METHOD FOR DETECTING PARTICLES OR AEROSOL IN A FLOWING FLUID, COMPUTER PROGRAM, AS WELL AS ELECTRICAL MEMORY MEDIUM
20220026338 · 2022-01-27
Inventors
Cpc classification
G01N21/718
PHYSICS
International classification
Abstract
A method for detecting particles or aerosol in a flowing fluid, using the principle of laser-induced incandescence. The method includes the following steps: a. focusing a laser light originating from a laser in a spot; b. conducting a fluid which includes particles or aerosol through the spot; c. detecting a thermal radiation originating from the spot with the aid of a detector; and d. evaluating a variable which is provided by the detector and characterizes the detected thermal radiation within time intervals, the duration of the time intervals being dependent on a velocity of the fluid.
Claims
1-14. (canceled)
15. A method for detecting particles or aerosol in a flowing fluid, using laser-induced incandescence, the method comprising the following steps: a. focusing a laser light originating from a laser in a spot; b. conducting the fluid which includes particles or aerosol through the spot; c. detecting a thermal radiation originating from the spot using a detector; and d. evaluating a variable which is provided by the detector and characterizes the detected thermal radiation within time intervals, a duration of the time intervals being dependent on a velocity of the fluid.
16. The method as recited in claim 15, wherein at least several of the time intervals overlap.
17. The method as recited in claim 16, wherein the duration of the time intervals is greater than an expected full width at half maximum (FWHM) of the variable characterizing the thermal radiation.
18. The method as recited in claim 17, wherein the duration of the time intervals is 1 to 2 times the expected FWHM.
19. The method as recited in claim 18, wherein the duration of the time intervals is 1.5 times the expected FWHM.
20. The method as recited in claim 16, wherein an overlapping time period of the time intervals corresponds to at least half the duration of the time interval.
21. The method as recited in claim 16, wherein a particle is considered to be detected when the variable characterizing the thermal radiation or ascertained from the variable at least reaches one limiting value or multiple different limiting values within a time interval.
22. The method as recited in claim 16, wherein at least several consecutive ones of the time intervals do not overlap.
23. The method as recited in claim 16, wherein at least several consecutive ones of the time intervals do not overlap and directly adjoining one another.
24. The method as recited in claim 22, wherein a particle is considered to be detected when the variable characterizing the thermal radiation or ascertained from the variable at least reaches a limiting value within at least two time intervals directly following one another.
25. The method as recited in claim 21, wherein the limiting value depends on an expected background signal.
26. The method as recited in claim 15, wherein the variable characterizing the thermal radiation is a continuous variable.
27. The method as recited in claim 15, wherein the variable characterizing the thermal radiation is an integral formed from a continuous variable ascertained within a time interval of the time intervals.
28. The method as recited in claim 15, wherein the variable characterizing the thermal radiation is a discontinuous variable formed by pulse-like signals, and a sum of the pulse-like signals is formed within a time interval of the time intervals.
29. The method as recited in claim 15, wherein the velocity of the fluid is ascertained from full width at half maximum (FWHM) of large particles, and the ascertained velocity is then used to determine a length of the time intervals for detection of small particles.
30. An electrical memory medium, for an evaluation unit for use in an exhaust gas system of an internal combustion engine, on which is stored a computer program for detecting particles or aerosol in a flowing fluid, using laser-induced incandescence, the computer program, when executed by the evaluation unit, causing the evaluation unit to perform the following steps: a. focusing a laser light originating from a laser in a spot; b. conducting the fluid which includes particles or aerosol through the spot; c. detecting a thermal radiation originating from the spot using a detector; and d. evaluating a variable which is provided by the detector and characterizes the detected thermal radiation within time intervals, a duration of the time intervals being dependent on a velocity of the fluid.
31. A state machine in the form of an ASIC, the ASIC being configured to detect particles or aerosol in a flowing fluid, using laser-induced incandescence, the state machine being configured to: a. focus a laser light originating from a laser in a spot; b. conduct the fluid which includes particles or aerosol through the spot; c. detect a thermal radiation originating from the spot using a detector; and d. evaluate a variable which is provided by the detector and characterizes the detected thermal radiation within time intervals, a duration of the time intervals being dependent on a velocity of the fluid.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
[0031]
[0032]
[0033]
[0034]
[0035]
[0036]
[0037]
[0038]
[0039]
[0040]
[0041] Functionally equivalent elements and areas bear the same reference numerals in the following description.
DETAILED DESCRIPTION OF EXAMPLE EMBODIMENTS
[0042]
[0043]
[0044] The dimensions of spot 22 are in the range of several μm, in particular, in the range of no more than 200 μm, so that particles 12 passing through spot 22 are excited to emit evaluatable radiation outputs, be it by laser-induced incandescence or by chemical reactions (in particular, oxidation). As a result, it may be assumed that no more than one particle 12 at a time is present in spot 22, and that an instantaneous measuring signal of particle sensor 16 only stems from this no more than one particle 12.
[0045] The measuring signal is generated by a detector 26 which is situated in particle sensor 16 in such a way that it detects radiation 14, in particular, thermal radiation, originating from particle 12 passing through spot 22. In this respect, the measuring signal provided by detector 26 is a variable characterizing the detected thermal radiation. For this purpose, detector 26 preferably includes at least one photodiode 26.1 which detects the thermal radiation and enables a quantification (intensity as a function of the time). In this way, an individual particle measurement becomes possible, which allows pieces of information about particle 12, such as size and velocity, to be extracted. For example, a cost-effective silicon photomultiplier (SiPM) or a single-photon avalanche diode (SPAD diode) is possible as photodiode 26.1.
[0046] As an alternative, the detector may also include a multi-pixel photon counter (MPPC).
[0047] As a result, it is already possible to detect a light signal which is generated by a particularly small particle and thus is extremely small, which is formed by a few 10 photons, for example. In this way, the dimensions of particles which are just barely still detectable decreases to a lower detection limit of up to 10 nm.
[0048] It is quite possible that the laser of laser module 18 is modulated or switched on and off (duty cycle <100%). However, it remains preferred that the laser of laser module 18 is a CW laser. This allows the use of cost-effective semiconductor laser elements (laser diodes), which reduces the cost of the entire particle sensor 16 and drastically simplifies the activation of laser module 18 and the evaluation of the measuring signal. However, the use of pulsed lasers is not precluded.
[0049]
[0050] Thermal radiation 14 (dotted arrows) of a particle 12 excited in spot 22 by laser light 10, in turn, reaches dichroic mirror 30 again through lens 24, where it is deflected, in the present example by way of example by 90°, passes through a focusing lens 31 and, through a filter 32 (which is not necessarily present), reaches photodiode 26.1 of detector 26 (it is also possible that the thermal radiation first passes through a filter, and then through a focusing lens). Filter 32 is designed in such a way that it filters out the wavelengths of laser light 10. The interfering background is thus reduced by filter 32. The exemplary embodiment including filter 32 specifically takes advantage of the narrow bandwidth of laser sources (e.g., laser diodes) by filtering out precisely this narrow bandwidth upstream from detector 26. The use of a simple edge filter is also possible. As a result, the signal-to-noise ratio improves.
[0051]
[0052] Particle sensor 16 includes a system made up of an outer protective tube 44 and an inner protective tube 46. The two protective tubes 44, 46 preferably have a general cylinder shape or prism shape. The base areas of the cylinder shapes are preferably circular, elliptic, or polygonal. The cylinders are preferably coaxially situated, the axes of the cylinders being aligned transversely to the flow of exhaust gas 48. Inner protective tube 46 protrudes in the direction of the axes beyond outer protective tube 44 into flowing exhaust gas 48. At the end of the two protective tubes 44, 46 which faces away from the flowing exhaust gas 48, outer protective tube 44 protrudes beyond inner protective tube 46. The inside diameter of outer protective tube 44 is preferably so much larger than the outside diameter of inner protective tube 46 that a first flow cross-section results between the two protective tubes 44, 46. The inside diameter of inner protective tube 46 forms a second flow cross-section.
[0053] As a result of this geometry, exhaust gas 48 enters the system of the two protective tubes 44, 46 via the first flow cross-section, then changes its direction at the end of protective tubes 44, 46 which faces away from exhaust gas 48, enters inner protective tube 46, and is suctioned out of it by exhaust gas 48 flowing past (arrows denoted by reference numeral 49). A laminar flow results in inner protective tube 46 in the process. This system of protective tubes 44, 46 is attached at or in an exhaust gas tube (not shown), together with soot particle sensor 16, transversely to the flow direction of exhaust gas 48.
[0054] Soot particle sensor 16 additionally includes laser 18, which preferably generates parallel laser light 10, as is shown in the present example. The beam splitter, in the form of dichroic mirror 30 already mentioned above by way of example, is situated in the beam path of the parallel laser light 10. A portion of laser light 10 passing through beam splitter 30 without deflection is focused by optical element 20 into the very small spot 22 in the interior of inner protective tube 46. In this spot 22, the light intensity is high enough to heat particles 12 transported together with exhaust gas 48 at the velocity of the flow in the inner protective tube (arrow 49) to several thousand degrees Celsius, so that the heated particles 12 emit significant radiation 14 in the form of thermal radiation.
[0055] Radiation 14 is in the near infrared and visible spectral range, for example, however it is not limited to this spectral range.
[0056] A portion of this undirected radiation 14 emitted in the form of thermal radiation (“LII light”) is detected by optical element 20, and deflected via beam splitter 30 and directed at detector 26 via lens 31 and filter 32. This configuration has the particularly important advantage that only a single optical access to exhaust gas 48 is required, since the same lens system, in particular, the same optical element 20, including lens 24 is used for the generation of spot 22 and for the detection of thermal radiation 14 originating from particle 12.
[0057] In the case of the subject matter of
[0058] Particle sensor 16 preferably includes a first part 16.1 exposed to the exhaust gas, and a second part 16.2 not exposed to the exhaust gas, which includes the optical components of particle sensor 16. Both parts are separated by a partition 16.3, which extends between protective tubes 44, 46 and the optical elements of particle sensor 16. Wall 16.3 is used to isolate the sensitive optical elements from the hot, chemically aggressive and “dirty” exhaust gas 48. In partition 16.3, a protective window 54 is provided in the beam path of laser light 10, through which laser light 10 is incident into exhaust gas 48 or flow 49 and via which thermal radiation 14 originating from spot 22 is able to be incident onto optical element 20 and, from there, via beam splitter 30 and filter 32, onto detector 26. It is also possible that particularly sensitive components of the particle sensor, for example the laser and the detector, are accommodated in a separate housing, and that, for example, optical waveguides, for example in the form of one or multiple glass fiber(s), are used for transporting the laser light and/or the thermal radiation to/from the optical components situated at the exhaust gas.
[0059] Particle sensor 16 may furthermore include an evaluation unit 56, which is programmed to carry out, based on the signals of the detector 26, an evaluation of the variable which is provided by the detector 26 and characterizes the detected thermal radiation. For this purpose, evaluation unit 56 includes further components which are not shown in greater detail, for example a microprocessor and an electrical memory medium on which a computer program for executing a method explained hereafter is stored.
[0060] Initially, reference is made to
[0061] When a particle emits thermal radiation 14, the measuring signal 58, which otherwise remains at a constant low level, increases to an elevated value (maximum Smax) and thereafter drops again. A full width at half maximum (FWHM) is denoted in the figures by a double arrow bearing reference numeral 60. Time intervals, which bear reference numerals 62a, 62b and 62c, are denoted in
[0062] It is furthermore shown in
[0063] Duration 64 of time intervals 62a through c is variable in the present example. It depends on the expected full width at half maximum 60. The expected full width at half maximum 60, in turn, depends on the instantaneous velocity of flow 49 of exhaust gas 48 in spot 22, and thus on the expected possible exposure time of a particle 12 in spot 22. In the application of an internal combustion engine described by way of example in the present example, the velocity of flow 49 of exhaust gas 48 in inner protective tube 46 may, in turn, be ascertained, or at least estimated, based on the instantaneous operating state of the internal combustion engine, for example based on an instantaneous rotational speed and an instantaneous torque, and based on the geometry of outer protective tube 44 and inner protective tube 46.
[0064] It is also possible to determine the expected FWHM from the signals of large particles occurring in a temporally adjoining manner, which have a high signal-to-noise (SNR) ratio, and thus are not so much dependent on the method described here.
[0065] The dependence of full width at half maximum 60, and thus also of duration 64 of time intervals 62a through c, on the velocity of flow 49 of exhaust gas 48 is such that, at a comparatively low velocity of flow 49 of exhaust gas 48, the expected full width at half maximum 60, and thus also duration 64, is rather large (
[0066] An evaluation of measuring signal 58 always only takes place in each case within a time interval 62a through c. During the evaluation, for example, an integral of measuring signal 58 is formed within the respective time interval 62a through c, i.e., the area beneath measuring signal 58 within the boundaries of the respective time interval 62a through c is calculated. This integral (“integral value”) is thus a variable which is ascertained from the variable which characterizes thermal radiation 14. The integral value obtained for each time interval 62a through c is then compared to a limiting value. A particle 12 is considered to be detected when the integral value reaches or exceeds the limiting value.
[0067] An alternative type of the evaluation is shown in
[0068] In all above-described methods, the limiting value, which when reached or exceeded allows the presence of a particle 12 to be inferred, may depend on an expected background signal (noise).
[0069]
[0070] The method for detecting particles 12 described in general terms above is now again explained with reference to
[0071] As was already mentioned above, detector 26 provides a measuring signal 58, which overall is evaluated in an evaluation block 80 shown in dotted form. Specifically, in a block 82 the integral beneath measuring signal 58 is formed (in the case of a continuous measuring signal 58) in each time interval 62a through c, or the number of individual photon pulses 58 within each time interval 62 is ascertained (in the case of a discontinuous measuring signal 58). In a block 84, the ascertained integrals or ascertained numbers are compared to a limiting value. If the limiting value is reached or exceeded, the detection of a particle 12 is assumed in block 86. If, in contrast, the limiting value is not reached, it is assumed in block 88 that no particle 12 was detected. The method ends in a block 90.
[0072] Exhaust gas 48 is only one example of a possible measuring gas. The measuring gas may also be another gas or gas mixture. The method may also be used for other scenarios and usage areas (e.g., with portable emission monitoring systems, measurement of the indoor air quality, emissions of combustion systems (private, industrial)).
[0073] In the shown particle sensor, the laser light and/or the thermal radiation may also be entirely or partially conducted with the aid of optical waveguides.
[0074] In addition, the use of the method with arbitrary HV corona sensors which are to measure the particle/aerosol concentration in a gas would be possible.