” force OF may be provided by said flow F which is greater than said closing force, effecting the lid 134 to “automatically” (i.e., without human interaction) open once the flow F is present. In this opened state, THz measurements may be made, and once the flow F is deactivated, the lid will close again due to the closing force of the spring or spring mechanism 135.
[0118] According to further embodiments, said apparatus 100m, cf.
[0119] According to further embodiments, an external supply 200 of protective gas may be arranged at or close to the robot 140, and a fluid or gas line 202 may provide said protective gas to an inlet port 124 provided at the measuring head 130 (i.e., housing). Similar to at least one of the apparatus 100 to 1001 explained above, the apparatus 100m of
[0120] Further embodiments relate to a measuring system 1000 comprising at least one apparatus 100m according to the embodiments and at least one measuring object 10, wherein preferably said apparatus 100m and said at least one measuring object 10 are spaced apart from each other by a measuring distance and of at least 2 centimeters, preferably of at least 5 centimeters, wherein preferably no body, preferably no solid body, (or any other material apart from said flow F of protective gas (and/or an optional sheath flow)) is arranged between said apparatus 100m and said measuring object 10.
[0121] Further embodiments relate to a method of operating an apparatus comprising at least one THz device, wherein said at least one THz device is configured to transmit and/or receive THz radiation, wherein said apparatus provides a flow of protective gas in at least one portion of a beam path of said THz radiation. This is exemplarily depicted by the simplified flow chart of
[0122] In this respect,
[0123] Conversely, when performing THz measurements 410 (
[0124] According to further embodiments, said at least one nozzle 122 may also be designed as a de Laval nozzle. According to Applicant's analysis, these embodiments are particularly suitable for even larger working distances.
[0125] According to further embodiments, it is also possible to provide a fully turbulent flow of said protective gas to at least one portion of said beam path, wherein adverse effects of said turbulent flow on the THz radiation may cancel each other statistically.
[0126] According to further embodiments, the principle according to the embodiments may be used for a wide variety of measurements based on THz radiation, such as e.g. reflection-based and/or transmission-based measurements, e.g. (time-domain) reflectometry-based layer thickness measurements and the like, spectrographic measurements, THz radiation based imaging methods, and soon. Apart from reducing the undesired effects of water (vapor) absorption, at least some embodiments enable to further reduce noise of THz measurements that may be cause by fluctuations of a surrounding medium such as atmospheric air. Further embodiments enable to provide a controllable, preferably homogenous, distribution of (gas) pressure over time and space in the region of the THz beam path BP, thus further increasing precision and reliability of THz radiation based measurements.