Fluid supply device for fluid chromatograph
11761933 ยท 2023-09-19
Assignee
Inventors
Cpc classification
B01D15/40
PERFORMING OPERATIONS; TRANSPORTING
B01D15/14
PERFORMING OPERATIONS; TRANSPORTING
International classification
B01D15/14
PERFORMING OPERATIONS; TRANSPORTING
Abstract
A fluid supply device for a fluid chromatograph includes a storage container, a pump device, a filter, a guide and a heat dissipation device. The pump device supplies a mobile phase to a column. The storage container stores the pump device and the filter and has an intake port. The guide guides gas that has been introduced into the storage container through the intake port to the filter. A heat dissipation device dissipates heat generated from the pump device to the outside of the storage container together with the gas inside of the storage container. The storage container includes a door having a front surface directed forwardly of the fluid supply device. The intake port is provided at the door to be directed sidewardly of the fluid supply device.
Claims
1. A fluid supply device for a fluid chromatograph comprising: a pump device for supplying a mobile phase to a column; a filter; a storage container that stores the pump device and the filter and has an intake port; a guide that guides gas that has been introduced into the storage container through the intake port to the filter; and a heat dissipation device that dissipates heat generated from the pump device to the outside of the storage container together with gas inside of the storage container, wherein the storage container includes a front surface member having a front surface facing a first direction, and the intake port is provided at the front surface member facing a second direction that intersects with the first direction.
2. The fluid supply device for a fluid chromatograph according to claim 1, wherein the storage container further includes a casing having a front surface opening, and a door that closes and opens at least a partial area of the front surface opening, and the front surface member is the door.
3. The fluid supply device for a fluid chromatograph according to claim 2, wherein the door has the front surface, a first side portion and a second side portion, the first side portion is provided at the casing to be turnable, and the intake port is provided at the second side portion.
4. The fluid supply device for a fluid chromatograph according to claim 2, further comprising a holding member that attachably and detachably holds the filter at the door.
5. The fluid supply device for a fluid chromatograph according to claim 4, wherein the holding member has a snap-fit mechanism and is configured to be attachable to and detachable from the door by the snap-fit mechanism.
6. The fluid supply device for a fluid chromatograph according to claim 4, wherein the holding member includes the guide, and the guide guides gas that has flowed in a direction opposite to the second direction through the intake port to the filter held by the holding member.
7. The fluid supply device for a fluid chromatograph according to claim 1, wherein the front surface member has an inner surface opposite to the front surface, and the filter is a plate-shape member having a ventilation plane, and the ventilation plane is arranged to face an inner surface of the front surface member.
8. The fluid supply device for a fluid chromatograph according to claim 1, wherein the intake port is provided at the front surface member not to be seen in a case where the front surface member is viewed in a direction opposite to the first direction.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
(1)
(2)
(3)
(4)
(5)
(6)
(7)
(8)
(9)
(10)
(11)
(12)
DESCRIPTION OF EMBODIMENTS
[1] Basic Configuration of Fluid Supply Device for Fluid Chromatograph
(13) A liquid sending device for a liquid chromatograph will be described as one example of a fluid supply device for a fluid chromatograph according to one embodiment of the present invention.
(14) As shown in
(15) The upper wall 110a and the lower wall 110b are formed to face each other in an up-and-down direction. The one sidewall 110c connects one side of the upper wall 110a to one side of the lower wall 110b, the other sidewall 110d connects another side of the upper wall 110a to another side of the lower wall 110b and the one sidewall 110c and the other sidewall 110d are formed to face each other. The end surface wall 110e is perpendicular to the upper wall 110a, the lower wall 110b, the one sidewall 110c and the other sidewall 110d, and is connected to the ends of the upper wall 110a, the lower wall 110b, the one sidewall 110c and the other sidewall 110d. The casing 110 has an opening OP in a portion opposite to the end surface wall 110e.
(16) The bi-parting door 120 includes doors 120A, 120B. The door 120A closes and opens the area from the one sidewall 110c to substantially the center of the opening OP in the opening OP of the casing 110. The door 120A may be provided at the one sidewall 110c to be turnable around a turning axis LA extending in the up-and-down direction.
(17) The door 120B closes and opens the area from the other sidewall 110d to substantially the center of the opening OP in the opening OP of the casing 110. The door 120B is provided at the other sidewall 110d to be turnable around the turning axis LB extending in the up-and-down direction.
(18) In the following description, the bi-parting door 120 and its peripheral portions of the liquid sending device 10 of
(19) Each of the two pump devices PP has the configuration in which one pump motor (not shown) and two pump heads PH are assembled into one pump body PB. In each pump device PP, two plungers (not shown) are provided in each of the two pump heads PH. The pump motor drives the two plungers in the two pump heads PH by receiving power from the power supply circuit (not shown) (a double plunger system). This causes each plunger to reciprocate in the pump head PH.
(20) In each pump device PP, the two pump heads PH are located in the front portion of the liquid sending device 10 inside of the storage container 100, and the pump body PB is located at a position farther rearward than the two pump heads PH in the liquid sending device 10. Thus, when the bi-parting door 120 is closed, each pump head PH is close to the inner surface of the bi-parting door 120.
(21) The heat dissipation device EX includes a heat dissipating fan and a fan motor that drives the heat dissipating fan and dissipates heat generated in the storage container 100 to the outside of the storage container 100 together with gas inside of the storage container 100. The heat generated in the storage container 100 includes heat generated from the pump motor and the power supply circuit when the pump device PP is operated.
(22) The storage container 100 is provided with an intake port for taking gas outside of the storage container 100 into the storage container 100 when heat is dissipated by the heat dissipation device EX. Further, the storage container 100 is provided with an exhaust port for exhausting gas inside of the storage container 100 to the outside of the storage container 100 when heat is dissipated by the heat dissipation device EX.
(23)
(24) When heat is dissipated by the heat dissipation device EX of
[2] Details of Configuration of Door 120A and its Peripheral Members
(25) The door 120A of
(26) The door 120A includes a frame member 200 and a cover member 300. The frame member 200 is a single member formed of metal such as an aluminum alloy and is constituted by an upper frame 220, a lower frame 230 and a frame coupler 240. The upper frame 220 and the lower frame 230 respectively have a substantially prismatic shape, are arranged to extend in parallel with each other and be opposite to each other. The frame coupler 240 has a substantially elongated plate shape and couples one end of the upper frame 220 and one end of the lower frame 230 to each other.
(27) The other end of the upper frame 220 is connected to the upper hinge attachment portion 93 via a hinge HI, and the other end of the lower frame 230 is connected to the lower hinge attachment portion 93 via a hinge HI. At this time, in each hinge HI, its axial center is located on the turning axis LA. Thus, the frame member 200 is attached to the door attachment 90 by the upper and lower hinges HI to be turnable around the turning axis LA.
(28) The cover member 300 is a single member formed of resin, for example, and includes a lid 310, an upper wall 320 and a lower wall 330. The cover member 300 is attached to the frame member 200 as indicated by the thick one-dot and dash outlined arrow in
(29) As indicated by the thick dotted and outlined arrow in
(30) In the following description, the side portion close to the turning axis LA of the both sides of the door 120A is referred to as one side portion of the door 120A, and the side portion opposite to the one side portion is referred to as another side portion of the door 120A. Further, the surface directed inwardly of the casing 110 (rearwardly of the liquid sending device 10) when the door 120A is closed is referred to as an inner surface of the door 120A. Further, the direction in which the inner surface of the door 120A is directed is referred to as rearward of the door 120A, and its opposite direction is referred to as forward of the door 120A.
(31)
(32) As shown in
(33) The upper wall 320 covers the upper frame 220 from above, and the lower wall 330 covers the lower frame 230 from below. When the door 120A is closed, the lid 310 covers the frame member 200 and the door attachment 90 as well as part of the opening OP from the front of the liquid sending device 10.
(34) A cover coupler 340 having a substantially elongated plate shape is formed at a portion of the cover member 300 located at the other side portion of the door 120A to connect the upper wall 320 and the lower wall 330 to each other. The cover coupler 340 is opposite to the inner surface of the lid 310 with a certain distance therebetween and adjacent to the frame coupler 240 in the horizontal direction. The intake port IN of
(35) Protrusions 221, 231, 241 for provision of the filter FI of
(36) Specifically, the protrusion 221 of the upper frame 220 protrudes from the lower surface of the upper frame 220 by a predetermined distance and extends from the upper end of the frame coupler 240 to substantially the center of the upper frame 220. Part of the protrusion 221 is meandering. A meandering portion of the protrusion 221 functions as an engaged portion 222 corresponding to a snap-fit mechanism 430 (
(37) Further, the protrusion 231 of the lower frame 230 protrudes from the upper surface of the lower frame 230 by a predetermined distance and extends from the lower end of the frame coupler 240 to substantially the center of the lower frame 230. Part of the protrusion 231 is meandering. A meandering portion of the protrusion 231 functions as an engaged portion 232 corresponding to an engaging portion 490 (
(38) Further, the protrusion 241 of the frame coupler 240 protrudes from the side surface directed toward the one side portion of the door 120A by a predetermined height and extends linearly from the upper end to the lower end of the frame coupler 240.
(39) Next, the holding member 400 will be described.
(40) The holding member 400 is a single member formed of resin, for example, and has a substantially rectangular plate-shape main body 410 extending in the up-and-down direction as shown in
(41) As shown in
(42) Two holding pieces 453 are provided at the guide 420 to be arranged in the up-and-down direction at intervals. Each holding piece 453 protrudes in the direction directed from the guide 420 to the other side of the plate-shape main body 410 as shown in
(43) As shown in
(44) As shown in
(45) Here, the above-mentioned predetermined distance is equal to the thickness of the filter FI or slightly larger than the thickness of the filter FI, for example. Thus, in the holding member 400, the filter FI of
(46) The snap-fit mechanism 430 is provided at the center of the upper end of the plate-shape main body 410. In the present embodiment, a snap-fit is the coupling method of two members respectively having an engaging portion and an engaged portion, and is the method of using elastic deformation of at least one member out of the engaged portion and the engaging portion and fixing the two members. As shown in
(47) The snap-fit mechanism 430 of the present example has a holder 431, a tapered portion 432 and an engaging portion 433. The holder 431 is a rear end portion of the snap-fit mechanism 430 and extends horizontally at a position farther rearward than the plate-shape main body 410. The tapered portion 432 is the tip of the snap-fit mechanism 430 and its peripheral portions and has an outer surface extending forwardly and downwardly above the plate-shape main body 410. The engaging portion 433 is the upper end of the snap-fit mechanism 430 and its peripheral portions, is located between the holder 431 and the tapered portion 432 and has an outer surface directed rearwardly.
(48) The engaging portion 490 is provided at the center of the lower end of the plate-shape main body 410. The engaging portion 490 protrudes downwardly from the one surface of the plate-shape main body 410.
(49) When the holding member 400 is to be attached to the frame member 200, the user arranges the engaging portion 490 of the holding member 400 at a position farther forward than the engaged portion 232 of the frame member 200 from a position farther rearward than the door 120A of
(50) In this case, the tapered portion 432 of the snap-fit mechanism 430 slides on the engaged portion 222 of the frame member 200, whereby the snap-fit mechanism 430 is elastically deformed, and the tapered portion 432 moves to a position farther forward than the engaged portion 222. At this time, one portion of the one surface of the plate-shape main body 410 directed forwardly abuts against the protrusions 221, 231, 241 of the frame member 200. In this state, the engaged portion 222 of the frame member 200 is engaged with the engaging portion 433 of the snap-fit mechanism 430. Further, the engaged portion 232 of the frame member 200 is engaged with the engaging portion 490 of the holding member 400. Thus, the holding member 400 is attached to the frame member 200 to be fixed.
(51)
(52) As shown in
(53) In this case, as shown in
(54) Thus, as indicated by the thick-dotted and outlined arrows in
(55) When detaching the holding member 400 holding the filter FI from the frame member 200, the user pulls out the holder 431 of the holding member 400 rearwardly of the door 120A while pressing the holder 431 of the holding member 400 downwardly from a position farther rearward than the door 120A of
(56) As described above, the holding member 400 is configured to be attachable to and detachable from the door 120A by the snap-fit mechanism 430. Thus, the user can easily attach the holding member 400 to and detach the holding member 400 from the door 120A without using a tool or the like by opening the door 120A. This facilitates replacement of the filter FI.
[3] Effects
(57) (a) In the above-mentioned liquid sending device 10, heat generated in the storage container 100 by an operation of the pump device PP is dissipated by the heat dissipation device EX to the outside of the storage container 100 together with gas in the storage container 100. At this time, gas introduced into the storage container 100 through the intake port IN is guided to the filter FI, whereby particles or the like are prevented from adhering to the pump devices PP stored in the storage container 100.
(58) In the front portion of the liquid sending device 10, the intake port IN provided at the door 120A is directed sidewardly of the liquid sending device 10. That is, the intake port IN is formed to be directed in the direction that intersects with the direction directed forwardly of the liquid sending device 10. Thus, in a case where the liquid sending device 10 is viewed from a position farther forward than the liquid sending device 10, the intake port IN is unlikely to be seen. Therefore, designability of the door 120A provided in the front portion of the liquid sending device 10 can be improved while the intake port IN is provided in the front portion of the liquid sending device 10.
(59) (b) In the door 120A, the intake port IN is provided at the other side portion that is opposite to the one side portion attached to the one sidewall 110c of the casing 110 to be turnable. In this case, the user can open and close the door 120A by inserting his or her finger into the intake port IN and holding the other side portion of the door 120A. Thus, it is not necessary to provide a holder such as a handle for opening and closing the door to be held by the user at the door 120A. Therefore, a reduction in designability of the door 120A is suppressed.
(60) (c) The filter FI is arranged such that its ventilation plane faces the inner surface of the door 120A while being attached to the door 120A by the holding member 400. In this case, it is possible to prevent the filter FI from being exposed forwardly of the storage container 100 without reducing an area of the ventilation plane of the filter FI. Therefore, a reduction in designability of the front portion of the liquid sending device 10 caused by the filter FI is suppressed, and a reduction in heat dissipation efficiency is suppressed because a cross section of the flow path of gas passing through the filter FI is largely ensured.
[4] Liquid Chromatograph
(61)
(62) The liquid sending device 10 supplies a mobile phase stored in a mobile phase container T1 to a column provided in the column oven 4. The autosampler 3 injects a liquid sample into the mobile phase supplied from the liquid sending device 10 to the column. The column oven 4 keeps the temperature of the column provided in the column oven 4 at a substantially constant temperature. The detector 5 detects each component of the liquid sample separated by the column. The mobile phase that has passed through the detector 5 is sent to a liquid waste container T2. The control device 2 includes a CPU and a memory, for example, and controls the operation of each element that constitutes the liquid chromatograph 1.
(63) Because the liquid chromatograph 1 of the present example has the liquid sending device 10 of
[5] Other Embodiments
(64) (a) While the liquid sending device 10 that is one example of the fluid supply device for a fluid chromatograph according to the present invention is used in a liquid chromatograph in the above-mentioned embodiment, the present invention is not limited to this. The configurations of the door 120A and the holding member 400 provided in the above-mentioned liquid sending device 10 are not limited to be used in the liquid sending device 10 for a liquid chromatograph and may be used in a fluid supply device for a supercritical fluid chromatograph. Even in this case, the effects similar to those of the example of the above-mentioned embodiment can be obtained.
(65) (b) While the bi-parting door 120 is provided in the front portion of the storage container 100 in the liquid sending device 10 according to the above-mentioned embodiment, the present invention is not limited to this. A wall having a front surface directed forwardly of a liquid sending device 10 may be formed in a front portion of a storage container 100 instead of the bi-parting door 120. In this case, an intake port IN directed sidewardly of the wall is formed, whereby designability of a front portion of the liquid sending device 10 can be improved while the intake port IN is provided in the front portion of the liquid sending device 10.
(66) (c) In the above-mentioned embodiment, when the bi-parting door 120 is closed, the intake port IN opens to be directed in the direction perpendicular to the direction directed forwardly of the liquid sending device 10 from the inside of the storage container 100. More specifically, the intake port IN opens to be directed sidewardly of the liquid sending device 10. However, the direction in which the intake port IN opens is not limited to the above-mentioned example.
(67) In the door 120A, the intake port IN may open to be directed in the direction that intersects with the direction directed forwardly of the liquid sending device 10 from the inside of the storage container 100. Therefore, the intake port IN may be formed to open upwardly of the liquid sending device 10 or may be formed to open downwardly of the liquid sending device 10. In this case, in a case where the bi-parting door 120 is viewed from a position farther forward than the liquid sending device 10, the intake port IN is provided preferably not to be seen.
(68) The intake port IN may be formed to open obliquely and forwardly of the liquid sending device 10. Also in this case, desirability of the front portion of the liquid sending device 10 can be improved as compared to the case where the intake port IN opens forwardly of the liquid sending device 10.
(69) (d) While the filter FI is constituted by a plate-shape member in the above-mentioned embodiment, the present invention is not limited to this. The filter FI may have a shape other than a plate shape. For example, the filter FI may be columnar or cubic.
(70) (e) While the holding member 400 is provided attachably and detachably at the frame member 200 by the snap-fit mechanism 430 in the above-mentioned embodiment, the present invention is not limited to this. The holding member 400 may be configured to be attachable to and detachable from at least one of the frame member 200 and the cover member 300 with a screw.
(71) (f) The filter FI may be directly attached to the door 120A with a screw. In this case, the holding member 400 is not required.
(72) (g) The storage container 100 may include a single opening door instead of the bi-parting door 120. In this case, the single opening door has the configuration similar to that of the above-mentioned door 120A, whereby the effects similar to those of the example of the above-mentioned embodiment can be obtained.
(73) (h) The door 120A may be provided at the upper wall 110a or the lower wall 110b to turn around the turning axis LA in parallel with the horizontal direction.
(74) (i) The door 120B of the above-mentioned bi-parting door 120 may have the configuration similar to that of the door 120A. Further, the filter FI may be held at the door 120B by the holding member 400. In this case, a flow path of gas from the outside to the inside of the storage container 100 can be more largely ensured. Thus, heat dissipation efficiency is improved.
(75) (j) While the liquid sending device 10 according to the above-mentioned embodiment has the configuration in which the two pump devices PP are stored in the storage container 100, the configuration of the liquid sending device 10 is not limited to the above-mentioned example. For example, a liquid sending device 10 may have the configuration in which only one pump device PP is stored in the storage container 100. In this case, the liquid sending device 10 in which only one pump device PP is stored in a storage container 100 may be used in the liquid chromatograph 1 of
[6] Correspondences Between Constituent Elements in Claims and Parts in Preferred Embodiments
(76) In the following paragraphs, non-limiting examples of correspondences between various elements recited in the claims below and those described above with respect to various preferred embodiments of the present disclosure are explained.
(77) In the above-mentioned embodiment, the direction directed forwardly of the liquid sending device 10 from the inside of the storage container 100 is an example of a first direction, the direction directed toward one side of the liquid sending device 10 is an example of a second direction, the one side portion of the door 120A attached to the casing 110 to be turnable is an example of a first side portion of a door and the other side of the door 120A at which the intake port IN is provided is an example of a second side portion of a door.
(78) As each of constituent elements recited in the claims, various other elements having configurations or functions described in the claims can be also used.