SYSTEM AND PROCESS FOR CONCENTRATING BRIX IN A LIQUID
20230356103 · 2023-11-09
Inventors
Cpc classification
International classification
Abstract
There is provided a system and process for concentrating Brix in a liquid using a bimodal vacuum and pressurized falling film evaporator for producing concentrated nectar and/or concentrated syrup products, wherein in the vacuum mode the system produces concentrated nectar having a Brix of 60 to 70%, and wherein the pressurized mode, the system produces concentrated syrup having a Brix of 66 to 67%.
Claims
1. A system for concentrating Brix in a liquid, the system comprising: a first pump in fluid communication with a main inlet pipe for supplying the liquid into the system; a preheating unit for preheating the liquid at a first temperature (T1), the preheating unit comprising: a first inlet opening, a second inlet opening, a first outlet opening, and a second outlet opening, the first inlet opening being in fluid communication with the first pump for pumping the liquid into the preheating unit, the second inlet opening being in fluid communication with a second pump for draining condensed water through the preheating unit and through a second outlet opening, wherein the liquid flows through the first outlet opening and into the system at the first temperature (T1); a falling film evaporator in fluid communication with the first outlet opening of the preheating unit, wherein the falling film evaporator is adapted to produce a concentrated product, and wherein the falling film evaporator comprises: (i) a housing comprising an accommodating cavity, a plurality of heat exchange tubes extending along a longitudinal axis in relation to the housing, a top outlet opening, a bottom outlet opening in fluid communication with a recirculating pump, a first inlet opening in fluid communication with the first outlet opening of the preheating unit, a second inlet opening, and a first outlet opening in fluid communication with a depressurizing tank that is in fluid communication with the second pump of the preheating unit; (ii) a spray tube comprising a plurality of spraying nozzles for spaying the liquid inside the housing; and (iii) a heating unit for heating the liquid at a second temperature (T2); a mechanical vapor recompression unit for compressing and decompressing steam, the mechanical vapor recompression unit comprising: (i) a first inlet opening in fluid communication with the top outlet opening of the falling film evaporator; (ii) a first outlet opening in fluid communication with the second inlet opening of the falling film evaporator; and (iii) a spraying nozzle for spraying water into the first inlet opening of the mechanical vapor recompression unit to reduce the heat therein; and a main outlet and recirculation pipe in fluid communication with the recirculating pump, the main outlet and recirculation pipe comprising a Brix reading apparatus for measuring Brix of the concentrated nectar product and the concentrated syrup product, wherein the system and/or the mechanical vapor recompression unit is adapted to operate under a nectar mode for producing concentrated nectar product and under a syrup mode for producing concentrated syrup product.
2. The system of claim 1, further comprising a steam generator in fluid communication with the falling film evaporator for initiating a first production of steam.
3. The system of claim 1, wherein the first temperature (T1) is between 1° C. and 25° C.
4. The system of claim 3, wherein the first temperature (T1) is between 4° C. and 10° C.
5. The system of claim 1, wherein the second temperature (T2) is between 11° C. to 36° C.
6. The system of claim 1, wherein the first inlet opening of the mechanical vapor recompression unit operates under the nectar mode between −0.93 ATM gauge to −0.16 ATM gauge.
7. The system of claim 6, wherein the falling film evaporator is configured to heat the liquid at a third temperature (T3) between 37° C. to 103° C.
8. The system of claim 1, wherein the first outlet opening of the mechanical vapor recompression unit operates under the syrup mode between 0.068 ATM gauge and 1.02 ATM gauge.
9. The system of claim 8, wherein the falling film evaporator is configured to heat the liquid at a fourth temperature (T4) between 85° C. to 103° C.
10. The system of claim 1, wherein the falling film evaporator is a horizontal falling film evaporator.
11. The system of claim 1, wherein the liquid is selected from the group consisting of sap, sweet vegetal water solution and sweet raw vegetal water solution.
12. The system of claim 1, wherein the system is configured for continuous operation.
13. A process for concentrating Brix in a liquid, the process comprising the steps of: providing a system according to claim 2; providing the liquid; actioning the steam generator to initiate a first production of steam, wherein the resulting heat generated is directed from the steam generator to the falling film evaporator exiting through the first outlet opening of the falling film evaporator onto the depressurizing tank and pumped into the preheating unit by the second pump to heat the liquid at the first temperature (T1) to produce a first preheated liquid; feeding the first preheated liquid to the second preheating unit for preheating the liquid at the second temperature (T2) to produce a second preheated liquid; directing the second preheated liquid to the spray tube and spraying the second preheated liquid on the plurality of heat exchange tubes by actioning the plurality of spraying nozzles; and further comprising: gradually actioning the mechanical vapor recompression unit to function in the nectar mode, heating the second preheated liquid to the third temperature (T3) concentrating the Brix in the liquid between 60% to 70% and recovering the concentrated nectar product having a Brix value between 60% to 70%, or actioning the mechanical vapor recompression unit to function in the syrup mode, heating the liquid to the fourth temperature (T4) concentrating the Brix in the liquid between 66% and 67% and recovering the concentrated syrup product having a Brix value between 66% and 67%.
14. The process of claim 13, comprising performing at least one of: brix monitoring, maple sap Brix monitoring, permeate flow reading, pH monitoring and control, conductivity meter readings, preventive management, and high and low pressure protection.
15. A process for concentrating Brix in a liquid, the process comprising the steps of: providing the liquid; preheating the liquid to a first preheated temperature to produce a first preheated liquid; preheating the first preheated liquid to a second preheated temperature to produce a second preheated liquid; and further comprising: feeding the second preheated liquid to a falling film evaporator configured to function under a nectar mode and heating the second preheated liquid to a temperature between 37° C. and 103° C. to produce a concentrated nectar product having a Brix level between 60% and 70%, or feeding the second preheated liquid to a falling film evaporator configured to function under a syrup mode and heating the second preheated liquid to a temperature between 85° C. and 103° C. to produce a concentrated syrup product having a Brix level between 66% and 67%.
16. The process of claim 15, comprising performing at least one of: brix monitoring, maple sap Brix monitoring, permeate flow reading, pH monitoring and control, conductivity meter readings, preventive management, and high and low pressure protection.
17. The process of claim 15, wherein the liquid is selected from a group consisting of sap, sweet vegetal water solution and sweet raw vegetal water solution.
18. The process of claim 15, wherein the process further comprises recovering the concentrated nectar product or the concentrated syrup product in response to receiving a reading from a Brix measuring means.
19. A concentrated nectar product produced according to the process of claim 15, wherein the process comprises feeding the second preheated liquid to a falling film evaporator configured to function under a nectar mode and heating the second preheated liquid to a temperature between 37° C. and 103° C. to produce a concentrated nectar product having a Brix level between 60% and 70%, and wherein the concentrated nectar product is high in sugar content and its taste, nature and quality have not been altered.
20. A concentrated syrup product produced according to the process of claim 15, wherein the process comprises feeding the second preheated liquid to a falling film evaporator configured to function under a syrup mode and heating the second preheated liquid to a temperature between 85° C. and 103° C. to produce a concentrated syrup product having a Brix level between 66% and 67%, and wherein the concentrated syrup product has undergone Maillard reactions and is at least partially caramelized.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
[0017] Having thus generally described the nature of the present disclosure, reference will now be made to the accompanying drawings, showing by way of illustration example embodiments thereof and in which:
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DETAILED DESCRIPTION OF EMBODIMENTS
[0029] In the following description, the same numerical references refer to similar elements. Furthermore, for the sake of simplicity and clarity, namely so as to not unduly burden the figures with several reference numbers, not all figures contain references to all the components and features, and references to some components and features may be found in only one figure, and components and features of the present disclosure which are illustrated in other figures can be easily inferred therefrom. The embodiments, geometrical configurations, materials mentioned and/or dimensions shown in the figures are optional and are given for exemplification purposes only.
[0030] Moreover, it will be appreciated that positional descriptions such as “above”, “below”, “forward”, “rearward”, “left”, “right” and the like should, unless otherwise indicated, be taken in the context of the figures only and should not be considered limiting. The use of “including,” “comprising,” or “having” and variations thereof herein is meant to encompass the items listed thereafter and equivalents thereof as well as additional suitable items. Unless specified or limited otherwise, the terms “mounted,” “connected,” “supported,” and “coupled” and variations thereof are used broadly and encompass both direct and indirect mountings, connections, supports, and couplings and are thus intended to include direct connections between two members without any other members interposed therebetween and indirect connections between members in which one or more other members are interposed therebetween. Further, “connected” and “coupled” are not restricted to physical or mechanical connections or couplings. Additionally, the words “lower”, “upper”, “upward”, “down” and “downward” designate directions in the drawings to which reference is made.
[0031] It is to be understood that the phraseology and terminology employed herein is not to be construed as limiting and are for descriptive purpose only. The principles and uses of the teachings of the present disclosure may be better understood with reference to the accompanying description, figures and examples. It is to be understood that the details set forth herein do not construe a limitation to an application of the disclosure.
[0032] Furthermore, it is to be understood that where the claims or specification refer to “a” or “an” element, such reference is not to be construed that there is only one of that element. It is to be understood that where the specification states that a component, feature, structure, or characteristic “may”, “might”, “can” or “could” be included, that particular component, feature, structure, or characteristic is not required to be included.
[0033] Variants, examples and preferred embodiments of the present disclosure are described hereinbelow. According to one embodiment, there is a system and process for concentrating Brix in a liquid using a bimodal vacuum and pressurized falling film evaporator for producing concentrated nectar and/or concentrated syrup products, wherein in the vacuum or nectar mode the system produces concentrated nectar having a Brix of 60 to 70%, and wherein in the pressurized or syrup mode, the system produces concentrated syrup having a Brix of 66 to 67%. Also whenever numerical values, such as Brix percentage values, are referred to in this specification, these values imply and include variations of approximately more or less 10% of the stated numerical values.
[0034] In embodiments, the system of the present technology uses a falling film evaporator that works in conjunction with a vapor compression unit, such as a mechanical recompression unit or the like, adaptable to work under a nectar mode or under a syrup mode.
[0035] In embodiments, under the nectar mode, the system produces a concentrated product from the liquid, such as the sap of the maple tree or the sweet vegetal water, that is very close to the original starting liquid without significantly altering the very nature of the product (e.g. nutritional value), therefore without denaturing or altering the nutritional properties of a resulting concentrated product. The product is a concentrated nectar product, having a Brix value of 60% to 70%, or more. A person of skill in the art would appreciate that the nectar product has not undergone any, or has undergone very small occurrences of Maillard reactions. Therefore, the concentrated nectar product does not have the characteristic syrup taste (e.g. there is no caramelization taste due to cooking), as such, it may be used as a natural sweetening agent. This process may also allow for a quick return on investment with very low energy consumption.
[0036] In embodiments, under the syrup mode, the system produces a concentrated syrup product having a Brix value between 66% and 67%. The concentrated syrup product has undergone Maillard reactions due to the increase in temperature, thereby, having the characteristic syrup taste (e.g., there is caramelization taste due to the cooking of the sugars). This process may also allow for a quick return on investment with very low energy consumption due to the reutilization of the vapor produced in the system as a heat source.
[0037] Referring now to
[0038] Referring now to
[0039] The processes (10) and (20) may comprise, before the step of providing the liquid, filtering the liquid by means of an ultrafiltration unit to produce a filtered liquid. The processes (10) and (20) may comprise concentrating the liquid by means of a reverse osmosis concentrator to produce a high Brix liquid solution of about 15% to about 40% Brix.
[0040] In embodiments, the process may comprise performing at least one of: Brix monitoring, maple sap Brix monitoring, permeate flow reading, pH monitoring and control, conductivity meter readings, preventive management, and high and low pressure protection.
[0041] In embodiments, the process may produce a concentrated nectar product that is high in sugar content and its taste, nature and quality have not been altered.
[0042] In embodiments, the process may produce a concentrated syrup product that has undergone Maillard reactions and is at least partially caramelized.
[0043] It will be understood that the principles disclosed herein may be implemented with a variety of equipment and configurations, for example with different pressurization and depressurization means, without departing from the present teachings. Referring to
[0044] It will be understood that the processes (10), (20) and (1100), or other processes carried out according to the principles disclosed herein, need not be mutually exclusive. Accordingly, in some embodiments, the process (10) may be initially carried out to produce a quantity of nectar product in a vacuum configuration at a temperature T3. The vacuum configuration may be switched to a pressurized configuration by adapting the operating parameters of the recompression unit accordingly. The process (20) may then proceed by increasing the temperature of the liquid to T4 and causing at least some Maillard reactions to occur, yielding a concentrated syrup product. The system for implementing processes (10) and (20) provided herein may thus be bimodal.
[0045] Referring now to
[0046] Still referring to
[0047] Referring now to
[0048] It will also be understood that the heating unit (130) receives the liquid (110) from preheating unit (120), when preheating unit (120) is present, and may be configured for heat exchange between the environment inside the evaporator (140) and the liquid (110). Upon exiting heating unit (130), the liquid (110) may be at an intermediate, second temperature T2. The liquid (110) may then be fed into the evaporator (140) through nozzles or other acceptable inlet means suitable in the operation of a falling film evaporator. The pre-heating of liquid (110) using heat present in the cavity (143) of the evaporator (140) provides for increased efficiency of the evaporation step. In particular, a pre-heated liquid (110) will more readily attain the predetermined operating temperature upon contacting the environment of the cavity (143) and the heat exchange tubes. Accordingly, heat use and heat recycling in the system (1000) are improved.
[0049] Referring to
[0050] Referring back
[0051] When vapor recompression unit (160) is a mechanical vapor recompression unit, the heat use and heat recycling efficiency of the system (1000) are improved. The vapor recompression unit (160) receives steam or vapor from the evaporator (140), at least part of the steam or vapor resulting from the evaporation of a portion of the liquid (110). The vapor recompression unit (160) compresses the vapor or steam received from the evaporator (140), causing the temperature of the vapor or steam to increase. The resulting compressed vapor or steam is fed into the evaporator (140), thus providing a source of heat for the evaporation step.
[0052] It will be understood that the vapor recompression unit may be configured to operate at very low pressures, including at pressures approaching a vacuum, as well as under atmospheric, near-atmospheric or above-atmospheric pressures. For example, when the evaporator (140) operates in nectar mode, the vapor recompression unit (160) is configured to maintain a low pressure. When the evaporator (140) operates in syrup mode, the vapor recompression unit (160) may be configured to maintain a near-atmospheric pressure, for example a pressure higher than the pressure in nectar mode.
[0053] Still referring to
[0054] Still referring to
[0055] Still referring to
[0056] Still referring to
[0057] In embodiments, (T2) may be higher than (T1).
[0058] Still referring to
[0059] Still referring to
[0060] In accordance to an embodiment, the liquid (110) may be transformed into the concentrated nectar product (300) having a Brix value of 60% to 70%, corresponding to a Brix level of 60% to 70%.
[0061] In accordance to another embodiment, still referring to
[0062] Still referring to
[0063] Still referring to
[0064] In embodiments, and still referring to
[0065] Still referring to
[0066] In embodiments, and still referring to
[0067] In embodiments, and still referring to
[0068] In embodiments, the Brix reading apparatus comprises a refractometer (not shown).
[0069] In embodiments, the liquid (110) is selected from a group consisting of sap, sweet vegetal water solution and sweet raw vegetal water solution.
[0070] Turning now to
[0071] Now referring to
[0072] In embodiments, there is provided a process for concentrating Brix in a liquid (110), the process may comprise the steps of: providing the system (1000) (referred to in
[0073] The vapor recompression unit (160) may be configured for gradual actioning, for example by gradually lowering the pressure in the evaporator (140). Gradual reduction in pressure favors a slower release of gases dissolved in the liquid (110), thus reducing foaming.
[0074] In embodiments, the process using the system (1000) (referred to in
[0075] In embodiments, the process using the system (1000) (referred to in
[0076] In embodiments, the process using the system (1000) (referred to in
[0077] In embodiments, the process using the system (1000) (referred to in
[0078] The system (1000) may be configured to recover the concentrated products, for example a nectar product (300) and/or a syrup product (400) in response to a reading provided a Brix measuring means, for example in response to receiving a reading from a Brix meter (191). This process may be automated, for example through configuring a controller, such as controller (500), to actuate valves or other fluid direction means (not shown) to withdraw the liquid 110 from the main outlet and recirculation pipe (190) when the Brix reading on Brix meter (191) reaches a predetermined threshold.
[0079] The Brix meter may comprise any or several Brix measuring technologies, including but not limited to refractometry, microwave technology and others. For example, the Brix meter may be a microwave Brix meter.
[0080] The principles described herein provide an advantageous method and system for concentrating Brix in a liquid. For example, one advantage of the present disclosure comprises recovering concentrated products based on a Brix reading, for example a Brix reading provided in real time. This improves the precision, consistency and reliability of the concentrated products produced using the systems and methods of the present disclosure compared to current methods and systems of concentrating Brix in a liquid.
[0081] In another example, the principles described herein provide the possibility of continuous, rather than batch operation of an evaporator, for example a falling film evaporator for concentrating Brix in a liquid. Accordingly, a liquid (110) may be continuously fed to a system (1000) operating in vacuum or pressurized mode, the system (1000) being at or near an equilibrium, wherein the conditions of pressure, temperature and flowrate allow the overall Brix in the liquid (110) comprised within the system (1000) to remain at or close to the predetermined Brix level for a concentrated product, thus allowing for continuous feeding of the liquid (110) and continuous withdrawal of a concentrated product (300, 400) having a predetermined Brix level. Characteristics of a Brix concentration operation such as throughput and downtime are thus improved.
[0082] In another example, the systems and processes described herein provide improved liquid concentration means by allowing liquid concentration to proceed in at least two modes, i.e. at least vacuum and pressurized modes using the same equipment. Use of the equipment is thus more readily adapted to satisfy changes in market demand, for example by addressing the seasonality of syrup demand while maintaining the capacity for manufacturing a minimally caramelized sweetening product such as nectar.
[0083] The one or more embodiments described above are intended to be exemplary only.