Dental hygiene wipes comprising microcapsules

11759408 · 2023-09-19

    Inventors

    Cpc classification

    International classification

    Abstract

    The invention relates to a dental cleaning wipe comprising a non-woven textile support impregnated with a dental hygiene composition containing mechanically-broken microcapsules, the content of which is released by breaking the wall, as well as controlled-release microcapsules, the content of which is released by permeation through the wall, the walls of said microcapsules being water-insoluble.

    Claims

    1. Dental cleaning wipe consisting of a non-woven textile support impregnated with a dental hygiene composition in which at least some of the constituents are encapsulated in microcapsules deposited on the surface of the said non-woven textile support being characterized in that it includes two different types of microcapsules: mechanically broken microcapsules, the contents of which are released by breaking of the wall; and Diffusion-controlled microcapsules whose contents are released by permeation through the wall, and in that the wall of these microcapsules is insoluble in water.

    2. Dental cleaning wipe according to claim 1, characterized in that said wipe comes in the form of a glove finger.

    3. Dental cleaning wipe according to one of the claim 1 or 2, characterized in that the non-woven textile support is chosen from cellulose, chemically modified cellulose and cellulose-derived absorbent materials.

    4. Dental cleaning wipe according to claim 1, characterized in that the thickness of the non-woven textile support is between 20 and 1500 μm, and is at least 2 times the average diameter of the microcapsules deposited on its surface.

    5. Dental cleaning wipe according to claim 1, characterized in that the average diameter of the microcapsules deposited on its surface is between 1 and 50 μm.

    6. Dental cleaning wipe according to claim 1, characterized in that the amount of microcapsules deposited on the non-woven textile support is 5 to 50 g/m2 of surface of the non-woven textile support.

    Description

    EXAMPLE 1: DISINFECTANT DENTAL CLEANER 1

    (1) TABLE-US-00001 % in % in Component microcapsule formula Purified Water 71.20 Glycerin 5.00 Xylitol 0.50 Sorbitol 2.00 Cocoyl glucoside 0.20 Sodium Benzoate 0.30 Sodium citrate 0.80 Diffusion-Controlled silicone 7.00 microcapsules medium diameter 5 μm containing: Melaleuca Alternifolia Essential Oil 10.00 Peppermint essential oil 30.00 Essential Oil Lemon 60.00 Crosslinked gelatin microcapsules with 13.00 an average diameter of 15 μm with mechanical rupture containing: Essential Oil Lemon 70.00 Peppermint essential oil 30.00 TOTAL 100.00

    (2) Diffusion-Controlled silicone microcapsules are prepared by in situ polymerization.

    (3) Mechanically broken gelatin microcapsules are prepared by complex coacervation in the presence of alginate.

    (4) A finger-shaped wipe, consisting of a 50 μm thick layer of cellulose, lined with a 20 μm thick waterproof film, was impregnated by scarfing with the composition shown in the table above, this composition being prepared by a simple cold mixture; both types of microcapsules, both in the form of a thick water yawn suspension at a concentration of about 35% of dry capsules, are added at the end of mixing under low agitation.

    EXAMPLE 2: DENTAL CLEANSER 2

    (5) TABLE-US-00002 % in % in Component microcapsule formula Purified Water 81.90 Glycerin 3.00 Xylitol 0.80 Sodium bicarbonate 2.00 Sodium Benzoate 0.30 Potassium Sorbate 0.20 Carboxymethyl cellulose 1.20 Polysorbate 80 0.60 Diffusion-controlled silicone 7.00 microcapsules medium diameter 5 μ containing: Essential Oil Eucalyptus Globulus 30.00 Essential Oil Lemon 70.00 Reticulated fish gelatin microcapsules 3.00 average diameter 15 μ mechanical rupture containing: Essential Oil Eucalyptus Globulus 30.00 Essential Oil Lemon 70.00 TOTAL 100.00

    (6) Silicone microcapsules with controlled diffusion are prepared by polymerization in situ.

    (7) Mechanically broken gelatin microcapsules are prepared by complex coacervation in the presence of cellulose carboxymethyl.

    (8) A finger-shaped wipe, consisting of a 50 μm thick cellulose layer, lined with a 20 μm thick waterproof film, was impregnated by spraying the cellulosic part with the composition shown in the table above, the non-microcapsule composition prepared by a simple mixture at a temperature of 45° C.; after cooling to a maximum of 30° C., the microcapsules are added under low agitation. Diffusion-controlled silicone microcapsules are integrated into a thick water suspension at the 35% concentration of dry capsules and mechanically broken fish gelatin microcapsules are found under form of dry capsules and are introduced at the end of the mixing process.

    EXAMPLE 3: DISINFECTANT DENTAL CLEANSER 3

    (9) TABLE-US-00003 % in % in Component microcapsule formula Purified Water 82.92 Glycerine 5.00 Acesulfame potassium 0.05 Fluoride sodium 0.03 Benzoate sodium 0.20 Carboxymethyl cellulose 1.20 Polysorbate 80 0.60 Microcapsules silicones with diffusion - 7.00 controlled medium diameter 5 μ containing: Peppermint essential oil 100.00 Reticulated fish gelatin microcapsules 3.00 average diameter 40 μ low thickness mechanical rupture containing: Chlorhexidine digluconate 2.00 Lemon Essential Oil 98.00 TOTAL 100.00

    (10) Diffusion-controlled silicone microcapsules are prepared by in situ polymerization.

    (11) Mechanically-broken microcapsules in low-thickness gelatin are prepared by complex coacervation in the presence of alginate.

    (12) A finger-shaped wipe, consisting of a 50 μm thick cellulose layer, lined with a 20 μm thick waterproof film, was impregnated by spraying the cellulosic part with the composition shown in the table above, the non-microcapsule composition being prepared by a simple mixture at a temperature of 45° C.; after cooling to a maximum of 30° C., the microcapsules are added under low agitation. Diffusion-controlled silicone microcapsules are integrated into a thick water suspension at the 35% concentration of dry capsules and mechanically broken fish gelatin microcapsules come in the form of dry capsules and are introduced at the end of the mixing process.

    EXAMPLE 4: DENTAL CLEANSER 4

    (13) TABLE-US-00004 % in % in Component microcapsule formula Purified water 83.70 Carbomer 940 1.80 Xylitol 0.80 Sodium bicarbonate 2.00 Sodium Benzoate 0.30 Triethanolamine 0.30 Camomile extract 0.50 Carraghenane 0.60 Microcapsules reticulated gelatin with 7.00 diffusion-controlled medium diameter 2 μ containing: Peppermint essential oil 80.00 Sweet Orange Essential Oil 20.00 Medium Diameter Polyamide 3.00 Microcapsules 18 u mechanically broken containing: Sweet Orange Essential Oil 30.00 Lemon Essential Oil 70.00 TOTAL 100.00

    (14) Diffusion-controlled reticulate microcapsules are prepared by complex coacervation.

    (15) Polyamide mechanically laid microcapsules are prepared by polymerization in situ.

    (16) A finger-shaped wipe, consisting of a 40 μm thick layer of cellulose, was sprayed with the composition shown in the table above, the non-microcapsule composition being prepared by simple mixture at a temperature of 45° C.; after cooling to a maximum of 30° C., the microcapsules are added under low agitation. Both types of microcapsules are integrated in the form of a thick slimy suspension water yawn suspension (slurry) at a concentration of 40% of dry capsules.