WATER-CONTAINING LIPSTICK AND PREPARATION METHOD THEREFOR

20210299015 · 2021-09-30

    Inventors

    Cpc classification

    International classification

    Abstract

    The invention provides a water-containing lipstick and preparation method therefor, said water-containing lipstick comprises the following components in terms of weight percentage: Emollient 20-40%, Hardener 13-15%, Brightener 10-15%, Polyglyceryl-2-Triisostearate 10-15%, Polyglyceryl-2-Diisostearate 10-15%, Pigment 0.5-5%, Lake 0.5%-5% and Humectant 10%. The water-containing lipstick of the invention has high level of water content which can reach 10%, can add different kinds of water soluble ingredients, has high stability, dropping point can reach 56-60° C., excellent effect of emulsification, no ultrasonic equipment is required to eliminate bubbles when filling the mould (can use general filling equipment). This lipstick has various colors and high saturation, it can be easily distinguished after using on the lips.

    Claims

    1. A water-containing lipstick, wherein the water-containing lipstick comprises the following components in terms of weight percentage: Emollient 20-40%, Hardener 13-15%, Brightener 10-15%, Polyglyceryl-2-Triisostearate 10-15%, Polyglyceryl-2-Diisostearate 10-15%, Pigment 0.5-5%, Lake 0.5%-5% and Humectant 10%.

    2. The water-containing lipstick of claim 1, wherein, said Emollient comprises any one component or the combination of at least two components of Polyoxyethylene Glyceryl Ether Cocoate, Ethylhexyl Palmitate, Olea europaea(Olive) Fruit Oil, Simmondsia chinensis(Jojoba) Seed Oil, Coconut Oil, Cocoamidopropyl Betaine, Octyl Methoxycinnamate, Meadowfoam Seed Oil, Dipolyhydroxystearate, Octyl 4-Methoxycinnamate or Avobenzone.

    3. The water-containing lipstick of claim 1, wherein, said Hardener comprises any one component or the combination of at least two components of Bees Wax, Carnauba Wax, Polyethylene or Methyl Cellulose.

    4. The water-containing lipstick of claim 1, wherein, said Brightener comprises any one component or the combination of at least two components of Cetyl Ethylhexanoate, Squalane Oil or Tri(Tridecyl) Benzene-1,2,4-Tricarboxylate.

    5. The water-containing lipstick of claim 1, wherein, said Pigment comprises any one of Iron Oxide Red, Beta-Carotene, Iron Oxide Yellow, Iron Oxide Black, Black Bean Red, Sorghum Red, Monascus Red, Black Currant Red, Hippophae Rhamnoides Yellow, Buddleia Yellow, Hibiscetin or Gardenia Yellow. Preferably, said Lake comprises any one of Amaranth Red Aluminium Lake, Ponceau 4R Altiminium Lake, Erythrosine Aluminium Lake, New Red Aluminium Lake or Tartrazine Aluminium Lake.

    6. The water-containing lipstick of claim 1, wherein, said Humectant comprises any one component or the combination of at least two components of Hyaluronic Acid, Chondroitin Sulfate, Aloe, Monocaprylin, Glycerol, Propylene Glycol, 1,2-Pentanediol or Water.

    7. The water-containing lipstick of claim 1, wherein, said water-containing lipstick also comprises Antioxidant, Spice and Preservative. Preferably, total weight percentage of said Antioxidant, Spice and Preservative is 0.5-2%. Preferably, said Antioxidant comprises any one component or the combination of at least two components of Butylated Hydroxytoluene, Tocopherol, Tea Polyphenol, Lecithin, Ethoxyquin, 2,6-Di-Tert-Butylphenol, L-Ascorbyl 6-Stearate or Calcium Diascorbate. Preferably, said Spice comprises any one component or the combination of at least two components of Vanillin, Coumarin, Phenethyl Alcohol or Piperonyl Aldehyde. Preferably, said Preservative comprises any one component or the combination of at least two components of Benzoic Acid, Sodium Benzoate, Potassium Sorbate, Calcium Diacetate or ε-Pilylysine.

    8. The preparation method of making said water-containing lipstick of claim 1, wherein, said preparation method comprises the following steps. (1) Use heated and dissolved Hardener to first mix with Emollient and Brightener. Then add Polyglyceryl-2-Diisostearate and Lake to have second mixing and get lipid composition. (2) Use Polyglyceryl-2-Triisostearate, Pigment, Humectant and any Antioxidant, Preservative and Spice to have third mixing and get hydrous composition. (3) Put the hydrous composition in Step (2) into lipid composition in Step (1) to have forth mixing, then fill into mould to get said water-containing lipstick.

    9. The preparation method of claim 8, wherein, said heating temperature in Step (1) is 87-93° C. Preferably, temperatures of said first and second mixing in Step (1) are 80-85° C.

    10. The preparation method of claim 8, wherein, temperature of said third mixing in Step (2) is 80-85° C.; temperature of said forth mixing in Step (3) is 80-85° C. Preferably, said filling in Step (3) proceeds in certain filling mould. Preferably, temperature of said filling mould is 80-85° C.

    11. The preparation method of claim 8, wherein, after the forth mixing, the hydrous composition forms hydrous particles and disperse in lipid composition; and such hydrous particles are wrapped by lipid composition.

    12. The preparation method of claim 8, wherein, the forth mixing that mixed by hydrous composition and lipid composition in said Step (3) needs to be vacuum-pumping, then fill into mould to get said water-containing lipstick.

    Description

    BRIEF DESCRIPTION OF THE DRAWINGS

    [0059] Below are explanations of the invention combining with drawings.

    [0060] FIG. 1 Process flow diagram of first and second mixing.

    [0061] FIG. 2 Process flow diagram of third mixing.

    [0062] FIG. 3 Process flow diagram of forth mixing, vacuum-pumping and filling mould.

    DETAILED DESCRIPTION OF THE INVENTION

    [0063] Below are the examples further describing the art of invention. The people skilled in the art should be aware that, said examples only help to understand the invention better, but should not be the limit to the invention.

    Example 1

    [0064] The water-containing lipstick in this example comprises the following components:

    [0065] Ethylhexyl Palmitate 20%, Octyl 4-Methoxycinnamate 4%, Avobenzone 5%, Carnauba Wax 15%, Cetyl Ethylhexanoate 3%, Squalane Oil 5%, Tri(Tridecyl) Benzene-1,2,4-Tricarboxylate 2%, Polyglyceryl-2-Triisostearate 10%, Polyglyceryl-2-Diisostearate 10%, Iron Oxide Red 4%, Ponceau 4R Altiminium Lake 4.5%, Monocaprylin 1%, Tri(Tridecyl) Benzene-1,2,4-Tricarboxylate 1%, 1,2-Pentanediol 1%, water 7%, Butylated Hydroxytoluene 0.5%, Vanillin 0.5% and Potassium Sorbate 0.5%.

    [0066] As shown in FIG. 1 to FIG. 3, the preparation method comprises the following steps: [0067] (1) After heating and dissolving Carnauba Wax at 90° C., first mix it with Ethylhexyl Palmitate, Octyl 4-Methoxycinnamate, Avobenzone, Cetyl Ethylhexanoate, Squalane Oil and Tri(Tridecyl) Benzene-1,2,4-Tricarboxylate. First mixing temperature is 82° C. Then add Polyglyceryl-2-Diisostearate and Ponceau 4R Altiminium Lake to have second mixing and get lipid composition. Second mixing temperature is 82° C. [0068] (2) Mix the Polyglyceryl-2-Triisostearate, Iron Oxide Red, Monocaprylin, Tri(Tridecyl) Benzene-1,2,4-Tricarboxylate, 1,2-Pentanediol and water, stir and emulsify them. Then add Butylated Hydroxytoluene, Vanillin and Potassium Sorbate to have third mixing and get hydrous composition. Temperature of third mixing is 82° C. [0069] (3) Put the hydrous composition into lipid composition to have forth mixing at 82° C., then fill into mould to get said water-containing lipstick.

    Example 2

    [0070] The water-containing lipstick in this example comprises the following components:

    [0071] Ethylhexyl Palmitate 10%, Carnauba Wax 10%, Bees Wax 5%, Cetyl Ethyl hexanoate 15%, Polyglyceryl-2-Triisostearate 15%, Polyglyceryl-2-Diisostearate 15%, Black Currant Red 4%, Ponceau 4R Altiminium Lake 4%, water 10%, Butylated Hydroxytoluene 1%, Lecithin 0.5%, Coumarin 0.2% and Potassium Sorbate 0.3%.

    [0072] The preparation method comprises the following steps: [0073] (1) After heating and dissolving Carnauba Wax and Bees Wax at 90° C., first mix them with Ethylhexyl Palmitate and Cetyl Ethylhexanoate at 80° C. Then add Polyglyceryl-2-Diisostearate and Ponceau 4R Altiminium Lake to have second mixing and get lipid composition. Second mixing temperature is 80° C. [0074] (2) Mix the Polyglyceryl-2-Triisostearate, Black Currant Red and water, stir and emulsify them. Then add Butylated Hydroxytoluene, Lecithin, Coumarin and Potassium Sorbate to have third mixing and get hydrous composition. Temperature of third mixing is 80° C. [0075] (3) Put the hydrous composition into lipid composition to have forth mixing at 80° C., then fill into mould to get said water-containing lipstick.

    Example 3

    [0076] The water-containing lipstick in this example comprises the following components:

    [0077] Meadowfoam Seed Oil 5%, Ethylhexyl Palmitate 15%, Octyl 4-Methoxycinnamate 9%, Avobenzone 5%, Carnauba Wax 13%, Cetyl Ethylhexanoate 5%, Squalane Oil 5%, Polyglyceryl-2-Triisostearate 11%, Polyglyceryl-2-Diisostearate 11%, Black Bean Red 0.5%, Amaranth Red Aluminium Lake 4.5%, 1,2-Pentanediol and water 8%.

    [0078] The preparation method comprises the following steps: [0079] (1) After heating and dissolving Carnauba Wax at 90° C., first mix it with Meadowfoam Seed Oil, Ethylhexyl Palmitate, Octyl 4-Methoxycinnamate and, Avobenzone, Cetyl Ethylhexanoate and Squalane Oil at 85° C. Then add Polyglyceryl-2-Diisostearate and Amaranth Red Aluminium Lake to have second mixing and get lipid composition. Second mixing temperature is 85° C. [0080] (2) Mix the Polyglyceryl-2-Triisostearate, Black Bean Red, 1,2-Pentanediol and water, stir and emulsify them to get hydrous composition. The mixing temperature is 80° C. [0081] (3) Put the hydrous composition into lipid composition to have forth mixing, then fill into mould to get said water-containing lipstick.

    Contrast Example 1

    [0082] The differences between Contrast example 1 and Example 1 are, this example does not comprise Polyglyceryl-2-Triisostearate and the weight percentage of Polyglyceryl-2-Diisostearate is 30%. Besides, the other components and preparation method of making are the same with Example 1, to get water-containing lipstick.

    Contrast Example 2

    [0083] The differences between Contrast example 2 and Example 1 are, this example does not comprise Polyglyceryl-2-Diisostearate and the weight percentage of Polyglyceryl-2-Triisostearate is 30%. Besides, the other components and preparation method of making are the same with Example 1, to get water-containing lipstick.

    Contrast Example 3

    [0084] The difference between Contrast example 3 and Example 1 is, this example does not comprise Polyglyceryl-2-Triisostearate and Polyglyceryl-2-Diisostearate. Besides, the other components and preparation method of making are the same with Example 1, to get water-containing lipstick.

    Contrast Example 4

    [0085] The difference between Contrast example 4 and Example 1 is, this example does not comprise Carnauba Wax 15%. Besides, the other components and preparation method of making are the same with Example 1, to get water-containing lipstick.

    Contrast Example 5

    [0086] The differences between Contrast example 5 and Example 1 are, the preparation method in this example is: Mix all ingredients directly, stir and emulsify them, finally fill into the mould and get water-containing lipstick.

    [0087] Functional test: Conducted stability tests (dropping point test: the higher the dropping point is, the better the stability is) and user sensory test (applied the lipsticks to 200 randomly selected females, had overall evaluation through moisturizing, comfort level and coloring; full score 100, lowest score 0, the higher the mark is, the better the lipstick is) with The water-containing lipsticks made in Example 1-3 and Contrast example 1-5. Test results are shown as Table 1 below.

    TABLE-US-00001 TABLE 1 Sample Dropping point (° C.) Overall score Example 1 57 96 Example 2 59 90 Example 3 56 94 Contrast example 1 52 84 Contrast example 2 54 86 Contrast example 3 51 76 Contrast example 4 38 72 Contrast example 5 50 67

    [0088] By the comparison between Example 1-3 and Contrast example 1-3, it can be seen the invention takes effect through adding Polyglyceryl-2-Triisostearate and Polyglyceryl-2-Diisostearate together, they coordinate with each other. It will lower the stability of lipstick and influence its taste if any one is missing. When both of them are missing, the taste and stability will drop significantly. By the comparison with Contrast example 4, it can be seen the missing of Carnauba Wax will sharply lower the dropping point, reduce stability and taste. By the comparison with Contrast example 5, it can be seen if directly mixing all ingredients together, the taste of lipstick will be bad that overall score is 67 only, and the stability is low.

    [0089] Besides, the components of water-containing lipstick in the invention is complicated and mixed by reasonable percentage which provide the best effect. It has relatively high value in practical application, and it also provides a new idea in developing lipstick.

    [0090] Applicant hereby declares that, the examples described in the invention are used to introduce The water-containing lipstick and its preparation method of making, but not limit to the above preparation method; it doesn't mean the invention must be made by said specific method. The people skilled in the art should be aware that, the following aspects should exist within the scope of protection and disclosure of the invention: any improvement, equivalent substitution of ingredient, addition of auxiliary component, selection of specific approach and etc.