Charged Particle Beam Device and Specimen Observation Method
20230343549 · 2023-10-26
Inventors
- Masahiro FUKUTA (Tokyo, JP)
- Tomoyo SASAKI (Tokyo, JP)
- Makoto Suzuki (Tokyo, JP)
- Masashi WADA (Tokyo, JP)
- Hiroshi Nishihama (Tokyo, JP)
Cpc classification
H01J37/244
ELECTRICITY
G01N23/2251
PHYSICS
H01J2237/24495
ELECTRICITY
International classification
H01J37/244
ELECTRICITY
H01J37/147
ELECTRICITY
Abstract
The present invention overcomes a trade-off between throughput, SNR, and spatial resolution in a charged particle beam device. Accordingly, a computer 18 sets at least one of a charged particle optical system and a detection system so as to modulate the intensity of signal charged particles or an electromagnetic wave detected by a detector 12 at a prescribed frequency. The charged particle optical system scans a specimen with a charged particle beam. The computer 18 generates an image or a signal profile by associating an irradiation position of the charged particle beam with a DC component of a signal acquired through synchronous detection of a detection signal from the detector at the irradiation position with a reference signal having a prescribed frequency.
Claims
1. A charged particle beam device comprising: a charged particle optical system including a charged particle source, one or more lenses configured to focus a charged particle beam from the charged particle source on a specimen, and a deflector configured to deflect the charged particle beam to scan the specimen; a detection system including a detector configured to detect signal charged particles or an electromagnetic wave emitted by irradiating the specimen with the charged particle beam; and a computer configured to control the charged particle optical system to scan the specimen with the charged particle beam and to generate an image or a signal profile based on a detection signal output from the detector when the detector detects signal charged particles or an electromagnetic wave emitted by irradiating an irradiation position corresponding to one pixel with the charged particle beam, wherein the computer controls at least one of the charged particle optical system or the detection system so as to modulate an intensity of the signal charged particles or the electromagnetic wave detected by the detector at a predetermined frequency, and generates the image or the signal profile by associating an irradiation position of the charged particle beam with a DC component of a signal acquired through synchronous detection of a detection signal from the detector at the irradiation position with a reference signal having the predetermined frequency, and the computer controls a phase difference between the detection signal from the detector and the reference signal for the synchronous detection to be fixed irrespective of the irradiation position of the charged particle beam.
2. The charged particle beam device according to claim 1, wherein the computer sets a period where the irradiation position corresponding to one pixel is irradiated with the charged particle beam to be a positive integer multiple of a modulation period of the intensity of the signal charged particles or the electromagnetic wave detected by the detector.
3. The charged particle beam device according to claim 1, wherein the charged particle optical system two-dimensionally scans the specimen by repeatedly scanning the specimen with the charged particle beam in a first direction while shifting the position in a direction perpendicular to the first direction, and the computer sets a period of time from start of scanning in the first direction at one position to start of scanning in the first direction at a next position to be a positive integer multiple of a modulation period of the intensity of the signal charged particles or the electromagnetic wave detected by the detector.
4. The charged particle beam device according to claim 1, wherein the charged particle optical system two-dimensionally scans the specimen by repeatedly scanning the specimen with the charged particle beam in a first direction while shifting the position in a direction perpendicular to the first direction, and at a timing of start of scanning in the first direction, the computer resets the modulation of the signal charged particles or the electromagnetic wave detected by the detector per scanning in the first direction such that the modulation of the intensity of the signal charged particles or the electromagnetic wave detected by the detector has the same phase.
5. The charged particle beam device according to claim 1, wherein the detection system includes a phase-sensitive detector configured to input the detection signal from the detector and the reference signal for the synchronous detection and a low-pass filter configured to output a DC component of an output signal of the phase-sensitive detector.
6. The charged particle beam device according to claim 5, wherein the detection system includes a phase adjuster configured to adjust a phase of the reference signal input to the phase-sensitive detector, and the computer adjusts a phase adjustment amount of the reference signal by the phase adjuster prior to the generation of the image or the signal profile.
7. The charged particle beam device according to claim 1, wherein the charged particle optical system modulates an intensity of the charged particle beam per unit area on the specimen at the predetermined frequency.
8. The charged particle beam device according to claim 7, wherein the charged particle optical system includes a signal generator configured to generate a control signal having the predetermined frequency and a chopper that is controlled based on the control signal generated by the signal generator, and the charged particle beam is pulsed in a period of the control signal generated by the signal generator.
9. The charged particle beam device according to claim 7, wherein the charged particle source is a photo-excitation electron source, the charged particle optical system includes a signal generator configured to generate a control signal having the predetermined frequency and a pulsed laser that is controlled based on the control signal generated by the signal generator, and the charged particle beam is a pulsed electron beam emitted when the photo-excitation electron source is irradiated with pulsed light that is output from the pulsed laser and has a period of the control signal generated by the signal generator.
10. The charged particle beam device according to claim 1, wherein the charged particle source is a photo-excitation electron source, the charged particle optical system includes a pulsed laser configured to output pulsed light and a photodetector, the charged particle beam is a pulsed electron beam emitted when the photo-excitation electron source is irradiated with the pulsed light that is output from the pulsed laser, and an output signal output from the photodetector when the photodetector detects the pulsed light output from the pulsed laser is set as the reference signal.
11. The charged particle beam device according to claim 1, wherein the detection system modulates the intensity of the signal charged particles or the electromagnetic wave detected by the detector at the predetermined frequency.
12. The charged particle beam device according to claim 11, wherein the detector includes a signal generator configured to generate a control signal having the predetermined frequency, a scintillator configured to convert electrons emitted by irradiating the specimen with the charged particle beam into light, and a photomultiplier tube configured to detect the converted light, and the detection system modulates a voltage applied to the scintillator at the predetermined frequency based on the control signal generated by the signal generator.
13. The charged particle beam device according to claim 1, wherein the detection system includes an amplifier configured to amplify the detection signal from the detector, and the detection signal from the detector that is amplified by the amplifier is filtered and subsequently undergoes the synchronous detection with the reference signal.
14. The charged particle beam device according to claim 1, wherein the computer converts the detection signal from the detector into a digital signal and takes in the digital signal, and a sampling frequency at which the computer converts the detection signal from the detector into a digital signal is two times or more of a modulation frequency of the intensity of the signal charged particles or the electromagnetic wave detected by the detector.
15. A specimen observation method using a charged particle beam device including a charged particle optical system, a detection system, and a computer, the charged particle optical system including a charged particle source, one or more lenses configured to focus a charged particle beam from the charged particle source on a specimen, and a deflector configured to deflect the charged particle beam to scan the specimen, the detection system including a detector configured to detect signal charged particles or an electromagnetic wave emitted by irradiating the specimen with the charged particle beam, and the specimen observation method comprising: allowing the computer to set at least one of the charged particle optical system or the detection system so as to modulate an intensity of the signal charged particles or the electromagnetic wave detected by the detector at a predetermined frequency; allowing the charged particle optical system to scan the specimen with the charged particle beam; allowing the computer to generate an image or a signal profile based on a detection signal output from the detector when the detector detects signal charged particles or an electromagnetic wave emitted by irradiating an irradiation position corresponding to one pixel with the charged particle beam; generating the image or the signal profile by associating an irradiation position of the charged particle beam with a DC component of a signal acquired through synchronous detection of a detection signal from the detector at the irradiation position with a reference signal having the predetermined frequency; and controlling a phase difference between the detection signal from the detector and the reference signal for the synchronous detection to be fixed irrespective of the irradiation position of the charged particle beam.
16. The specimen observation method according to claim 15, wherein the computer sets a period where the irradiation position corresponding to one pixel is irradiated with the charged particle beam to be a positive integer multiple of a modulation period of the intensity of the signal charged particles or the electromagnetic wave detected by the detector.
17. The specimen observation method according to claim 16, wherein the computer sets a period where the irradiation position corresponding to one pixel is irradiated with the charged particle beam to be a positive integer multiple of a modulation period of the intensity of the signal charged particles or the electromagnetic wave detected by the detector, the positive integer multiple varying depending on areas of the specimen.
18. The specimen observation method according to claim 15, wherein the computer adjusts a phase difference between the detection signal from the detector and the reference signal for the synchronous detection prior to the generation of the image or the signal profile.
19. A charged particle beam device comprising: a charged particle optical system including a charged particle source, one or more lenses configured to focus a charged particle beam from the charged particle source on a specimen, and a deflector configured to deflect the charged particle beam to scan the specimen; a detection system including a detector configured to detect signal charged particles or an electromagnetic wave emitted by irradiating the specimen with the charged particle beam; a computer configured to control the charged particle optical system to scan the specimen with the charged particle beam and to generate an image or a signal profile based on a detection signal output from the detector when the detector detects signal charged particles or an electromagnetic wave emitted by irradiating an irradiation position corresponding to one pixel with the charged particle beam, wherein the computer controls at least one of the charged particle optical system or the detection system so as to modulate an intensity of the signal charged particles or the electromagnetic wave detected by the detector at a predetermined frequency, and generates the image or the signal profile by associating an irradiation position of the charged particle beam with a DC component of a signal acquired through synchronous detection of a detection signal from the detector at the irradiation position with a reference signal having the predetermined frequency, and the computer converts the detection signal from the detector into a digital signal and takes in the digital signal based on a sampling signal, sets a frequency of the sampling signal to be two times or more of a modulation frequency of the intensity of the signal charged particles or the electromagnetic wave detected by the detector, and executes a control such that the modulation of the intensity of the signal charged particles and the electromagnetic wave detected by the detector and the sampling signal are synchronized with a predetermined phase difference.
20. The charged particle beam device according to claim 19, wherein the predetermined phase difference is determined such that a pixel value of the image or the signal profile is maximized.
Description
BRIEF DESCRIPTION OF DRAWINGS
[0020]
[0021]
[0022]
[0023]
[0024]
[0025]
[0026]
[0027]
[0028]
[0029]
[0030]
[0031]
[0032]
[0033]
[0034]
[0035]
[0036]
DESCRIPTION OF EMBODIMENTS
[0037] An electron microscope (frequency modulation SEM) will be described as an example of a charged particle beam device according to the present disclosure.
First Embodiment
[0038]
[0039] A primary beam 2 emitted from the electron emission unit 1 is accelerated by the acceleration electrode 3 and is focused by the focusing lens 4. Regarding the primary beam, the amount of a current is adjusted by the aperture 5, and then the beam intensity per unit area on a specimen is frequency-modulated by the chopper 6. In this example, the primary beam 2 is modulated based on a deflection voltage (control signal) of a square wave from the signal generator 15. The chopper 6 can be configured using a blanking deflector having an aperture, and the beam intensity is modulated (the primary beam 2 is pulsed) by controlling whether or not to allow the primary beam 2 to pass through the aperture depending on the deflection amount of the deflector. The chopper 6 is disposed at a cross position of the primary beam by the focusing lens 4 (an object point position of the lower focusing lens 7) such that noise generated by modulation can be reduced.
[0040] The frequency-modulated primary beam 2 is then focused by the focusing lens 7, passes through the objective lens 9, and is emitted to a specimen 10. In addition, the deflector 8 is disposed between the focusing lens 7 and the objective lens 9 and deflects the primary beam 2 to scan the specimen 10. The size or material of the specimen 10 is not limited. For example, the specimen 10 may be a semiconductor wafer. By irradiating the specimen 10 with the primary beam 2, signal electrons 11 are emitted due to an interaction between the primary beam 2 and the specimen 10. The signal electrons 11 are detected by the signal detector 12. The beam intensity of the primary beam 2 is frequency-modulated such that the intensity of the signal electrons 11 detected by the signal detector 12 is also frequency-modulated. A detection signal from the signal detector 12 is amplified by the amplifier 13 and then input to the phase-sensitive detector 14. Examples of the signal detector 12 include an E-T detector. In the E-T detector, the signal electrons can be efficiently detected using a scintillator and a photomultiplier tube.
[0041] A reference signal having the same period as the deflection voltage for modulating the primary beam 2 is also input from the signal generator 15 to the phase-sensitive detector 14. This reference signal is transmitted from the signal generator 15, the phase of the reference signal is adjusted by the phase adjuster 16, and then the reference signal is input to the phase-sensitive detector 14.
[0042] In the phase-sensitive detector 14, multiplication (synchronous detection, phase detection) is performed using the two signals including the detection signal from the signal detector 12 and the reference signal from the signal generator 15. By performing the synchronous detection, the signal can be detected with a high SNR.
[0043] The detection signal is represented by Asin(ω.sub.st + θ.sub.s), the reference signal is represented by sin(ω.sub.rt + θ.sub.r), and the noise is represented by N(ω) sin (ωt). Here, the noise is mainly noise that is superimposed on the detection signal in the signal detector 12 or the amplifier 13. A represents the amplitude of the detection signal with respect to 1 that is the amplitude of the reference signal, ω.sub.s represents the frequency of the detection signal, θ.sub.s represents the phase of the detection signal, t represents the time, ω.sub.r represents the frequency of the reference signal, θ.sub.r represents the phase of the reference signal, N(ω) represents the amplitude of the noise, and ω represents the frequency of the noise. The amplitude of the noise has frequency dependence and thus is represented by a function of the frequency ω.
[0044] In the phase-sensitive detector 14, the detection signal and the reference signal to which the noise is added are multiplied by each other, and an output signal S of the phase-sensitive detector 14 is represented by (Expression 1).
[Expression 1]
[0045] The product of the detection signal and the calculation signal to which the noise is added can be modified as in (Expression 1) using a trigonometric identity. Here, the frequencies of the detection signal and the reference signal are the same and thus can be represented by ω.sub.s = ω.sub.r. Therefore, (Expression 1) can be modified into (Expression 2).
[Expression 2]
[0046]
[0047] In addition, the third term in (Expression 2) can also be modified as in (Expression 3) using a trigonometric identity.
[Expression 3]
[0048]
[0049] The output signal S of the phase-sensitive detector 14 is input to the low-pass filter 17, and a DC component S.sub.DC thereof is extracted. In (Expression 3), the DC component in the third term of (Expression 2) is ω = ω.sub.r. Therefore, when dω represents the bandwidth, the DC component S.sub.DC is represented by (Expression 4).
[Expression 4]
[0050]
[0051] In (Expression 4), when the phase θ.sub.s of the detection signal and the phase θ.sub.r of the reference signal are matched to each other, the first term is A/2, and the noise remaining as the second term is only the noise component of the frequency ω.sub.r. Accordingly, the frequency ω.sub.r of the reference signal, that is, the modulation frequency of the primary beam 2 is set to a frequency band having a low noise (for example, a high frequency band in the E-T detector), and the reference signal of which the phase θ.sub.r is adjusted to match the phase θ.sub.s of the detection signal by the phase adjuster 16 is input to the phase-sensitive detector 14, so that the amplitude A of the detection signal can be acquired with a high SNR.
[0052] In the computer 18, the DC component S.sub.DC is extracted from the low-pass filter 17 and is associated with the irradiation position of the primary beam 2 on the specimen (corresponding to a pixel position of an image or a signal profile) to form a SEM image or a signal profile. This way, the detection signal can be obtained with a high SNR. Therefore, a signal acquisition interval (sampling time) of the output signal of the low-pass filter 17 in the computer 18 may be set irrespective of the modulation frequency of the signal generator 15, and data may be acquired once for each pixel.
[0053]
[0054] The detection signal of the signal electrons 11 generated from the specimen 10 by irradiation with the pulsed primary beam 120 is input to the phase-sensitive detector 14 and is processed as in the device configuration of
[0055]
[0056]
[0057] Regarding a beam modulation period T.sub.M on the specimen indicated in the primary beam intensity 22, the beam modulation period T.sub.M and the primary beam dwell time T.sub.s are adjusted such that the beam modulation period T.sub.M is shorter than the primary beam dwell time T.sub.s per pixel.
[0058] The detection signal 25 is input to the phase-sensitive detector 14 in a state where a detection delay D.sub.D from the modulation of the primary beam intensity 22 occurs. The reference signal 27 is also input to the phase-sensitive detector 14, and a phase difference θ.sub.D-R between the reference signal 27 and the detection signal 25 is present. The phase adjuster 16 delays the reference signal to be input to the phase-sensitive detector 14, and inputs the reference signal to the phase-sensitive detector 14 in a state where the phase difference θ.sub.D-R between the detection signal and the reference signal is 0. Accordingly, when the primary beam dwell time T.sub.s is a positive integer multiple of the beam modulation period T.sub.M, the phase adjustment amounts by the phase adjuster 16 at the irradiation positions corresponding to respective pixels can be made the same. In addition, since the intensities of electron beams with which respective pixels are irradiated can be made the same, an effect of suppressing a variation in the obtained signal amount or damage can also be obtained.
[0059]
[0060] During the two-dimensional scanning with the primary beam 2, as illustrated in an enlarged view 30, the primary beam dwell time T.sub.s per pixel is set to be longer than the beam modulation period T.sub.M on the specimen. Due to the same reason as that of the one-dimensional scanning illustrated in
[0061] As described above, when the primary beam dwell time T.sub.s per pixel is not a positive integer multiple of the beam modulation period T.sub.M and when the X-direction scanning period T.sub.L is not a positive integer multiple of the beam modulation period T.sub.M, the phase difference θ.sub.D-R between the detection signal 25 and the reference signal 27 varies depending on the beam irradiation positions. This means that even when the primary beam dwell time T.sub.S where the primary beam 2 is emitted is fixed, the intensity of the primary beam 2 is modulated such that the amount of an irradiation probe current at the irradiation position or the number of electrons in the dwell period varies depending on the irradiation positions. This way, the variation in the phase difference θ.sub.D-R generates a noise component, which leads to deterioration in the SEM image. Accordingly, in order to improve the spatial resolution of the SEM image, it is desirable to control the scanning and the modulation of the primary beam 2 such that the phase difference θ.sub.D-.sub.R is fixed at all of the irradiation positions of the primary beam 2.
[0062] This way, in the frequency modulation SEM according to the present embodiment, by modulating the primary beam at the frequency in a high frequency band where the noise of the detector is low, the signal component is detected at the modulation frequency where the amount of the signal component is sufficiently more than that of the noise component. Accordingly, an image can be generated with a higher SNR than that of a SEM image in the related art.
[0063] In the frequency modulation SEM according to the present embodiment, the SNR of the signal is significantly improved. Therefore, the acquisition time of one image can be reduced, which contributes to the improvement of throughput. For example, in the SEM in the related art, in order to improve the SNR of an image, it is necessary to increase a cumulative number of sheets, to increase the primary beam dwell time T.sub.S per pixel, or to increase the amount of a probe current. On the other hand, in the frequency modulation SEM, the detection signal can be obtained with a high SNR even without integrating images or increasing the primary beam dwell time T.sub.S. A decrease in the image acquisition time for integration or in the primary beam dwell time T.sub.S leads to the improvement of throughput and a decrease in damage to the specimen. In addition, since it is not necessary to increase the amount of a probe current, there is an advantageous effect in that deterioration in spatial resolution or charging caused by an increase in the amount of a probe current also does not occur. That is, the trade-off between the three performances including throughput, SNR, and spatial resolution can be resolved.
[0064] In particular, in the measurement or the inspection of a semiconductor wafer, charge-up of a specimen or damage to a specimen or carbon contamination caused by irradiation with the primary beam is a problem. By reducing the number of irradiation electrons per irradiation position, damage or deformation such as charge-up or shrink, adhesion of carbon contamination, and the like can be significantly reduced. Therefore, more accurate dimensional measurement or improvement of defect detection rate can be achieved.
[0065] Various modifications can be made for the frequency modulation SEM according to the present disclosure and will be described below.
(First Modification Example)
[0066]
(Second Modification Example)
[0067] Even when the phase difference θ.sub.D-R is set to be the same at all of the irradiation points of the primary beam 2 using the control methods illustrated in
[0068] In the second modification example, the phase adjustment amount of the phase adjuster 16 can be automatically controlled such that the phase difference θ.sub.D-R at an irradiation position corresponding to a pixel is corrected to 0 in the phase-sensitive detector 14. In the device configuration illustrated in
(Third Modification Example)
[0069] In order to extract the DC component S.sub.DC from the output signal of the phase-sensitive detector 14 at a higher speed, a sample hold circuit 81 may be used instead of the low-pass filter 17.
[0070] The signal output from the low-pass filter 17 has a low SNR, but the SNR of the signal is significantly improved as compared to the SEM in the related art. In the frequency modulation SEM using the sample hold circuit 81, only the maximum value and the minimum value in one period of the reference signal need to be acquired. Therefore, the primary beam dwell time T.sub.S per pixel and the beam modulation period T.sub.M can be made the same. As a result, the primary beam dwell time T.sub.S per unit pixel can be further reduced, and thus higher throughput and lower damage can be achieved.
[0071] The method of extracting the DC component S.sub.DC from the output signal of the phase-sensitive detector 14 using the sample hold circuit 81 has been described. However, the same process can be performed using a method of directly inputting the output signal of the phase-sensitive detector 14 to the computer 18, converting the output signal into a digital signal, and detecting a peak.
(Fourth Modification Example)
[0072] The configuration example of the frequency modulation SEM can be implemented using the chopper 6 or the photo-excitation electron source 121 when the frequency modulation of the primary beam 2 and 120 is a square wave. As described above, the intensity modulation of the primary beam 2 does not need to be a square wave and may be a sine wave.
[0073] The voltage applied to the acceleration electrode 111 is not limited, and even by frequency-modulating a voltage applied to a deceleration electrode 112, a retarding voltage applied to the observation specimen 10, a voltage applied to the electron emission unit 1, a current applied to the focusing lenses 4 and 7 or the objective lens 9, or the like, the conditions for irradiating the specimen with the primary beam 2 can be modulated, and the intensity of the primary beam 2 per unit area can be modulated.
(Fifth Modification Example)
[0074] In the above-described embodiment or the modification examples, by modulating the primary beam 2, the intensity of the signal electrons 11 emitted is frequency-modulated. On the other hand, the SNR can be improved by frequency-modulating the detection system that detects the signal electrons 11 instead of the electron optical system.
[0075] In this configuration, by using the scintillator that responds to the scintillator 91 at a high speed, the scanning speed can be increased. The response speed of the scintillator, that is, the extinction time and the emission intensity have a trade-off relationship. Accordingly, in order to implement high-speed imaging in the SEM in the related art, even when an attempt to increase the scanning speed of the primary beam is made using the scintillator having a high response speed, the scintillator having a high response speed has a weak emission intensity and a poor SNR. Therefore, the scanning speed cannot be sufficiently increased or the number of images integrated needs to be increased, and thus, there is a limit in reducing the imaging time. On the other hand, in the frequency modulation SEM, the SNR can be improved by the frequency modulation. Therefore, the scintillator having a high response speed (for example, a scintillator having an extinction time of 10 ns or shorter) can be used in the signal detector 90. As a result, not only further improvement of throughput but also low-charging observation and low-contamination observation can be achieved.
[0076] The configuration is not limited to the frequency modulation of the voltage applied to the scintillator 91, and when an energy filter or the like for changing the collection efficiency of the signal electrons is disposed before the signal detector 90, it is also possible to frequency-modulate the detection signal by frequency-modulating the condition of the energy filter.
[0077] The fifth modification example can also be combined with another embodiment. In this case, the frequency modulation SEM performs both of the modulation of the primary beam 2 and the modulation of the detection system that detects the signal electrons 11. For example, the signal generator 15 is shared in the electron optical system and the detection system, and the control signal from the signal generator 15 is configured to be input to each of the chopper 6 and the scintillator 91. Here, for example, the phase adjuster or a delay circuit that can adjust the amount of delay is provided in at least one of the electron optical system or the detection system such that a phase difference between a phase for modulating the electron optical system and a phase for modulating the detection system can be adjusted. The signal generator may also be provided in each of the electron optical system and the detection system, and a method of controlling the phase difference is not particularly limited.
[0078]
[0079] In the example of
(Sixth Modification Example)
[0080] Instead of making the primary beam dwell time T.sub.S per pixel the same at all of the beam irradiation positions, the primary beam dwell time T.sub.S per pixel or the beam modulation period T.sub.M can change depending on locations in a two-dimensional plane to be scanned. Note that the values are set such that the relationship where the primary beam dwell time T.sub.S per pixel is a positive integer multiple of the beam modulation period T.sub.M is maintained even after the change. In addition, even when the X-direction scanning period T.sub.L changes depending on scanning lines, the X-direction scanning period T.sub.L is controlled to be a positive integer multiple of the beam modulation period T.sub.M or the modulation is reset to have the same phase for each of the scanning lines.
[0081]
[0082]
[0083]
Second Embodiment
[0084] In the first embodiment, the example where the phase-sensitive detector performs the synchronous detection using an analog signal is described. On the other hand, a computer can also perform the synchronous detection using digital processing. In the second embodiment, a frequency modulation SEM using the digital processing (hereinafter, referred to as “digital frequency SEM”) will be described.
[0085]
[0086] The functional blocks relating to the synchronous detection of the digital frequency modulation SEM include an AD conversion unit 73, a synchronous detection unit 74, a signal generation unit 75, a phase adjustment unit 76, a low-pass filter 77, and a control unit 78. The synchronous detection unit 74, the signal generation unit 75, the phase adjustment unit 76, the low-pass filter 77, and the control unit 78 are functional blocks corresponding to the phase-sensitive detector 14, the signal generator 15, the phase adjuster 16, the low-pass filter 17, and the computer 18 of the frequency modulation SEM illustrated in the first embodiment, respectively, and the description thereof will not be repeated. In the frequency modulation SEM, the output of the low-pass filter 17 is converted into a digital signal, and the digital signal is taken into the computer 18. On the other hand, in the digital frequency modulation SEM, the output of the amplifier 13 is converted into a digital signal by the AD conversion unit 73, and the detection signal as the digital signal is taken into the computer 71 based on a sampling signal.
[0087]
[0088] The detection signal as the digital signal converted by the AD conversion unit 73 is sampled based on the sampling signal and the synchronous detection is performed by the synchronous detection unit 74. As illustrated in
[0089] By adjusting a phase difference between the detection signal and the sampling signal 163 of the AD conversion unit 73, the effect of an unstable rise of the detection signal 161 can be reduced.
[0090] The modulation signal of the primary beam 2 and the sampling signal 163 of the AD conversion unit 73 are synchronized with each other such that the effect of noise can be made uniform irrespective of the irradiation positions of the primary beam 2 on the specimen. In the example of
[0091] In addition, in the above-described configuration, by allowing the AD conversion unit 73 to further sample the detection signal as the digital signal based on the sampling signal under the condition satisfying the sampling theorem, the AD conversion can be performed at the fixed sampling frequency irrespective of the modulation frequency of the detection signal. The sampling frequency of the AD conversion unit 73 may be controlled in association with the modulation frequency of the detection signal. In this case, the sampling frequency of the AD conversion unit 73 is synchronized with the modulation frequency of the detection signal, and the phase difference between the sampling period of the AD conversion unit 73 and the modulation period of the detection signal is adjusted. As a result, the effect of an unstable rise of the detection signal 161 can be reduced.
[0092] It is also effective to filter the input digital signal through a high-pass filter or a low-pass filter to suppress a noise component of other than the desired frequency (S03). Next, in the synchronous detection unit 74, the sampled digital signal is multiplied by the reference signal output from the phase adjustment unit 76 (S04). The reference signal may be a digital signal converted from an analog signal or may be a digital signal or a fixed value generated in the computer 71. In addition, the signal waveform of the reference signal may be a sine wave or may be a square wave.
[0093] Instead of sequentially multiplying the sampled digital signals, the sampled digital signal may be temporarily stored in a storage device of the computer 71 in a one-dimensional form or a two-dimensional form (for example, in an image form), and the stored digital signal may be collectively multiplied by the reference signal that is also generated in a one-dimensional form or a two-dimensional form. Here, storing in a one-dimensional form represents that the digital signals or the reference signals taken in based on the sampling signal are sequentially arranged in a time series and stored. The signals that are arranged in a time series may be digital signals that are taken in or may be the results obtained by performing either or both of filtering and arithmetic processing on the digital signals. In addition, data stored in a one-dimensional form may be data regarding only one irradiation position or may be one-dimensional form data where data regarding a plurality of irradiation positions are arranged in a time series. Storing in a two-dimensional form represents storing a plurality of pieces of one-dimensional form data. A plurality of pieces of the same one-dimensional form data may be stored, or different one-dimensional form data may be stored.
[0094] Next, a low-pass filter 77 outputs a desired signal component from a value obtained by multiplying the reference signal and the digital signal by each other (S05), and the control unit 78 images the output of the low-pass filter 77 (S06). At this time, for example, integration of data in a given period or movement integration may be used instead of the low-pass filter 77. In addition, the output data of the low-pass filter may be averaged to construct data of one pixel.
[0095] The digital frequency modulation SEM does not require the analog signal processing circuits such as the phase-sensitive detector 14, the phase adjuster 16, and the low-pass filter 17, and thus can adopt a simpler configuration than the frequency modulation SEM described in the first embodiment. Since the analog circuits are not necessary, circuit noise of the phase-sensitive detector 14 and the like can be reduced, the shape, the cutoff frequency, and the like of the filter can be freely adjusted easily, and the filter design optimum for the observation target can be achieved. This way, in the digital frequency modulation SEM, the SNR or the dynamic range of the observation image can be easily improved with the simple configuration.
[0096] Hereinabove, the present disclosure has been described using the embodiments and the modification examples. The present disclosure is not limited to the embodiments and the modification examples described above, and combinations of the configurations described in the embodiments and the modification examples or changes, replacements, deletions, and the like of a part of the components can also be made.
[0097] In addition, secondary electrons and backscattered electrons are described as the example of the signal electrons 11. However, the signal electrons 11 may be other electrons or other charged particles. In addition, light or an electromagnetic wave such as an X-ray may be detected, and the signal detection method according to the present disclosure may be used for the detection signal thereof. When the detection target is light or an electromagnetic wave such as an X-ray, a detector that detects the light or the X-ray may be used as the detector, and an optical mirror, a condenser lens, or a condensing mirror may be disposed at an appropriate position in order to detect the light or the X-ray emitted from a specimen.
[0098] In addition, the specimen 10 may be a biological specimen. The biological specimen is affected by an electron beam more strongly than an inorganic material. Therefore, it can be said that the biological specimen is an observation target that is particularly effective for use in the frequency modulation SEM according to the present disclosure. When the biological specimen is observed, the specimen needs to be observed in an environment where the biological specimen is not damaged, for example by holding the specimen in a capsule for underwater observation or by disposing the specimen in a low vacuum environment.
[0099] In addition, the SEM is described as the example of the charged particle beam device. However, the configuration and the effects of the present disclosure are not limited to the application to the SEM and are also applicable to a scanning transmission electron microscope (STEM), a device where an ion beam is used as a charged particle beam, or a device having similar configurations including the function of irradiation with a charged particle beam and the function of detecting a signal generated by the irradiation. ×
TABLE-US-00001 Reference Signs List 1: electron emission unit 2: primary beam 3: acceleration electrode 4, 7: focusing lens 5: aperture 6: chopper 8: deflector 9: objective lens 10: specimen 11: signal electron 12, 90: signal detector 13: amplifier 14: phase-sensitive detector 15: signal generator 16: phase adjuster 17, 77: low-pass filter 18, 71: computer 21: scanning signal 22: primary beam intensity 25: detection signal 27: reference signal 30, 60: enlarged view 31: X-direction scanning signal 32: Y-direction scanning signal 61: X-direction scanning signal 73: AD conversion unit 74: synchronous detection unit 75: signal generation unit 76: phase adjustment unit 78: control unit 81: sample hold circuit 82: phase adjuster 91: scintillator 92: photomultiplier tube 101: virtual detection signal 102, 162: voltage stable region 103: control voltage 111: acceleration electrode 112: deceleration electrode 120: pulsed primary beam 121: photo-excitation electron source 122: pulsed laser 123: photodetector 131: high-pass filter 141: acquired image display unit 142: signal intensity monitor 143: condition setting unit 144: phase setting unit 151: area selection unit 152: condition setting unit 161: detection signal 163: sampling signal