Method for forming pressure sensor involves filling a chamber with non compressible fluid and shaping etched cladding to convert external pressure within chamber by anisotropic stress
11441961 · 2022-09-13
Assignee
Inventors
Cpc classification
G02B6/274
PHYSICS
G02B6/022
PHYSICS
International classification
Abstract
A method for forming a pressure sensor is provided wherein an optical fibre is provided, the optical fibre comprising a core, a cladding surrounding the core, and a birefringence structure for inducing birefringence in the core. The birefringence structure comprises first and second holes enclosed within the cladding and extending parallel to the core. A portion of the optical fibre comprising of the core and the birefringence structure is encased within a chamber, wherein the chamber is defined by a housing comprising a pressure transfer element for equalising pressure between the inside and the outside of the housing. An optical sensor is provided along the core of the optical fibre. The cladding is internally etched by flowing an etchant through the first and second holes along a length of the portion of optical fibre which comprises the optical sensor so as to increase the width of the first and second holes. The chamber is filled with a substantially non-compressible fluid. Consequently, the etched cladding is shaped so as to convert an external pressure provided by the non-compressible fluid within the chamber to an anisotropic stress in the optical sensor.
Claims
1. A method for forming a pressure sensor comprising: providing an optical fibre comprising a core, a cladding surrounding the core, and a birefringence structure for inducing birefringence in the core, wherein the birefringence structure comprises first and second holes enclosed within the cladding and extending parallel to the core; encasing a portion of the optical fibre comprising the core and the birefringence structure within a chamber, wherein the chamber is defined by a housing comprising a pressure transfer element for equalising pressure between the inside and the outside of the chamber; providing an optical sensor along the core of the portion of optical fibre; internally etching the cladding by flowing an etchant through the first and second holes along a length of the portion of optical fibre which comprises the optical sensor so as to increase the width of the first and second holes; heating the cladding during the internal etching using a localised heat source so as to increase the internal etching rate in a region of the encased portion encompassing the optical sensor; and filling the chamber with a substantially non-compressible fluid; wherein the etched cladding is shaped so as to convert an external pressure provided by the non-compressible fluid within the chamber to an anisotropic stress in the optical sensor, wherein the internal etching causes the first and second holes to have a larger cross sectional area along the region of the portion encompassing the optical sensor than along another region of the portion not encompassing the optical sensor.
2. A method according to claim 1, wherein the first and second holes remain enclosed within the cladding after the internal etching.
3. A method according to claim 1, wherein the localised heat source comprises a resistive coil, a Peltier heater or an induction coil.
4. A method according to claim 1, wherein the axes of the first and second holes and the core lie within a common plane.
5. A method according to claim 1, wherein the birefringence structure further comprises third and fourth holes enclosed within the cladding and extending parallel to the core, the method further comprising: externally etching the cladding along a length of the portion of optical fibre which comprises the optical sensor so as to expose the third and fourth holes.
6. A method according to claim 5, wherein the perimeter of the externally etched cladding comprises a partial outline of the third and fourth holes.
7. A method according to claim 5, wherein said external etching is performed using laser ablation.
8. A method according to claim 7, wherein the housing further comprises a window for transmitting a laser beam directed onto the length of the portion of optical fibre.
9. A method according to claim 5, wherein external etching comprises flowing an etching fluid into the chamber and immersing the outside of the cladding in said etching fluid until the third and fourth holes are exposed.
10. A method according to claim 9, further comprising flushing the etching fluid from the chamber prior to filling the chamber with the substantially non-compressible fluid.
11. A method according to claim 5, wherein the axes of the core and the first and second holes lie within a first plane, and wherein the axes of the core and the third and fourth holes lie within a second plane, the second plane being different from the first plane.
12. A method according to claim 5, wherein the birefringence structure further comprises one or more additional holes enclosed within the cladding and extending parallel to the core, wherein the additional holes remain enclosed within the cladding after said internal and external etching.
13. A method according to claim 1, wherein the birefringence structure further comprises third and fourth holes enclosed within the cladding and extending parallel to the core, wherein the core is arranged between the first hole and the second hole, and wherein the core is arranged between the third hole and the fourth hole, and wherein the internal etching causes the first hole to merge with the fourth hole and the second hole to merge with the third hole.
14. A method according to claim 13, wherein internally etching the cladding comprises flowing an etchant through the third and fourth holes along a length of the portion of optical fibre which comprises the optical sensor so as to increase the width of the third and fourth holes.
15. A method according to claim 1, wherein the core is pre-formed to exhibit birefringence.
16. A method according to claim 1, further comprising splicing one or each end of the optical fibre protruding from the housing with a single-mode optical fibre.
17. A pressure sensor comprising: a housing defining a chamber, the housing comprising a pressure transfer element for equalising pressure between the inside and the outside of the chamber; a substantially non-compressible fluid contained within the chamber; and an optical fibre, wherein a portion of the optical fibre is encased within the chamber, the portion comprising a core, an optical sensor provided along the core, a cladding surrounding the core, and a birefringence structure for inducing birefringence in the core, wherein the birefringence structure comprises first and second holes enclosed within the cladding and extending parallel to the core, and wherein the first and second holes have a larger cross sectional area along a region of the portion encompassing the optical sensor than along another region of the portion not encompassing the optical sensor.
18. A pressure sensor according to claim 17, further comprising an etching member for enabling etching of the cladding within the chamber.
19. A pressure sensor according to claim 18, wherein the etching member comprises a conduit configured to enable a flow of etchant to and from the chamber.
20. A pressure sensor according to claim 18, wherein the cladding has a non-elliptical outline as viewed in a plane having a normal parallel to the axis of the core.
21. A pressure sensor according to claim 20, wherein the outline comprises two re-entrant features.
22. A pressure sensor according to claim 17, wherein the first and second holes are dumbbell shaped along the portion encompassing the optical sensor, when viewed in a plane having a normal parallel to the core.
23. A pressure sensor according to claim 17, wherein the optical fibre protrudes from one or each end of the encased portion.
24. A pressure sensor according to claim 17, wherein the optical sensor comprises a Fibre Bragg Grating.
25. A pressure sensor according to claim 17, wherein the pressure transfer element is a flexible member.
26. A pressure sensor according to claim 17, wherein the pressure transfer element is an orifice.
27. A system for monitoring pressure comprising: a pressure sensor according to claim 17; a light source optically coupled to the encased portion of optical fibre; and a detector configured to receive light transmitted by the light source along the optical fibre.
28. A system according to claim 27, wherein the optical sensor is configured to simultaneously reflect light at two peak wavelengths, and wherein the detector is configured to monitor the pressure of the non-compressible fluid from the difference between the two peak wavelengths.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
(1) Embodiments of the invention will now be discussed with reference to the accompanying drawings in which:
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DETAILED DESCRIPTION
(16) A first embodiment of a method for forming a pressure sensor 10 will now be discussed with reference to
(17) If the holes which are drilled into the pre-form are too large then they will collapse during the drawing process. Care is taken therefore to avoid this. An optical sensor in the form of a Fibre Bragg Grating (FBG) 5 is then formed along the core 7 by directing spatially-varying patterns of ultraviolet or infrared light onto the core 7. A photosensitive core 7, such as a germanium-doped silica fibre, is used such that the ultraviolet light creates systematic variations in the refractive index of the core 7.
(18) The first and second holes 2, 4 are cylindrical voids within the cladding 3 which form part of a birefringence structure for inducing birefringence within the core 7. These holes 2, 4 extend parallel to the core 7, on opposing sides of the core 7, and at approximately equal distances from the core 7. This is illustrated by
(19) At step 102 a portion of the length of optical fibre 1 is encased within a chamber defined by an elongate housing 11. This is shown by
(20) The optical fibre 1 is held taut between apertures provided on opposing ends of the housing 11 by clamps 13, 15 so as to extend through the chamber. The housing 11 thus fixes the length of the portion of optical fibre 1 that is contained encased so as to protect against differential thermal expansion effects on the optical fibre 1.
(21) The housing 11 is sealed at the opposing apertures through which the optical fibre 1 extends. The seals may be formed of an epoxy resin. In the event that the optical fibre 1 is metal-coated, a metal-to-metal seal may be applied for example by soldering or brazing. Suitable sealant materials include stainless steels, nickel alloys, gold-based solders and brass. Optionally, a glass-to-metal seal may be applied, for example by the use of a glass mixture having a lower melting point than the cladding 3 and the housing 11. A substantially non-compressible fluid 14 is then introduced to the chamber using one or more ports (not shown). The fluid 14 could be one of a variety of inert liquid. Suitable examples include mineral oil, silicone oil, grease or a liquid metal based on gallium or indium and their alloys. In other examples this fluid 14 is introduced to the chamber before the portion of optical fibre 1 is encased within the housing 11.
(22) The housing 11 is formed of a corrosion resistant alloy, such as Inconel (RTM), capable of resisting the harsh environments found within a well of a hydrocarbon reserve. The housing 11 comprises a pressure transfer element in the form of a flexible diaphragm 12 that forms part of the walls surrounding the optical fibre 1. The diaphragm 12 may be located anywhere along the housing 11 so as to form a barrier between the fluid 14 contained within and any surrounding fluids that are outside of the housing 11. In the present embodiment the diaphragm 12 forms a discrete part of the walls of the housing 11 however the diaphragm 12 may alternatively fully surround the encased portion of optical fibre 1. The diaphragm 12 is typically formed of a corrosion resistant flexible material and so may comprise the same material as the remainder of the housing 11 (e.g. Inconel (RTM)), albeit made sufficiently thin so as to flex without breaking under normal operating conditions. The diaphragm 12 is configured to flex so as to transmit a hydrostatic pressure applied to the outside of the housing 11 into the fluid 14 so as to equalise the hydrostatic pressure on opposing sides of the diaphragm 12. In other embodiments bellows may be used instead of the diaphragm 12. Alternatively, the pressure transfer element may take the form of an aperture which is open so as to expose the substantially non-compressible fluid 14 to any surrounding process fluid. In this case, a substantially non-compressible fluid 14 may be used which is immiscible with the surrounding process fluid.
(23) The housing 11 may be constructed so as to isolate the encased portion of optical fibre 1 from any axial stresses caused by thermal expansion of the housing 11. For example, the housing 11 may be further formed of one or more low-expansion materials (such as Invar (RTM), other nickel-iron alloys, Kovar (RTM) or a carbon fibre composite). Alternatively, the portion of optical fibre 1 may be held slightly slack between opposing ends of the chamber so as to compensate from any axial expansion of the chamber. Such axial stresses would not typically affect any pressure measurements however they could interfere with any temperature measurements obtained using the FBG 5.
(24) At step 103, with the portion of optical fibre 1 encased within the housing 11, an etching process is performed. In the first embodiment the optical fibre 1 is etched internally only. A liquid etchant is flowed through the first and second holes 2, 4 through the portion of optical fibre 1 encased within the housing and along the direction indicated by the rightward pointing arrows in
(25) The etchant will etch the cladding 3 at a predictable rate so as to increase the diameter of the first and second holes 2, 4, as illustrated by
(26) The first and second holes 2, 4 are located sufficiently towards the centre of the cladding 3 so that if the internal etching were allowed to continue, the etchant would eventually come into contact with the core 7, which could degrade its optical transmission properties. Further internal etching would then cause the first and second holes 2, 4 to become exposed to the non-compressible fluid 14. The etchant is therefore passed along the first and second holes 2, 4 for a predetermined amount of time so as to increase the diameter of the first and second holes 2, 4 by a controlled amount, without bringing the etchant into contact with the core 7. Typically the diameter of the first and second holes 2, 4 is increased from 10 micrometres to 25-35 micrometres by the internal etching. Depending on the width of the cladding 3, wider first and second holes 2, 4 may be desirable. For example, if the cladding is 280 micrometres in diameter, the first and second holes 2, 4 may be internally etched to achieve respective diameters of around 100 micrometres.
(27) The etchant is then flushed from the first and second holes 2, 4 at step 104, for example using an inert liquid such as water. This liquid may then be ejected from the first and second holes 2, 4, for example using a jet of hot air. After the internal etching, the first and second holes 2, 4 remain enclosed within the cladding 3 and each of the core 7 and the first and second holes 2, 4 remain separate and non-interconnected within the optical waveguide 1. In an alternative embodiment the FBG 5 may be written onto the optical fibre 1 only after the etching process is complete.
(28) At step 105 the opposing ends of the length of optical fibre 1 held by the grips 13, 15 are spliced onto first and second single mode optical fibres 18, 19 respectively. The pressure sensor 20 of
(29) The single mode optical fibres 18, 19 are typically solid fibres having a core and a cladding with diameters of 9 and 125 micrometres respectively, and a mode field diameter of approximately 10 micrometres at 1550 nm. These fibres are widely used for transmitting signals reliably over long distances. It is therefore advantageous to couple the optical fibre 1 to such fibres 18, 19 at either end to ensure compatibility with any peripheral components to the system that may be provided and to increase the ease of any additional splicing that may be required for coupling such components to the pressure sensor 20.
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(31) Increases in pressure within each of the pressure sensors 20, 20′, 20″ will increase the birefringence along the encased portions of optical fibre. This will cause two distinct signals to be reflected at different peak wavelengths by each FBG. The difference in peak wavelength between these signals is measured by the detector 24 and the pressure acting on the sensors 20, 20′, 20″ is calculated from this. U.S. Pat. No. 5,841,131 provides an example of how the birefringent pressure sensor operates and the pressure may be calculated from changes in a peak wavelength.
(32) An optical fibre-based system is therefore provided for measuring the pressure at a plurality of locations along a single waveguide. Advantageously therefore, if such a system were implemented within a high pressure environment such as within a hydrocarbon well, the number of penetrations through each of the pressure barriers that are required for accommodating the system is limited to one. This is practically easier to implement and reduces the number of potential leak points.
(33) A particular benefit of the above technique is that the cladding 3 is etched whilst the optical fibre 1 is supported within the housing 11 that goes on to form part of the pressure sensor 20. In contrast, if the optical fibre 1 were not supported within the housing 11 during the etching, significant stresses could be applied to the fibre through handling it. For example, if the optical fibre 1 were bent even slightly, the stresses would be concentrated in the region where the cladding 3 was thinnest. It would therefore not be possible to remove as much cladding material via etching without making the fibre susceptible to breaking apart when handled. However, since the etched optical fibre 1 no longer requires further handling in order to incorporate it within the pressure sensor, more cladding may be removed during etching and so the sensitivity of the pressure sensor may be increased.
(34) Further embodiments of the invention will now be discussed which introduce further developments on the first embodiment. Similar components described and illustrated take an identical form to the first embodiment unless stated otherwise. In a second embodiment, illustrated by
(35) When the liquid etchant is then conveyed along the first and second holes 32, 34 at step 103, the etching rate will be increased where the temperature of the cladding 33 is higher. The internal etching may thus be controlled so as to produce enlarged voids 36, 38 within the first and second holes 32, 34 respectively along a specific region that encompasses the FBG 35. The birefringence may thus be increased at this region, without compromising the structural integrity of the remainder of the optical fibre 31. These voids 36, 38 have a diameter of 45 micrometres whereas the remainder of the first and second holes 32, 34 have a diameter of 25 micrometres.
(36) Typically the liquid etchant used is BOE (as before). A useful feature of BOE is the etching rate approximately doubles for every 10 degrees Celsius increase in temperature, within an operating range of 20-80 degrees Celsius. Thus, the increased etching may be carefully predicted in advance in accordance from the temperature profile of the cladding 33. Useful temperature ranges are generally in the region of 20 to 80 degrees Celsius.
(37) A third embodiment of a method for forming a pressure sensor 80 will now be discussed with reference to
(38) The third and fourth holes 56, 58 are initially fully enclosed within the cladding 53 such that the cladding has a circular profile (as before). At step 103 however a liquid etchant is introduced into the chamber through an inlet 68 whereupon it comes into contact with the outside of the cladding 53. Typically the etchant is continuously circulated through the chamber via the inlet 68 and an outlet 69 during this stage. The etchant is allowed to etch the cladding 53, generally reducing its diameter, until the cladding material between each of the third and fourth holes 56, 58 and the outside of the optical fibre 51 is removed, thereby exposing the third and fourth holes 56, 58 to the liquid etchant. At this point the optical fibre 51 no longer has a circular profile, when viewed along a plane perpendicular to the core 57. Instead this profile now comprises a partial outline of the third and fourth holes 56, 58, these holes forming respective re-entrant features for the cladding 53. The cladding 53 thereby has a cross-sectional outline in the form of a bow tie profile, as illustrated by
(39) The liquid etchant will etch the cladding 53 approximately equally around its circumference during the external etching. The first and second holes 52, 54 are provided radially inwards of the third and fourth holes 56, 58 however and so these will remain enclosed by the cladding 53 at the point that the third and fourth holes 56, 58 are exposed. At this moment, the liquid etchant is flushed from the chamber through the outlet 69 so as to prevent unwanted removal of cladding material either between the third and fourth holes 56, 58, or the between either of the first and second holes 52, 54 and the outside of the cladding 53. The substantially non-compressible fluid may be introduced into the chamber via the inlet 68 to help achieve this flushing. The flow of liquid into and out from the chamber via the outlet 69 is indicated by the vertical arrows in
(40) The housing 61 may therefore advantageously provide the dual-purpose of providing a container for the liquid etchant and then subsequently containing the substantially non-compressible fluid. This improves the simplicity of the method for forming the pressure sensor 80.
(41) Internal etching typically occurs either during the external etching or afterwards, with either the etchant or the substantially non-compressible fluid which surrounds the optical fibre 51 being used as a medium to transfer heat from the heating element 66 to the cladding 53. Optionally no such surrounding fluid is provided during this stage however. After the internal etching, the ends of the optical fibre 51 which trail from the apertures of the housing 61 are spliced onto respective single mode optical fibres 78, 79, as before. Advantageously, unlike the portion of the optical fibre 51 which has been subject to external etching, these ends have a circular profile that corresponds to the profile of the single mode optical fibres 78, 79. These ends will therefore be practically easier to splice together whilst maintaining a good optical coupling. The completed pressure sensor 80 having single mode optical fibres 78, 79 spliced onto either end of the birefringent optical fibre 51 is shown by
(42) A cross-sectional end view of an optical fibre 71 in accordance with a fourth embodiment is illustrated by
(43) Optionally, the same light source may be used to perform two or more of: writing the FBG onto the core 77, heating the cladding 73 during internal etching, ablating the cladding 73 during external etching and transmitting a pulse of light along the core 77 during subsequent pressure monitoring.
(44) A fifth embodiment of a pressure sensor will now be discussed with reference to
(45) Two pairs of parallel holes are initially drilled into the cladding of a pre-form which is then drawn so as to form the optical fibre 91 having a cross-sectional outline shown by
(46) An optical sensor is formed on the core 97. A portion of the optical fibre 91 comprising the optical sensor is positioned within a chamber having a pressure transfer element, and the chamber is then filled with an inert fluid (as before). A heating element is provided so as to heat the portion of the optical fibre 91 within the chamber via the surrounding fluid. An internal etching process is then performed during which a liquid etchant is flowed through each of the first, second, third and fourth holes 92, 94, 96, 98 so as to remove a portion of the surrounding cladding 93. A higher etching rate occurs along the heated portion of the optical fibre 91 (as occurred in the second embodiment). The diameter of each of these holes 92, 94, 96, 98 is thereby enlarged until the first hole 92 coalesces with the fourth hole 98, and the second hole 94, coalesces with the third hole 96—each along the heated portion. Care is taken not to merge any portions of the holes that extend outside of the chamber (where the birefringence structure is comparatively weak). At this point the etchant is flushed from the holes 92, 94, 96, 98 so as to prevent the first and third, or second and fourth holes from merging, and to prevent any of the holes 92, 94, 96, 98 from coming into contact with the core 97.
(47) A cross sectional view of the resulting structure is shown by
(48) The core 97 is positioned midway between the centre of the etched holes 92′, 94′. The thickness of cladding 93 separating the core 97 from the outside of the optical fibre 91 therefore varies significantly about the rotational axis of the core 97. This thickness is relatively high for the sectors not encompassing the first or second etched holes 92′, 94′ and relatively low for the sectors encompassing the first or second etched holes 92′, 94′. Isotropic forces applied to the outside of the encased portion of optical fibre 91 are therefore converted into anisotropic stress on the core 97 with a high level of asymmetry (without the need for external etching). This can lead to relatively large changes in the birefringence of the optical sensor and so the formation of a pressure sensor having a particularly high sensitivity.
(49) In an alternative embodiment, dumbbell-shaped holes may be formed along the encased portion of optical fibre without flowing an etchant along the third and fourth holes. For example the etchant may be flowed through the first and second holes only until these holes combine with the fourth and third holes respectively.
(50) In a further embodiment (not illustrated) one or more additional holes (in addition to the four already discussed) may be provided within the cladding. These holes will extend parallel to the core and remain enclosed within the cladding after any internal and external etching processes. Desirable levels of birefringence may hence be induced according to these techniques.
(51) In a further embodiment, the core may be pre-formed so as to exhibit birefringence. For example, an elliptical core could be used. The birefringence structure may also comprise stress rods. The rods may be inserted into holes drilled in the preform to form a “PANDA” fibre. Alternatively, doped regions may be provided outside the core to induce anisotropic stress in the core. For example, the preform may comprise regions of the cladding formed of highly-doped silica glass that has a different coefficient of thermal expansion (CTE) from the surrounding cladding. When the fibre cools from the drawing process, this difference in CTE causes different parts of the fibre will contract by different amounts, thereby creating stress-induced birefringence in the core. This forms a “BOWTIE” fibre. The birefringence is then modulated in response to changes in pressure supplied by the substantially non-compressible fluid by the birefringence structure.
(52) The above techniques may be used in any combination with the other embodiments disclosed.
(53) It is envisaged that the pressure sensor and system herein will be particularly useful for acquiring pressure measurements within lubricating and cooling fluid conduits in pumps, motors, compressors and other subsea machinery used by the oil and gas industry. Other potential uses include internal and external measurements of process fluid in Electrical Submersible Pumps for oil recovery. The system typically has a low-mass and does not require protection from electromagnetic interference. This makes it well suited for acquiring pressure readings within aircrafts, in particular along their hydraulic systems. Furthermore, the pressure sensors are non-intrusive, making them well suited for process pressure measurements. Such pressure sensors could therefore be integrated into components such as valves and seals, providing additional functionality and potentially enhancing the effectiveness and safety of process plants.
(54) As will be appreciated, a pressure sensor is therefore provided which offers improved sensitivity over the prior art. This pressure sensor is relatively simple and therefore inexpensive to construct. Furthermore the pressure sensor may be constructed so as to be physically smaller than some prior art sensors. It may also be used as part of a system for monitoring pressure that is resistant to high pressure and temperature environments and requires no additional electrical cabling that could provide potential leak points within high pressure environments.