VARIABLE-POROSITY FILTERING APPARATUS HAVING COMPRESSIBLE FILTERING MEDIUM
20220062797 · 2022-03-03
Inventors
Cpc classification
B01D2201/0423
PERFORMING OPERATIONS; TRANSPORTING
B01D39/04
PERFORMING OPERATIONS; TRANSPORTING
B01D24/042
PERFORMING OPERATIONS; TRANSPORTING
International classification
B01D24/04
PERFORMING OPERATIONS; TRANSPORTING
B01D24/46
PERFORMING OPERATIONS; TRANSPORTING
Abstract
A filtering apparatus has a volume-changeable filtering chamber having one or more flexible enclosing walls and receiving therein a compressible porous filtering medium, a fluid inlet coupled to the filtering chamber for introducing an input fluid stream with impurities into the filtering chamber, a fluid outlet coupled to the filtering chamber for discharging a filtered fluid stream from the filtering chamber, and a volume-changing structure coupled to or in association with the filtering chamber, adapted to permit increasing or decreasing of the volume of the filtering chamber so as to compress or decompress the compressible porous filtering medium therein so as to correspondingly adjust the pore size of the compressible porous filtering medium in said filtering chamber. A method for flushing a compressible filter media, and a method of variably adjusting the amount of filtering, is further disclosed and claimed.
Claims
1. A filtering apparatus comprising: a volume-changeable filtering chamber having one or more flexible enclosing walls and containing therein a compressible porous filtering medium; a fluid inlet coupled to the filtering chamber for introducing an input fluid stream with impurities into the filtering chamber; a fluid outlet coupled to the filtering chamber for discharging a filtered fluid stream from the filtering chamber; and a volume-changing structure coupled to or in association with the volume-changeable filtering chamber, adapted to permit increasing or decreasing of the volume of the volume-changeable filtering chamber so as to compress or decompress the compressible porous filtering medium therein so as to correspondingly decrease or increase the pore size of the compressible porous filtering medium in said filtering chamber.
2. The filtering apparatus of claim 1, wherein said volume-changeable filtering chamber comprises a thin, resiliently flexible, substantially impermeable elongate bladder contained within said filtering chamber.
3. The filtering apparatus of claim 1, wherein said volume-changing structure further comprises: a vessel comprising the volume-changeable filtering chamber with the fluid inlet and the fluid outlet extending out of the vessel; wherein the vessel comprises: a pressure-adjustment medium in an annulus between the filtering chamber and the vessel; and a pressure-adjustment port in fluid communication with the annulus between the filtering chamber and the vessel for adjusting the pressure of the pressure-adjustment medium.
4. The filtering apparatus as claimed in any one of claims 1 to 3, wherein the pressure-adjustment medium is a fluid.
5. The filtering apparatus as claimed in any one of claims 1 to 3, wherein the compressible porous filter medium is a filter medium selected from the group of filter mediums consisting of crushed walnut shells, activated carbon, and an extrusion blown moldable thermoplastic vulcanatizate.
6. The filtering apparatus as claimed in claim 1, wherein: (i) the volume-changing structure comprises at least one moveable piston, and the volume of said volume-changing structure may be changed by movement of said piston,
7. The filtering apparatus as claimed in claim 6, further wherein: (ii) said volume-changeable filtering chamber comprises an elongate bladder formed of a resiliently-flexible material; and (iii) said elongate bladder is situated in said volume-changing structure.
8. A method of filtering a fluid containing a contaminant, comprising the steps of: (i) applying a pressure to an exterior of an elongate resiliently-flexible bladder containing therewithin a compressible filtering medium, so as to compress said compressible filtering medium; (ii) directing a contaminant-laden fluid stream into an inlet end of said resiliently-flexible bladder, and causing filtered fluid to exit an outlet end of said resiliently-flexible bladder; (ii) when desired to flush said compressed filter media, reducing pressure applied to an exterior of said resiliently-flexible bladder and thus reducing pressure applied to said filter media in said resiliently-flexible bladder and permitting said compressible media in said resiliently-flexible bladder to expand; and (iii) directing a flushing fluid into said outlet end of said resiliently-flexible bladder and causing said flushing fluid to exit said inlet end of said resiliently-flexible bladder.
9. The method as claimed in claim 8, wherein the step of reducing pressure to said resiliently-flexible bladder comprises reducing a pressure of fluid which is supplied to a region surrounding an exterior of said resiliently-flexible bladder.
10. The method as claimed in claim 8, wherein the step of reducing pressure to said elongate hollow bladder comprises the step of reducing a force that a moveable piston is applying against a portion of said resiliently-flexible bladder.
11. A method of filtering a fluid containing a contaminant, comprising the steps of: (i) applying a pressure to an exterior of an elongate resiliently-flexible bladder containing therewithin a compressible filtering medium, so as to compress said compressible filtering medium; (ii) directing a contaminant-laden fluid stream into an inlet end of said resiliently-flexible bladder, and causing filtered fluid to exit an outlet end of said resiliently-flexible bladder; (ii) when desired to reduce a concentration of contaminant in said contaminant-laden fluid stream, increasing pressure applied to about an exterior of said resiliently-flexible bladder and thus increase pressure applied to said filter media in said resiliently-flexible bladder so as to further compress said filter media in said resiliently-flexible bladder.
12. The method of claim 11, wherein the increased pressure applied to an exterior of the resiliently-flexible bladder decreases its porosity by at least 10%.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
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DETAILED DESCRIPTION OF SOME PREFERRED EMBODIMENTS OF THE INVENTION
[0050] With reference to
[0051] The pressure-adjustment port 104 is in fluid communication with a suitable pressuring device such as a pump (not shown) for adjusting the pressure in the outer vessel using a suitable pneumatic or hydraulic pressure-adjustment medium. For example, in some embodiments, the pressure-adjustment medium may be a suitable gas-phase medium such as air, CO.sub.2, N.sub.2, and/or the like. In some other embodiments, the pressure-adjustment medium may be a suitable liquid-phase medium such as water, oil, and/or the like.
[0052] The filtering structure 106 comprises a filtering chamber 108 receiving therein a porous filtering medium 110. The filtering chamber 108 is coupled to and in fluid communication with a fluid inlet 112 and a fluid outlet 114 via an inlet screen 116 and an outlet screen 118, respectively. The fluid inlet 112 extends out of the outer vessel 102 for receiving a “contaminated” input fluid stream 122 having a target fluid with impurities, and injecting the input fluid stream 122 into the filtering chamber 108 via the inlet member 116, which retains the filter medium 110 in close proximity thereto so as to be able to resist the downstream force of pressurized inlet fluid being introduced to the filter medium 110. The fluid outlet 114 extends out of the outer vessel 102 for discharging out of the vessel 102 via the outlet member 118 which likewise retains the filter medium 110 in close proximity thereto so as to be able to resist the reversed force of pressurized fluid being introduced to the filter medium 110 during a cleaning cycle During normal operation, however, the fluid outlet generally receives a filtered stream generally comprising the target fluid but substantially without the impurities originally entrained in such target fluid.
[0053] In these embodiments, the input fluid stream 122 may be a liquid such as water, oil, and/or the like, with solid impurities. However, those skilled in the art would appreciate that, in other embodiments, the input fluid stream 122 may be in any suitable form. For example, the target fluid may be gas and/or liquid. The impurities may be gas, liquid, and/or solids or combinations thereof.
[0054] The filtering medium 110 may be a suitable material for forming a porous volume in the filtering chamber 108 for filtering the solid impurities from the liquid, with the pore structure, shape, size, and/or porosity being adjustable under pressure or upon changing of the volume of the filtering chamber 108.
[0055] In some embodiments, the filtering medium 110 may be in the form of particles such as crushed walnut shells, activated carbon, and/or the like, with suitable shapes, sizes, and/or compressibilities which, when located in the filtering chamber 108, may form a porous layer, or volume with the particle density thereof and thus the pore characteristics thereof being variably adjustable upon application of pressure or upon changing of the volume of the filtering chamber 108.
[0056] In some embodiments, the filtering medium 110 may be in the form of one or more spongy materials deformable under pressure, such as Viprene™, such being a trademark of Alliance Polymers and Services Ltd. of Westand, Mich. for an extrusion blow-moldable thermoplastic vulcanizate that can be press blow molded, suction blow molded, or 3D sequential coextruded, so as to be comprised of a plurality of micron-sized pores substantially uniformly dispersed throughout.
[0057] In these embodiments, the flexible exterior 126 of the filtering chamber 108 is impermeable with respect to the input fluid stream 122, and is volume-changeable under external pressure for adjusting the pore structure, shape, or size, and/or porosity of the filtering medium 110 therein. For example, in the embodiment shown in
[0058] The rubber sleeve 126 may change volume under pressure. For example, as shown in
[0059] As shown in
[0060] As shown in
[0061]
[0062] As shown, the filtering apparatus 100 comprises a tubular vessel 102 removably coupled to two end couplings 132 and 134 on the opposite ends thereof with one end coupling 132 comprising the fluid inlet 112 and the other end coupling 134 comprising the fluid outlet 114. The tubular vessel 102 comprises a pressure-adjustment port 104 thereon intermediate the fluid inlet and outlet 112 and 114.
[0063] In one embodiments, the tubular vessel 102 may be a steel pipe with a length of 48″ (i.e., 48 inches) or 1219 millimeter (mm) and an outer diameter (OD) of 4¼″ or 108 mm. The pressure-adjustment port 104 is a ½″ or 13 mm National Pipe Taper (NPT; American National Standard Taper Pipe Thread) Thredolet® (Thredolet is a registered trademark of Bonney Forge Corporation of Mt Union, Pa., U.S.A.).
[0064] As shown in
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[0066] The end coupling 134 in these embodiments comprises an angled stopper 142, an insert 144, a needle-roller thrust bearing 146, and a threaded pipe cap 148. As shown in
[0067] The insert 144 comprises a cylindrical main body 156 with an OD slightly smaller than the enlarged ID of the tubular vessel 102, a cylindrical distal end 158 of a smaller OD, and a substantially conical frustum shaped proximal portion 160 with the OD at the distal end thereof greater than that at the proximal end thereof. The insert 144 has suitable dimensions such that, when it is received into the ID-enlarged end of the tubular vessel 102 and the impermeable flexible tubing member, the angled outer surface of the proximal portion 160 forces and traps the flared end of impermeable flexible tubing 126 against s the angled inner surface of the angled stopper 142 to affix an end of the rubber sleeve 126 therebetween. One or more O-rings 162 may be used to seal the insert 144 against the inner surface of the tubular vessel 102. The insert 144 also comprises a longitudinal bore 164 forming the fluid outlet 114. In these embodiments, the fluid outlet 114 (and also the fluid inlet 112) has a diameter of ½″ or 13 mm.
[0068] The needle-roller thrust bearing 146 is coupled to the insert 144 about the cylindrical distal end 158 thereof. The threaded pipe cap 148 comprises a sidewall 166 with threads 171 on the inner surface thereof and an end wall 168 having a bore 170 for extending the cylindrical distal end 158 of the insert 144 therethrough. The threaded pipe cap 148 is coupled to the ID-enlarged end of the tubular vessel 102 by engaging the threads 171 on its inner surface with corresponding threads (not shown) on the outer surface of the ID-enlarged end of the tubular vessel 102. The end wall 168 of the threaded pipe cap 148 presses the insert 144 to firmly retain the end of the rubber sleeve 126 in place.
[0069] The filtering apparatus 100 in these embodiments may be used for filtering an input fluid such as produced water with a flowrate of about 12 gallons per minute (gpm) per square-foot (gpm/ft.sup.2) to about 25 gpm/ft.sup.2 at approximately 1.5″ diameter. The impurities or contaminant of the input fluid is about 20 parts per million (ppm) to about 100 ppm oil and suspended solids with mean particle-size of about 5 micron (i.e., micrometer, μm) to 25 μm. The pressure difference between the pressure in the tubular vessel 102 (i.e., exterior to the rubber sleeve 126) and that in the rubber sleeve 126 is adjustable between about 10 pounds per square inch (psi) and about 1000 psi.
[0070] The operation of the filtering apparatus 100 is similar that described above. In particular, by adjusting the pressure in the tubular vessel 102 via the pressure-adjustment port 104, the volume of the rubber sleeve 126 is thereby varied, thereby adjusting the porosity and/or the pore size of the filtering medium 110 therein for filtering specific sizes of impurities, or for flushing.
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[0072] Similar to the filtering apparatus in above-described embodiments, in these embodiments, the position of the piston 202 may be adjusted to change the volume of the filtering chamber 108 to compress or decompress the filtering medium 110 within rubber sleeve 126, for thereby adjusting the pore characteristics and pore size of such filtering medium 110 to achieve various filtering performances or for flushing, as shown in
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Experimental Test Equipment and Test Procedure and Results
[0074] Test Apparatus and Test Procedure
[0075] A test apparatus as shown in
[0076] In the test apparatus used and as shown in
TABLE-US-00001 TABLE 1 (Non-limiting) Compressible Media “A” and “B” Tested: Compressible Crushed walnut shells, of relatively low Filter compressibility, of 10-12 mesh size Media “A” Compressible an extrusion blow moldable thermoplastic vulcanizate Filter made by Alliance Polymers And Services, LLC of Media “B” Romulus, Michigan, marketed under the unregistered Trademark Viprene ™, of relatively high compressibility. Viprene can be press blow molded, suction blow molded, or 3D sequential coextruded, and be optimized with specific compressibility or measured hardness, from a 45A-50D hardness temperatures ranging from 40° F. to 347° F. while retaining flexibility. Vipren ™ used was a “series G”, of a hardness of 45A-50D.
[0077] During forward flow or normal filtering operation, the contaminated fluid stream ‘A’ was directed through fluid inlet 700 in media filtering system 520 where it entered resiliently-flexible bladder 126 formed of synthetic impermeable rubber.
[0078] Oil droplet size was measured by the FlowCam 8000 series device made by Fluid Imaging Technologies, and the Oil-In-Water (OIW) concentration (in parts per million “ppm”) was measured by an InfraCal 2 device manufactured by Spectro Scientific. OIW was further validated through the services of an independent third party.
[0079] Pressure gauges 525 and 527 were used to measure the differential pressure drop across the filter media 110, they each having been calibrated beforehand with calibration certificates.
[0080] Pressure gauge 526 was further used and calibrated to measure the fluid pressure (hereinafter “overburden pressure”) applied to the inner annular space 600 surrounding resiliently-flexible bladder 126, which was used in compressing and decompressing resiliently-flexible bladder 126 to thereby adjust the amount of compression of the filter media 126, and thus adjust the porosity of the filter media 126.
[0081] Oil used was API 26, and the average inlet loading to fluid inlet 700 was 50 ppm, with an average inlet oil droplet size of 21-26 microns.
[0082] Table II below sets out additional test parameters used, as follows:
TABLE-US-00002 TABLE II Inlet Flow rate 510 cm.sup.3/min Inlet Oil Pump Rate 0.03 mL/min Initial Cross-sectional area of filter 1320 mm.sup.2 media in interior of resiliently-flexible bladder 126 Overburden pressure Variable (0 psi, 20 psi, 40psi) Temperature 21-25° C.
[0083] During forward flow, the contaminated fluid “A” was provide to the top fluid inlet 700 of the filter media system 520, flows through the tightly packed filter media 110 in resiliently-flexible bladder 126, and filtered fluid ‘Z” leaves from the outlet end 701 of apparatus 520. Pressurized water was provided, from reservoir 527 via pump 528 to interstitial area 600 between the exterior of the vessel and the resiliently-flexible bladder 126, to allow further compression of filter media, in an increment of 20 psi, from 0 psi to 40 psi.
[0084] Treated fluid ‘Z’ thereafter was flowed to a volumetric free oil knock out 550, which aided in capturing any free oil that is entrained in the outlet stream of the filter, before the filtered fluid ‘Z’ passed to a disposal tank 560. Sample points 529 and b were used to measure oil droplet size and concentration, at both the inlet 700 and the outlet 701 respectively.
[0085] The design allowed for allows for fluid pressure to be applied at aperture ‘B” to the interstitial region 600 thus allowing for varying levels of compressibility applied to the filter resiliently-flexible bladder 126.
Analysis and Findings
[0086] Pore volume and porosity testing was conducted to confirm the effect of increasing the amount of compression of the filter media, and thus thereby decreasing the pore size (interstitial spaces) within the respective Media A and Media B.
[0087] The amount of fluid fill space in each media A and B was first measured. Thereafter, the overburden pressure applied in incremental 10 psi increments, from 0 psi to 100 psi, and the amount of liquid pushed out of the resiliently-flexible bladder containing the respective Media A or Media B was recorded. Knowing the volume of media needed to fill the system, the pore volume and porosity was then calculated as a percentage.
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[0089] As may be seen from
[0090] Using Media A, and measured values for oil concentration at fluid outlet 701 as compared to fluid inlet, over a 24 hour run of contaminated fluid being supplied, the following results were obtained:
TABLE-US-00003 TABLE III Average removal efficiency for Media A at various porosity reductions Overburden Pressure (which Average Contaminant from FIG. 14 may be calibreated Removal Efficiency to porosity reduction (%) 0 psi <80% 20 psi 96% 40 psi 98%
[0091] By reference to
[0092] Further similar testing was likewise conducted with both Media B and Media A, but using a constant overburden pressure of 20 psig. Table IV below sets out results obtained as to Average removal efficiency
TABLE-US-00004 TABLE IV 48 Hour Run with Media A & B, at 20 psi OB, 50 ppm oil inlet oil loading MEDIA Avg. Removal Efficiency Media A 92% Media B 96%
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[0094] As may be seen from
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[0096] As may be seen from
[0097] In full-scale applications, there is thus a design advantage in implementing the invention and method of the present invention, using a compressible media having a compressibility resulting in a reduction in porosity of ˜10% (in this case 12%), which results in an increased filtration capability capable, at least using these parameters, of a reduction of ˜200-300% in parts per million concentration at a fluid outlet of the compressible media system.
[0098] Accordingly, among other things, the test apparatus of